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1. 发明授权

US5583246A Lactone-modified organopolysiloxane compound and a process for its preparation 失效
标题翻译：内酯改性的有机聚硅氧烷化合物及其制备方法
公开(公告)号：US5583246A
公开(公告)日：1996-12-10
申请号：US573545
申请日：1995-12-15
申请人： Haruhiko Aida , Noboru Nakai , Osamu Isozaki
发明人： Haruhiko Aida , Noboru Nakai , Osamu Isozaki
IPC分类号： C08G77/445 , C07F7/04 , C08G77/02 , C08G77/42 , C09D183/04 , C09D183/06 , C07F7/18 , C07F7/08
CPC分类号： C08G77/02 , C07F7/04
摘要： The invention provides a lactone-modified organopolysiloxane compound represented by the formula ##STR1## wherein R.sub.1, R.sub.2, R.sub.3 and R.sub.4 are the same or different and each represents a methyl group, an ethyl group, a n-propyl group, an isopropyl group or a group represented by the formula ##STR2## wherein R.sub.5 is a methyl group, an ethyl group, a n-propyl group or an isopropyl group, X is a saturated divalent hydrocarbon group having 2 to 14 carbon atoms, and m is an integer of 1 to 3, provided that at least one of R.sub.1, R.sub.2, R.sub.3 and R.sub.4 is a group represented by the formula ##STR3## wherein R.sub.5, X and m are as defined above, and n is an integer of 1 to 100. The polysiloxane compound of the invention is excellent in compatibility with various organic resins.
摘要翻译：本发明提供由式（I）表示的内酯改性的有机聚硅氧烷化合物，其中R 1，R 2，R 3和R 4相同或不同，并且各自表示甲基，乙基，正丙基，异丙基或由下式表示的基团：其中R 5为甲基，乙基，正丙基或异丙基，X为碳原子数2〜14的饱和二价烃基，m为其中R 1，R 2，R 3和R 4中的至少一个是由下式表示的基团：其中R 5，X和m定义同上，n为1至100的整数。本发明的聚硅氧烷化合物与各种有机树脂的相容性优异。

2. 发明授权

US5609918A Method of forming a top coat 失效
标题翻译：形成面漆的方法
公开(公告)号：US5609918A
公开(公告)日：1997-03-11
申请号：US477613
申请日：1995-06-07
申请人： Sachio Yamaguchi, deceased , Akimasa Nakahata , Satoshi Ikushima , Yasumasa Okumura , Haruhiko Aida , Shigeo Nishiguchi , Osamu Isozaki
发明人： Sachio Yamaguchi, deceased , Akimasa Nakahata , Satoshi Ikushima , Yasumasa Okumura , Haruhiko Aida , Shigeo Nishiguchi , Osamu Isozaki
IPC分类号： B05D7/00 , C09D133/06 , C09D163/00 , C09D201/02 , B05D1/36
CPC分类号： B05D7/53 , C09D133/066 , C09D133/068 , C09D163/00 , C09D201/02
摘要： The invention provides a method of forming a top coat by forming in sequence a colored base coat on a substrate and a clear coat, the method being characterized in that at least one of the colored base coat and the clear coat is formed by a curable coating composition consisting essentially of:(a) (a-1) a resin having a hydroxyl group, a carboxyl group and an epoxy group in the same molecule, or (a-2) a mixture of a hydroxyl- and carboxyl-containing resin with a polyepoxide;(b) a silicon compound having, per molecule, at least one silanol group and/or at least one hydrolyzable group directly bound to a silicon atom; and(c) an organic solvent.
摘要翻译：本发明提供一种通过在基材上形成有色底涂层和透明涂层来形成顶涂层的方法，其特征在于，着色底涂层和透明涂层中的至少一个通过可固化涂层形成组合物基本上由以下组成：（a）（a-1）在同一分子中具有羟基，羧基和环氧基的树脂，或（a-2）含羟基和羧基的树脂与聚环氧化物（b）每分子具有至少一个硅烷醇基和/或至少一个与硅原子直接结合的可水解基团的硅化合物; 和（c）有机溶剂。

3. 发明授权

US5684095A Hydroxyl-containing polyester, polyepoxide and silicon compound 失效
标题翻译：含羟基的聚酯，聚环氧化物和硅化合物
公开(公告)号：US5684095A
公开(公告)日：1997-11-04
申请号：US678743
申请日：1996-07-11
申请人： Kotaro Morimoto , Chicara Kawamura , Noboru Nakai , Haruhiko Aida , Noboru Takoh , Satoru Ito
发明人： Kotaro Morimoto , Chicara Kawamura , Noboru Nakai , Haruhiko Aida , Noboru Takoh , Satoru Ito
IPC分类号： C08G59/28 , C08G59/70 , C08K5/5415 , C09D163/00 , C09D167/00 , C08L63/00 , C08L67/02
CPC分类号： C09D163/00 , C08G59/28 , C08G59/70 , C08K5/5415 , C09D167/00
摘要： The invention relates to a curable coating composition comprising: (a) a hydroxyl-containing polyester resin having a solubility parameter in the range of 10.0 to 12.0, (b) a polyepoxide, (c) a silicon compound having 1 to 20 silicon atoms in one molecule and represented by the rational formula SiO.sub.(4-(a+b))/2 (OR.sup.1).sub.a (OR.sup.2).sub.b (1) wherein R.sup.1 is an alkyl group having 1 to 3 carbon atoms, or a hydrogen atom, R.sup.2 is an aryl group, an aralkyl group, or a monovalent hydrocarbon group containing an ether linkage and/or ester linkage and having 4 to 24 carbon atoms, a represents a number between 0.10 to 3.95 and b represents a number between 0.05 and 1.95, provided that a+b=4 or less, (d) at least one chelate compound selected from the group consisting of aluminum chelate compounds, titanium chelate compounds, zirconium chelate compounds and tin chelate compounds, and (e) an organic solvent.
摘要翻译：本发明涉及一种可固化涂料组合物，其包含：（a）溶解度参数在10.0至12.0范围内的含羟基的聚酯树脂，（b）聚环氧化物，（c）具有1至20个硅原子的硅化合物一个分子，由合理的式（4-（a + b））/ 2（OR1）a（OR2）b（1）表示，其中R1是具有1至3个碳原子的烷基或氢原子，R2是芳基，芳烷基或含有醚键和/或酯键并具有4〜24个碳原子的一价烃基，a表示0.10〜3.95的数，b表示0.05〜1.95的数，条件是 a + b = 4以下，（d）至少一种选自铝螯合化合物，钛螯合物，锆螯合物和锡螯合物的螯合物，和（e）有机溶剂。

4. 发明授权

US6015848A Coating composition and method for application thereof 失效
标题翻译：涂料组合物及其应用方法
公开(公告)号：US6015848A
公开(公告)日：2000-01-18
申请号：US985907
申请日：1997-12-05
申请人： Satoshi Ikushima , Seiji Wada , Yasumasa Okumura , Haruhiko Aida , Motoshi Yabuta , Yoshiyuki Yukawa , Ken-ichi Hasada
发明人： Satoshi Ikushima , Seiji Wada , Yasumasa Okumura , Haruhiko Aida , Motoshi Yabuta , Yoshiyuki Yukawa , Ken-ichi Hasada
IPC分类号： C08G59/24 , C08L27/12 , C08L33/06 , C08L33/16 , C08L63/00 , C08L63/02 , C09D133/06 , C09D163/00 , C08J3/28 , C08L83/04
CPC分类号： C08L63/00 , C08G59/24 , C09D133/068 , C09D163/00 , C08L27/12 , C08L33/068 , C08L33/16 , Y10S525/922
摘要： The present invention provides a thermosetting organic solvent type coating capable of forming a cured coating film having a TUKON hardness at 20.degree. C. of 15 or more and the minimum value of dynamic modulus E' at a frequency of 110 Hz in the temperature range of 150-200.degree. C., of 1.times.1O.sup.9 dyn/cm.sup.2 or more. The cured film formed from the coating, as compared with the cured films formed from conventional organic solvent type coatings used as a top coat for automobile (e.g. an organic solvent type coating containing, as main components, a hydroxyl group-containing acrylic resin and a melamine resin, or a carboxylic-epoxy type coating), is at least equivalent in weatherability, finish appearance, acid resistance, etc. and superior in stain resistance.
摘要翻译：本发明提供一种热固性有机溶剂型涂料，其能够在20℃下的TUKON硬度形成15或更高的固化涂膜，并且在110℃的频率下在110Hz的频率下形成动态模量E'的最小值 150-200℃，为1×10 9 dyn / cm 2以上。与由用作汽车面漆的常规有机溶剂型涂料形成的固化膜（例如含有含羟基的丙烯酸树脂的主要成分的有机溶剂型涂料）相比，由涂层形成的固化膜三聚氰胺树脂或羧基环氧型涂料）在耐候性，外观，耐酸性等方面至少相当，并且耐污染性优异。

5. 发明授权

US06174965B1 Polyester resin, process for its production and its use 失效
标题翻译：聚酯树脂，其生产和使用的过程
公开(公告)号：US06174965B1
公开(公告)日：2001-01-16
申请号：US09255336
申请日：1999-02-23
申请人： Fumio Yamashita , Yoshiyuki Yukawa , Haruhiko Aida
发明人： Fumio Yamashita , Yoshiyuki Yukawa , Haruhiko Aida
IPC分类号： C08F2000
CPC分类号： C08G63/6854
摘要： The present invention provides a polyester resin having in the molecule at least one quaternary ammonium base represented by the formula (wherein X is halogen and R is alkyl), and a process for its production. The present invention further provides a pigment dispersion containing a pigment and the above polyester resin as resin for dispersion of the pigment, and also provides a coating composition containing the above pigment dispersion.
摘要翻译：本发明提供一种在分子中具有至少一个由式（其中X是卤素且R是烷基）表示的季铵碱的聚酯树脂及其制备方法。本发明还提供了含有颜料和上述聚酯树脂作为颜料分散树脂的颜料分散体，并且还提供了含有上述颜料分散体的涂料组合物。

6. 发明授权

US06395340B1 Coating composition and method for coating therewith 失效
标题翻译：涂料组合物及其涂布方法
公开(公告)号：US06395340B1
公开(公告)日：2002-05-28
申请号：US09529854
申请日：2000-04-20
申请人： Seiji Wada , Satoshi Ikushima , Haruhiko Aida , Hideo Sugai
发明人： Seiji Wada , Satoshi Ikushima , Haruhiko Aida , Hideo Sugai
IPC分类号： B05D136
CPC分类号： C08G59/50 , C09D163/00 , Y10T428/31511 , C08L2666/54
摘要： This invention provides a thermosetting organic solvent paint comprising (A) a compound having at least two alicyclic epoxy groups in one molecule and having a number average molecular weight of less than 2000, (B) a secondary amino group-containing compound and (C) a thermolatent cationically polymerizable catalyst and further, under circumstances, (D) colloidal silica, and capable of forming a rigid coating film which is hard, tough and excellent in stain resistance, and from which pollutants, if adhered, are easily removed. This invention further provides a method to form a multi-layered top coating film which comprises applying, to a material to be coated, one or more species of colored paint and one or more species of clear paint in order, said method being characterized in that the above-mentioned paint is used as a clear paint which is to be applied on the uppermost layer.
摘要翻译：本发明提供一种热固性有机溶剂涂料，其包含（A）在一个分子中具有至少两个脂环族环氧基并且数均分子量小于2000的化合物，（B）含仲氨基的化合物和（C）另外，在（D）胶体二氧化硅的情况下，还可以形成硬质，坚韧，耐污染性优异的刚性涂膜，容易除去附着污染物的情况。本发明还提供一种形成多层顶涂层的方法，该方法包括将一种或多种着色涂料和一种或多种透明涂料应用于待涂覆的材料，所述方法的特征在于：使用上述涂料作为涂布在最上层的透明涂料。

7. 发明授权

US06319557B1 Coating composition and method for application thereof 失效
标题翻译：涂料组合物及其应用方法
公开(公告)号：US06319557B1
公开(公告)日：2001-11-20
申请号：US09437145
申请日：1999-11-10
申请人： Satoshi Ikushima , Seiji Wada , Yasumasa Okumura , Haruhiko Aida , Motoshi Yabuta , Yoshiyuki Yukawa , Ken-ichi Hasada
发明人： Satoshi Ikushima , Seiji Wada , Yasumasa Okumura , Haruhiko Aida , Motoshi Yabuta , Yoshiyuki Yukawa , Ken-ichi Hasada
IPC分类号： B05D302
CPC分类号： C08L63/00 , C08G59/24 , C08L27/12 , C08L33/068 , C08L33/16 , C09D133/068 , C09D163/00 , Y10T428/31692 , Y10T428/31699 , C08L2666/04 , C08L2666/06 , C08L2666/14 , C08L2666/54
摘要： The present invention provides a thermosetting organic solvent type coating capable of forming a cured coating film having a TUKON hardness at 20° C. of 15 or more and the minimum value of dynamic modulus E′ at a frequency of 110 Hz in the temperature range of 150-200° C., of 1×109 dyn/cm or more. The cured film formed from the coating, as compared with the cured films formed from conventional organic solvent type coatings used as a top coat for automobile (e.g. an organic solvent type coating containing, as main components, a hydroxyl group-containing acrylic resin and a melamine resin, or a carboxylic-epoxy type coating), is at least equivalent in weatherabiIity, finish appearance, acid resistance, etc. and superior in stain resistance.
摘要翻译：本发明提供一种热固性有机溶剂型涂料，其能够在20℃下形成具有15℃以上的TUKON硬度的固化涂膜，在110Hz的温度范围内形成频率为110Hz的动态模量E'的最小值 150-200℃，1×10 9 dyn / cm以上。与由用作汽车面漆的常规有机溶剂型涂料形成的固化膜（例如含有含羟基的丙烯酸树脂的主要成分的有机溶剂型涂料）相比，由涂层形成的固化膜三聚氰胺树脂或羧基环氧型涂料）在耐候性，外观，耐酸性等方面至少相当，耐污染性优异。

8. 发明授权

US06262147B1 Coating composition and method for application thereof 失效
标题翻译：涂料组合物及其应用方法
公开(公告)号：US06262147B1
公开(公告)日：2001-07-17
申请号：US09384299
申请日：1999-08-26
申请人： Satoshi Ikushima , Seiji Wada , Yasumasa Okumura , Haruhiko Aida , Motoshi Yabuta , Yoshiyuki Yukawa , Ken-ichi Hasada
发明人： Satoshi Ikushima , Seiji Wada , Yasumasa Okumura , Haruhiko Aida , Motoshi Yabuta , Yoshiyuki Yukawa , Ken-ichi Hasada
IPC分类号： C08L6300
CPC分类号： C08L63/00 , C08G59/24 , C08L27/12 , C08L33/068 , C08L33/16 , C09D133/068 , C09D163/00 , Y10S525/922 , C08L2666/04 , C08L2666/06 , C08L2666/14 , C08L2666/54
摘要： The present invention provides a thermosetting organic solvent type coating capable of forming a cured coating film having a TUKON hardness at 20° C. of 15 or more and the minimum value of dynamic modulus E′ at a frequency of 110 Hz in the temperature range of 150-200° C., of 1×109 dyn/cm2 or more. The cured film formed from the coating, as compared with the cured films formed from conventional organic solvent type coatings used as a top coat for automobile (e.g. an organic solvent type coating containing, as main components, a hydroxyl group-containing acrylic resin and a melamine resin, or a carboxylic-epoxy type coating), is at least equivalent in weatherability, finish appearance, acid resistance, etc. and superior in stain resistance.
摘要翻译：本发明提供一种热固性有机溶剂型涂料，其能够在20℃下形成具有15℃以上的TUKON硬度的固化涂膜，在110Hz的温度范围内形成频率为110Hz的动态模量E'的最小值 150-200℃，1×10 9 dyn / cm 2以上。与由用作汽车面漆的常规有机溶剂型涂料形成的固化膜（例如含有含羟基的丙烯酸树脂的主要成分的有机溶剂型涂料）相比，由涂层形成的固化膜三聚氰胺树脂或羧基环氧型涂料）在耐候性，外观，耐酸性等方面至少相当，并且耐污染性优异。

9. 发明授权

US06261642B1 High-solids coating composition and method for forming topcoat using the same 失效
标题翻译：高固含量涂料组合物和使用其形成面漆的方法
公开(公告)号：US06261642B1
公开(公告)日：2001-07-17
申请号：US09462383
申请日：2000-01-07
申请人： Kenichi Nagai , Masaaki Saika , Haruhiko Aida , Motoshi Yabuta , Hiroshi Igarashi , Yasumasa Okumura
发明人： Kenichi Nagai , Masaaki Saika , Haruhiko Aida , Motoshi Yabuta , Hiroshi Igarashi , Yasumasa Okumura
IPC分类号： B05D136
CPC分类号： C09D151/003 , C08F265/04 , C08F283/12 , C08L33/066 , C09D143/04 , C09D167/00 , Y10T428/31663 , Y10T428/31678 , C08L2666/04 , C08L2666/28 , C08L2666/02 , C08L2666/10
摘要： This invention provides a thermosetting high solids coating composition comprising: (A) a copolymer prepared by polymerizing monomer components comprising (a) 30 to 50 wt. % of vinyltrimethoxysilane and/or vinyltriethoxysilane, (b) 5 to 15 wt. % of N-methylol(meth)acrylamide alkyl ether and (c) 35 to 65 wt. % of another polymerizable unsaturated monomer, (B) a hydroxyl-containing resin having a hydroxyl value of 10 to 200 mg KOH/g, and (C) a curing catalyst. This invention further provides a method for forming a topcoat using said composition. The composition of the invention achieves the following remarkable effects: it forms a coating film excellent in acid resistance and scratch resistance, and it is superior in storage stability and recoat adhesion.
摘要翻译：本发明提供了一种热固性高固体涂料组合物，其包含：（A）通过聚合单体组分制备的共聚物，所述单体组分包含（a）30至50重量％％的乙烯基三甲氧基硅烷和/或乙烯基三乙氧基硅烷，（b）5〜15wt。％的N-羟甲基（甲基）丙烯酰胺烷基醚和（c）35-65重量％％的另一种可聚合不饱和单体，（B）羟基值为10-200mg KOH / g的羟基树脂，（C）固化催化剂。本发明还提供了一种使用所述组合物形成面漆的方法。本发明的组合物具有以下显着效果：形成耐酸性和耐刮擦性优异的涂膜，其保存稳定性和再涂覆性优异。

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