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1. 发明申请

US20070088106A1 Preparation of cellulose ether products of increased viscosity and fineness 有权
标题翻译：制备纤维素醚产品的粘度和细度增加
公开(公告)号：US20070088106A1
公开(公告)日：2007-04-19
申请号：US11505278
申请日：2006-08-15
申请人： Hartwig Schlesiger , Roland Bayer , Daniel Auriel , Jurgen Engelhardt , Frank Hohl , Erik-Andreas Klohr , Arne Kull , Jorn-Bernd Pannek , Marc Schmidt
发明人： Hartwig Schlesiger , Roland Bayer , Daniel Auriel , Jurgen Engelhardt , Frank Hohl , Erik-Andreas Klohr , Arne Kull , Jorn-Bernd Pannek , Marc Schmidt
IPC分类号： C08L1/26 , C08B11/20
CPC分类号： C04B24/383 , C04B40/0039 , C04B2103/0049 , C04B2103/44 , C04B2201/10 , C08J3/005 , C08J2301/28 , C08L1/26 , C08L1/28 , C08L1/284 , C08L33/02 , C08L33/08 , C08L33/10 , C08L33/20 , C08L51/02 , C04B24/2641 , C04B28/02 , C04B24/2652 , C08L2666/02 , C08L2666/24 , C08L2666/04 , C08L2666/26 , C08L2666/14
摘要： The present invention relates to a process for preparing cellulose ether products which is characterized in that superabsorbent polymers (SAPs) are dried and milled, or mill-dried, conjointly with moist cellulose ether and also to the cellulose ether products resulting from this process.
摘要翻译：本发明涉及一种制备纤维素醚产品的方法，其特征在于将超吸收性聚合物（SAP）与湿纤维素醚一起干燥和研磨或研磨干燥，并且还涉及由该方法得到的纤维素醚产物。

2. 发明申请

US20050034636A1 Additives containing cellulose derivatives having gel-like rheological properties, use thereof in construction material systems and also a process for cement extrusion using these additives 有权
标题翻译：含有具有凝胶状流变性的纤维素衍生物的添加剂，其在建筑材料体系中的应用，以及使用这些添加剂的水泥挤出方法
公开(公告)号：US20050034636A1
公开(公告)日：2005-02-17
申请号：US10914401
申请日：2004-08-09
申请人： Hartwig Schlesiger , Roland Bayer , Frank Hohl , Arne Kull , Jurgen Engelhardt , Burkhard Kressdorf , Jorn-Bernd Pannek
发明人： Hartwig Schlesiger , Roland Bayer , Frank Hohl , Arne Kull , Jurgen Engelhardt , Burkhard Kressdorf , Jorn-Bernd Pannek
IPC分类号： B28B3/20 , C04B24/38 , C04B28/02 , C04B103/44 , C08B15/00 , C04B7/00
CPC分类号： C04B24/383 , C04B28/02 , C04B2111/00129 , C08B15/005 , C04B20/0048
摘要： A description is given of additives for the extrusion of construction material systems, characterized in that the additives comprise irreversibly crosslinked cellulose ethers having gel-like rheological properties, and the use of irreversibly crosslinked cellulose derivatives as additives for the extrusion of construction material systems and also of an extrusion process for construction material systems.
摘要翻译：给出了用于建筑材料体系挤出的添加剂的描述，其特征在于所述添加剂包括具有凝胶状流变性的不可逆交联的纤维素醚，以及使用不可逆交联的纤维素衍生物作为用于建筑材料体系挤出的添加剂的建筑材料系统的挤压工艺。

3. 发明申请

US20050080167A1 Cellulose ether composition for the extrusion of mineral shaped bodies and also a process for the extrusion of mineral shaped bodies using this cellulose ether composition 失效
标题翻译：用于挤出矿物形状体的纤维素醚组合物以及使用该纤维素醚组合物挤出矿物质体的方法
公开(公告)号：US20050080167A1
公开(公告)日：2005-04-14
申请号：US10914470
申请日：2004-08-09
申请人： Roland Bayer , Frank Hohl , Hartwig Schlesiger , Arne Kull , Jorn Pannek , Jurgen Engelhardt , Burkhard Kressdorf
发明人： Roland Bayer , Frank Hohl , Hartwig Schlesiger , Arne Kull , Jorn Pannek , Jurgen Engelhardt , Burkhard Kressdorf
IPC分类号： C08J3/20 , C04B24/24 , C04B24/38 , C04B28/00 , C04B33/13 , C04B35/63 , C04B40/00 , C04B103/44 , C08L1/26 , C08L1/28 , C08L33/08 , C08K3/34 , C08K11/00
CPC分类号： C08L1/26 , C04B28/00 , C04B40/0039 , C04B2111/00129 , C08L1/28 , C08L33/08 , C04B24/383 , C04B2103/0051 , C04B20/0048 , C04B20/002 , C08L2666/02 , C08L2666/04
摘要： A description is given of a cellulose ether composition as additive for the extrusion of mineral masses which comprises 70 to 99.9% by weight of cellulose ether and 0.1 to 30% by weight of superabsorbent polymer, as well as a process for the extrusion of mineral masses using these compositions as additive.
摘要翻译：对纤维素醚组合物作为用于挤出矿物质的添加剂的描述，其包含70至99.9重量％的纤维素醚和0.1至30重量％的超吸收性聚合物，以及用于挤出矿物质的方法使用这些组合物作为添加剂。

4. 发明申请

US20050282939A1 Storage-stable particle composition of polysaccharides and/or polysaccharide derivatives and at least one synthetic polymer, a process for production thereof and use thereof in construction material mixtures 审中-公开
标题翻译：多糖和/或多糖衍生物和至少一种合成聚合物的储存稳定的颗粒组合物，其制备方法及其在建筑材料混合物中的应用
公开(公告)号：US20050282939A1
公开(公告)日：2005-12-22
申请号：US10981016
申请日：2004-11-04
申请人： Gunter Weber , Meinolf Brackhagen , Hartwig Schlesiger , Grit Siegmund , Arne Kull , Hans-Jurgen Juhl , Roland Bayer , Erik-Andreas Klohr
发明人： Gunter Weber , Meinolf Brackhagen , Hartwig Schlesiger , Grit Siegmund , Arne Kull , Hans-Jurgen Juhl , Roland Bayer , Erik-Andreas Klohr
IPC分类号： C08J3/12 , C04B40/00 , C08B11/02 , C08J3/20 , C08L1/00 , C08L1/26 , C08L3/00 , C08K5/15
CPC分类号： C04B40/0042 , C08L1/26 , C04B24/2652 , C04B24/383 , C04B28/02 , C04B40/0046 , C04B26/02 , C08L2666/04
摘要： A description is given of particle compositions of polysaccharides and/or polysaccharide derivatives and at least one synthetic polymer and if appropriate other aids, characterized in that I. the particles contain a plurality of solid phases, II. the solid phase of the synthetic polymer being contained in the solid phase of the polysaccharide and/or polysaccharide derivative. Likewise a description is given of a process for producing these particle compositions and also of their use in construction material mixtures, for example mortars, plasters, fillers or thin-bed adhesives.
摘要翻译：给出了多糖和/或多糖衍生物和至少一种合成聚合物的颗粒组成的描述，以及适当的其它助剂，其特征在于，所述颗粒含有多个固相II。所述合成聚合物的固相包含在所述多糖和/或多糖衍生物的固相中。同样地描述了制备这些颗粒组合物的方法，以及它们在建筑材料混合物中的用途，例如灰浆，灰泥，填料或薄床粘合剂。

5. 发明授权

US07683110B2 Preparation of cellulose ether products of increased viscosity and fineness 有权
标题翻译：制备纤维素醚产品的粘度和细度增加
公开(公告)号：US07683110B2
公开(公告)日：2010-03-23
申请号：US11505278
申请日：2006-08-15
申请人： Hartwig Schlesiger , Roland Bayer , Daniel Auriel , Jürgen Engelhardt , Frank Höhl , Erik-Andreas Klohr , Arne Henning Kull , Jörn-Bernd Pannek , Marc Oliver Schmidt
发明人： Hartwig Schlesiger , Roland Bayer , Daniel Auriel , Jürgen Engelhardt , Frank Höhl , Erik-Andreas Klohr , Arne Henning Kull , Jörn-Bernd Pannek , Marc Oliver Schmidt
IPC分类号： C08L1/26 , B02C17/00
CPC分类号： C04B24/383 , C04B40/0039 , C04B2103/0049 , C04B2103/44 , C04B2201/10 , C08J3/005 , C08J2301/28 , C08L1/26 , C08L1/28 , C08L1/284 , C08L33/02 , C08L33/08 , C08L33/10 , C08L33/20 , C08L51/02 , C04B24/2641 , C04B28/02 , C04B24/2652 , C08L2666/02 , C08L2666/24 , C08L2666/04 , C08L2666/26 , C08L2666/14
摘要： The present invention relates to a process for preparing cellulose ether products which is characterized in that superabsorbent polymers (SAPs) are dried and milled, or mill-dried, conjointly with moist cellulose ether and also to the cellulose ether products resulting from this process.
摘要翻译：本发明涉及一种制备纤维素醚产品的方法，其特征在于将超吸收性聚合物（SAP）与湿纤维素醚一起干燥和研磨或研磨干燥，并且还涉及由该方法得到的纤维素醚产物。

6. 发明申请

US20050240016A1 Process for the production of methylhydroxyalkyl cellulose 审中-公开
标题翻译：生产甲基羟烷基纤维素的方法
公开(公告)号：US20050240016A1
公开(公告)日：2005-10-27
申请号：US11105679
申请日：2005-04-14
申请人： Hartwig Schlesiger , Wolfgang Dannhorn , Erik-Andreas Klohr , Martin Kowollik , Marc Schmidt
发明人： Hartwig Schlesiger , Wolfgang Dannhorn , Erik-Andreas Klohr , Martin Kowollik , Marc Schmidt
IPC分类号： C08B11/193 , C08B11/02
CPC分类号： C08B11/193
摘要： A process of producing methylhydroxyalkyl cellulose (MHAC) is described and involves in a first step (a), (i) introducing cellulose and a suspension medium into an autoclave, the suspension medium comprising 20 wt. % to 50 wt. % of chloromethane, based on the total weight of the said suspension medium, and (ii) spraying the cellulose in the autoclave with an aqueous alkali metal hydroxide solution, thereby alkalizing the cellulose and reacting the cellulose with chloromethane. In a second step (b), hydroxyalkylating agent is optionally introduced into the autoclave at a temperature above 60° C. In a third step (c) alkali metal hydroxide is introduced into the autoclave in a hyperstoichiometric quantity of at least +0.1 mol eq., relative to the chloromethane utilised. In a fourth step (d), at least one hydroxyalkylating agent is optionally introduced into the autoclave at a temperature above 60° C., and the introduced hydroxyalkylating agent is allowed to react for at least 20 min. In a fifth step (e), additional chloromethane is introduced into the autoclave in a hyperstoichiometric quantity of at least +0.2 mol eq., relative to the total alkali metal hydroxide utilised up to this point. In a sixth step (f), additional alkali metal hydroxide is optionally introduced into the autoclave, and the reaction is allowed to continue at a temperature of from 60° C. to 110° C. Finally, the suspension medium is removed by means of distillation, thus forming a distillate comprising residual chloromethane, and the methylhydroxyalkyl cellulose is isolated. Optionally, the isolated methylhydroxyalkyl cellulose may be washed, and dried. The addition of hydroxyalkylating agent occurs in step (b) and/or step (d).
摘要翻译：描述了生产甲基羟烷基纤维素（MHAC）的方法，并涉及第一步（a），（i）将纤维素和悬浮介质引入高压釜中，所述悬浮介质包含20wt。％至50重量％％的氯甲烷，基于所述悬浮介质的总重量，和（ii）用碱金属氢氧化物水溶液在高压釜中喷涂纤维素，由此碱化纤维素并使纤维素与氯甲烷反应。在第二步（b）中，任选地将羟烷基化试剂在高于60℃的温度下引入高压釜中。在第三步骤（c）中，将碱金属氢氧化物以高化学计量的至少+0.1mol当量相对于所用的氯甲烷。在第四步骤（d）中，任选地在高于60℃的温度下将至少一种羟烷基化剂引入高压釜中，使引入的羟烷基化剂反应至少20分钟。在第五步（e）中，相对于直到此为止使用的总碱金属氢氧化物，额外的氯甲烷以至少+0.2mol当量的超化学计量量被引入高压釜中。在第六步（f）中，任选地将另外的碱金属氢氧化物引入高压釜中，使反应在60℃至110℃的温度下继续。最后，通过蒸馏，从而形成包含残余氯甲烷的馏出物，并分离甲基羟烷基纤维素。任选地，分离的甲基羟烷基纤维素可以被洗涤并干燥。羟化烷基化剂的添加发生在步骤（b）和/或步骤（d）中。

7. 发明授权

US07371279B2 Cellulose ether composition 有权
标题翻译：纤维素醚组成
公开(公告)号：US07371279B2
公开(公告)日：2008-05-13
申请号：US11475406
申请日：2006-06-27
申请人： Roland Bayer , Hartwig Schlesiger , Daniel Auriel
发明人： Roland Bayer , Hartwig Schlesiger , Daniel Auriel
IPC分类号： C04B24/38
CPC分类号： C04B40/0042 , C04B24/38 , C04B28/02 , C04B40/00 , C04B2111/00129 , C04B24/26 , C04B24/32 , C04B24/383 , C04B24/168 , C04B2103/32 , C04B2103/50
摘要： A composition comprising cellulose ether, a superplasticizer and defoamer suitable for use as an additive in extruding inorganic compositions is disclosed. The inventive composition functions as a water retention agent, plasticizer and lubricant in the extrusion of inorganic compositions. The use of the inventive composition in the extrusion of building materials leads to improved processing properties, to a higher surface quality and product properties of the extruded article.
摘要翻译：公开了包含纤维素醚，超增塑剂和消泡剂的组合物，其适合用作挤出无机组合物中的添加剂。本发明的组合物在无机组合物的挤出中起到保水剂，增塑剂和润滑剂的作用。在建筑材料的挤出中使用本发明的组合物导致改进的加工性能，更高的表面质量和挤压制品的产品性能。

8. 发明申请

US20070004826A1 Cellulose ether composition 有权
标题翻译：纤维素醚组成
公开(公告)号：US20070004826A1
公开(公告)日：2007-01-04
申请号：US11475406
申请日：2006-06-27
申请人： Roland Bayer , Hartwig Schlesiger , Daniel Auriel
发明人： Roland Bayer , Hartwig Schlesiger , Daniel Auriel
IPC分类号： C08L5/00
CPC分类号： C04B40/0042 , C04B24/38 , C04B28/02 , C04B40/00 , C04B2111/00129 , C04B24/26 , C04B24/32 , C04B24/383 , C04B24/168 , C04B2103/32 , C04B2103/50
摘要： A composition comprising cellulose ether, a superplasticizer and defoamer suitable for use as an additive in extruding inorganic compositions is disclosed. The inventive composition functions as a water retention agent, plasticizer and lubricant in the extrusion of inorganic compositions. The use of the inventive composition in the extrusion of building materials leads to improved processing properties, to a higher surface quality and product properties of the extruded article.
摘要翻译：公开了包含纤维素醚，超增塑剂和消泡剂的组合物，其适合用作挤出无机组合物中的添加剂。本发明的组合物在无机组合物的挤出中起到保水剂，增塑剂和润滑剂的作用。在建筑材料的挤出中使用本发明的组合物导致改进的加工性能，更高的表面质量和挤压制品的产品性能。

9. 发明授权

US08197699B2 Process for preparing methylhydroxyalkylcellulose having a small number of coloured particles 有权
标题翻译：制备具有少量着色颗粒的甲基羟烷基纤维素的方法
公开(公告)号：US08197699B2
公开(公告)日：2012-06-12
申请号：US11522218
申请日：2006-09-15
申请人： Martin Kowollik , Wolfgang Dannhorn , Erik-Andreas Klohr , Hartwig Schlesiger , Bernhard Kranz , Helmut Holste , Gerd Sonnenberg
发明人： Martin Kowollik , Wolfgang Dannhorn , Erik-Andreas Klohr , Hartwig Schlesiger , Bernhard Kranz , Helmut Holste , Gerd Sonnenberg
IPC分类号： B01D37/00
CPC分类号： B01D33/06 , B01D33/073 , C08B11/193 , C08B11/20 , C08B11/22
摘要： The present invention describes a process for preparing methylhydroxyalkylcellulose having a small number of colored particles by separation of methylhydroxyalkylcellulose from aqueous suspension with subsequent washing of the methylhydroxyalkylcellulose using a specially equipped rotary pressure filter.
摘要翻译：本发明描述了一种通过从水性悬浮液中分离甲基羟基烷基纤维素来制备具有少量着色颗粒的甲基羟基烷基纤维素的方法，随后使用专门设置的旋转压滤器洗涤甲基羟烷基纤维素。

10. 发明授权

US07402668B2 Process of preparing alkylhydroxyalkylcellulose 有权
标题翻译：制备烷基羟烷基纤维素的方法
公开(公告)号：US07402668B2
公开(公告)日：2008-07-22
申请号：US10197070
申请日：2002-07-17
申请人： Wolfgang Dannhorn , Erik-Andreas Klohr , Martin Kowollik , Hartwig Schlesiger , Jörn-Bernd Pannek
发明人： Wolfgang Dannhorn , Erik-Andreas Klohr , Martin Kowollik , Hartwig Schlesiger , Jörn-Bernd Pannek
IPC分类号： C07H1/00 , C08B11/08 , C08B11/02 , C08B1/00
CPC分类号： C08B11/193
摘要： A process of preparing alkylhydroxyalkylcellulose (e.g., methylhydroxyethylcellulose and methylhydroxypropylcellulose) by reaction of cellulose in the presence of alkali metal hydroxide with an alkylating agent and a hydroxyalkylating agent is described. The process includes: (a) alkalizing cellulose by means of 0.9 to 2.9 equivalents of an alkali metal hydroxide I/AGU of the cellulose in the form of an aqueous alkali metal hydroxide solution, in the presence of a suspension medium containing at least 0.2 equivalents of an alkylating agent I/AGU of the cellulose; (b) reacting the alkalized cellulose of step (a) with alkylating agent I and a hydroxyalkylating agent at a temperature above 65° C.; (c) adding additional alkali metal hydroxide 11 in the form of an aqueous alkali metal hydroxide solution; and (d) adding additional alkylating agent 11 in an amount of at least the absolute value of the difference between (i) the number of equivalents of alkylating agent I/AGU of the cellulose already added, and (ii) the total number of equivalents of alkali metal hydroxide/AGU of the cellulose added. Additional alkylating agent 11 is not added in step (d) if (i) the number of equivalents of alkylating agent I/AGU of the cellulose already added exceeds (ii) the total number of equivalents of alkali metal hydroxide/AGU of the cellulose already added. In a further step (e), the alkylhydroxyalkylcellulose is isolated from the reaction mixture. The isolated alkylhydroxyalkylcellulose may be optionally purified.
摘要翻译：描述了通过在碱金属氢氧化物存在下纤维素与烷基化剂和羟烷基化剂反应来制备烷基羟烷基纤维素（例如甲基羟乙基纤维素和甲基羟丙基纤维素）的方法。该方法包括：（a）在含有至少0.2当量的悬浮介质存在下，通过0.9至2.9当量的碱金属氢氧化物I / AGU将纤维素碱化为碱金属氢氧化物水溶液形式的纤维素碱化纤维素的纤维素的烷基化剂I / AGU; （b）在高于65℃的温度下使步骤（a）的碱化纤维素与烷基化剂I和羟烷基化剂反应; （c）加入碱金属氢氧化物水溶液形式的另外的碱金属氢氧化物11; 和（d）添加额外的烷基化剂11，其量至少为（i）已经加入的纤维素的烷基化剂I / AGU的当量数之间的差异的绝对值，和（ii）总当量数的碱金属氢氧化物/ AGU的纤维素加入。如果（i）已经加入的纤维素的烷基化剂I / AGU的当量数超过（ii）已经在纤维素中的碱金属氢氧化物/ AGU的当量的总数，则在步骤（d）中不加入另外的烷基化剂11 添加。在另外的步骤（e）中，从反应混合物中分离烷基羟烷基纤维素。分离的烷基羟烷基纤维素可以任选地纯化。

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