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1. 发明申请

US20110031103A1 Method and Apparatus For Removal Of Oil From Utility Gas Stream 审中-公开
标题翻译：用于从有用气体流中除去油的方法和装置
公开(公告)号：US20110031103A1
公开(公告)日：2011-02-10
申请号：US12921532
申请日：2009-03-18
申请人： Harry W. Deckman , Preeti Kamakoti , Peter I. Ravikovitch , Bruce T. Kelley , Paul Scott Northrop , Peter C. Rasmussen , Paul Lawrence Tanaka , Martin N. Webster , Wieslaw Jerzy Roth , Edward W. Corcoran
发明人： Harry W. Deckman , Preeti Kamakoti , Peter I. Ravikovitch , Bruce T. Kelley , Paul Scott Northrop , Peter C. Rasmussen , Paul Lawrence Tanaka , Martin N. Webster , Wieslaw Jerzy Roth , Edward W. Corcoran
IPC分类号： B01D53/047 , B01D3/00
CPC分类号： B01D53/04 , B01D53/0407 , B01D53/0438 , B01D53/0462 , B01D53/047 , B01D53/0473 , B01D53/0476 , B01D2253/102 , B01D2253/104 , B01D2253/108 , B01D2253/1085 , B01D2253/1124 , B01D2253/20 , B01D2253/204 , B01D2253/342 , B01D2257/70 , B01D2259/40088 , F04D29/124
摘要： The present application is directed to a method and system for preparing gaseous utility streams from gaseous process streams, particularly, removing oil contamination from such streams prior to use in a dry gas seal. The methods and systems may include at least one kinetic swing adsorption process including pressure swing adsorption, temperature swing adsorption, calcination, and inert purge processes to treat gaseous streams for use in dry gas seals of rotating equipment such as compressors, turbines and pumps and other utilities. The adsorbent materials used include a high surface area solid structured microporous and mesoporous materials.
摘要翻译：本申请涉及一种用于从气态工艺流中制备气体有用物流的方法和系统，特别是在干燥气体密封中使用之前，从这些流中除去油污染物。所述方法和系统可以包括至少一个动态挥发吸附过程，包括变压吸附，变温吸附，煅烧和惰性吹扫工艺，以处理用于诸如压缩机，涡轮机和泵等旋转设备的干气密封中的气流公用事业使用的吸附剂材料包括高表面积的固体结构微孔和介孔材料。

2. 发明授权

US09126138B2 Method and apparatus for removal of oil from utility gas stream 有权
标题翻译：从有用气流中除去油的方法和装置
公开(公告)号：US09126138B2
公开(公告)日：2015-09-08
申请号：US12921532
申请日：2009-03-18
申请人： Harry W. Deckman , Preeti Kamakoti , Peter I. Ravikovitch , Bruce T. Kelley , Paul Scott Northrop , Peter C. Rasmussen , Paul Lawrence Tanaka , Martin N. Webster , Wieslaw Jerzy Roth , Edward W. Corcoran
发明人： Harry W. Deckman , Preeti Kamakoti , Peter I. Ravikovitch , Bruce T. Kelley , Paul Scott Northrop , Peter C. Rasmussen , Paul Lawrence Tanaka , Martin N. Webster , Wieslaw Jerzy Roth , Edward W. Corcoran
IPC分类号： B01D53/02 , B01D53/04 , B01D53/047
CPC分类号： B01D53/04 , B01D53/0407 , B01D53/0438 , B01D53/0462 , B01D53/047 , B01D53/0473 , B01D53/0476 , B01D2253/102 , B01D2253/104 , B01D2253/108 , B01D2253/1085 , B01D2253/1124 , B01D2253/20 , B01D2253/204 , B01D2253/342 , B01D2257/70 , B01D2259/40088 , F04D29/124
摘要： The present application is directed to a method and system for preparing gaseous utility streams from gaseous process streams, particularly, removing oil contamination from such streams prior to use in a dry gas seal. The methods and systems may include at least one kinetic swing adsorption process including pressure swing adsorption, temperature swing adsorption, calcination, and inert purge processes to treat gaseous streams for use in dry gas seals of rotating equipment such as compressors, turbines and pumps and other utilities. The adsorbent materials used include a high surface area solid structured microporous and mesoporous materials.
摘要翻译：本申请涉及一种用于从气态工艺流中制备气体有用物流的方法和系统，特别是在干燥气体密封中使用之前，从这些流中除去油污染物。所述方法和系统可以包括至少一个动态挥发吸附过程，包括变压吸附，变温吸附，煅烧和惰性吹扫工艺，以处理用于诸如压缩机，涡轮机和泵等旋转设备的干气密封中的气流公用事业使用的吸附剂材料包括高表面积的固体结构微孔和介孔材料。

3. 发明授权

US07038100B2 Aromatics alkylation 有权
公开(公告)号：US07038100B2
公开(公告)日：2006-05-02
申请号：US09845856
申请日：2001-04-30
申请人： Ajit B. Dandekar , John P. McWilliams , Thomas Francis Degnan , Michael Hryniszak , Donald J. Klocke , Wieslaw Jerzy Roth
发明人： Ajit B. Dandekar , John P. McWilliams , Thomas Francis Degnan , Michael Hryniszak , Donald J. Klocke , Wieslaw Jerzy Roth
IPC分类号： C07C2/66
CPC分类号： C07C2/66 , C07C2529/70 , Y02P20/52 , C07C15/02 , C07C15/085
摘要： The present invention provides a process for producing an alkylaromatic compound comprising the step of contacting an alkylatable aromatic compound with an alkylating agent under alkylation conditions in the presence of a alkylation catalyst comprising phosphorus and a porous crystalline inorganic oxide material having an X-ray diffraction pattern including the d-spacing maxima at 12.4±0.25, 6.9±0.15, 3.57±0.07 and 3.42±0.07 Angstrom.

4. 发明授权

US07569739B2 Aromatics alkylation 有权
标题翻译：芳烃烷基化
公开(公告)号：US07569739B2
公开(公告)日：2009-08-04
申请号：US11873865
申请日：2007-10-17
申请人： Ajit B. Dandekar , John P. McWilliams , Thomas Francis Degnan , Michael Hryniszak , Donald J. Klocke , Wieslaw Jerzy Roth
发明人： Ajit B. Dandekar , John P. McWilliams , Thomas Francis Degnan , Michael Hryniszak , Donald J. Klocke , Wieslaw Jerzy Roth
IPC分类号： C07C2/68
CPC分类号： C07C2/66 , C07C2529/70 , Y02P20/52 , C07C15/02 , C07C15/085
摘要： The present invention provides a process for producing an alkylaromatic compound comprising the step of contacting an alkylatable aromatic compound with an alkylating agent under alkylation conditions in the presence of a alkylation catalyst comprising phosphorus and a porous crystalline inorganic oxide material having an X-ray diffraction pattern including the d-spacing maxima at 12.4±0.25, 6.9±0.15, 3.57±0.07 and 3.42±0.07 Angstrom.
摘要翻译：本发明提供一种生产烷基芳族化合物的方法，包括使烷基化芳族化合物与烷基化剂在烷基化条件下在包含磷的烷基化催化剂和具有X射线衍射图的多孔结晶无机氧化物材料存在下接触的步骤包括12.4±0.25,6.9±0.15,3.57±0.07和3.42±0.07埃的d间距最大值。

5. 发明授权

US07297829B2 Aromatics alkylation 有权
标题翻译：芳烃烷基化
公开(公告)号：US07297829B2
公开(公告)日：2007-11-20
申请号：US11128721
申请日：2005-05-13
申请人： Ajit B. Dandekar , John P. McWilliams , Thomas Francis Degnan , Michael Hryniszak , Donald J. Klocke , Wieslaw Jerzy Roth
发明人： Ajit B. Dandekar , John P. McWilliams , Thomas Francis Degnan , Michael Hryniszak , Donald J. Klocke , Wieslaw Jerzy Roth
IPC分类号： C07C2/66
CPC分类号： C07C2/66 , C07C2529/70 , Y02P20/52 , C07C15/02 , C07C15/085
摘要： The present invention provides a process for producing an alkylaromatic compound comprising the step of contacting an alkylatable aromatic compound with an alkylating agent under alkylation conditions in the presence of a alkylation catalyst comprising phosphorus and a porous crystalline inorganic oxide material having an X-ray diffraction pattern including the d-spacing maxima at 12.4±0.25, 6.9±0.15, 3.57±0.07 and 3.42±0.07 Angstrom.
摘要翻译：本发明提供一种生产烷基芳族化合物的方法，包括使烷基化芳族化合物与烷基化剂在烷基化条件下在包含磷的烷基化催化剂和具有X射线衍射图的多孔结晶无机氧化物材料存在下接触的步骤包括12.4±0.25,6.9±0.15,3.57±0.07和3.42±0.07埃的d间距最大值。

6. 发明授权

US09296619B2 Large crystal molecular sieves and their manufacture 有权
标题翻译：大型晶体分子筛及其制造
公开(公告)号：US09296619B2
公开(公告)日：2016-03-29
申请号：US12865679
申请日：2009-01-19
申请人： Wieslaw Jerzy Roth , Carrie L. Kennedy , Thomas Yorke
发明人： Wieslaw Jerzy Roth , Carrie L. Kennedy , Thomas Yorke
IPC分类号： C07C1/20 , C01B39/38 , B01J29/06 , B01J29/40 , C01B39/46
CPC分类号： C01B39/38 , B01J29/06 , B01J29/40 , C01B39/46
摘要： A process for the manufacture of large crystal size synthetic porous crystalline molecular sieve requires an aqueous reaction mixture that is organic structure directing agent-free, has a H2O/MOH molar ratio (M is an alkali metal) of 75 or less, a source of X2O3 (X is a trivalent element) and a source of YO2 (Y is a tetravalent element). The source of X2O3 and YO2 is an amorphous material containing both X2O3 and YO2 and having a YO2/X2O3 molar ratio of 15 to 40. The resultant highly crystalline novel materials have crystals with at least one dimension greater than 1 μm, such as greater than 3 μm.
摘要翻译：制造大晶体合成多孔结晶分子筛的方法需要一种无机结构导向剂的水性反应混合物，其H 2 O / MOH摩尔比（M为碱金属）为75以下， X 2 O 3（X为三价元素）和YO 2（Y为四价元素）的源。 X 2 O 3和YO 2的源是含有X 2 O 3和YO 2并且YO 2 / X 2 O 3摩尔比为15至40的无定形材料。所得高结晶的新型材料具有至少一个尺寸大于1μm的晶体，例如大于 3μm。

7. 发明申请

US20110207983A1 Large Crystal Molecular Sieves and Their Manufacture 有权
标题翻译：大型水晶分子筛及其制造
公开(公告)号：US20110207983A1
公开(公告)日：2011-08-25
申请号：US12865679
申请日：2009-01-19
申请人： Wieslaw Jerzy Roth , Carrie L. Kennedy , Thomas Yorke
发明人： Wieslaw Jerzy Roth , Carrie L. Kennedy , Thomas Yorke
IPC分类号： C07C1/20 , C01B39/00 , C01B39/02 , C01B39/38 , C07C7/12
CPC分类号： C01B39/38 , B01J29/06 , B01J29/40 , C01B39/46
摘要： A process for the manufacture of large crystal size synthetic porous crystalline molecular sieve requires an aqueous reaction mixture that is organic structure directing agent-free, has a H2O/MOH molar ratio (M is an alkali metal) of 75 or less, a source of X2O3 (X is a trivalent element) and a source of YO2 (Y is a tetravalent element). The source of X2O3 and YO2 is an amorphous material containing both X2O3 and YO2 and having a YO2/X2O3 molar ratio of 15 to 40. The resultant highly crystalline novel materials have crystals with at least one dimension greater than 1 μm, such as greater than 3 μm.
摘要翻译：制造大晶体合成多孔结晶分子筛的方法需要一种无机结构导向剂的水性反应混合物，其H 2 O / MOH摩尔比（M为碱金属）为75以下， X 2 O 3（X为三价元素）和YO 2（Y为四价元素）的源。 X 2 O 3和YO 2的源是含有X 2 O 3和YO 2并且YO 2 / X 2 O 3摩尔比为15至40的无定形材料。所得高结晶的新型材料具有至少一个尺寸大于1μm的晶体，例如大于 3μm。

8. 发明申请

US20110044891A1 High Metal Content Molecular Sieves and Their Manufacture 审中-公开
标题翻译：高金属含量分子筛及其制造
公开(公告)号：US20110044891A1
公开(公告)日：2011-02-24
申请号：US12865686
申请日：2009-01-19
申请人： Wieslaw Jerzy Roth , Mae Koenig Rubin
发明人： Wieslaw Jerzy Roth , Mae Koenig Rubin
IPC分类号： C01B39/38 , B01D53/14 , C10G11/00 , C07C41/14 , C07C2/00 , C07C5/22 , C07C5/333 , C07C15/02 , C07C15/12 , C07C1/00 , C07C2/02 , C07B53/00 , C07C69/00
CPC分类号： C01B39/40 , B01J29/06 , B01J29/40 , C01B39/38 , C01B39/46 , C01B39/48
摘要： A process for manufacturing a synthetic porous crystalline molecular sieve requires an aqueous reaction mixture comprising a source of X2O3 (X is a trivalent element), a source of YO2 (Y is a tetravalent element) and a source of MOH (M is an alkali metal). The H2O/MOH molar ratio is within the range of 70 to 126 and the source of X2O3 and YO2 is an amorphous material containing both X2O3 and YO2 and having YO2/X2O3 molar ratio of 15 or less. The molecular sieve products are useful as catalysts and/or absorbents. Such molecular sieves having MFI structure type, TON structure type or the structure type of zeolite beta and a composition involving the molar relationship (n) YO2:X2O3 wherein n is from 2 to less than 15 are novel compositions of matter.
摘要翻译：制造合成多孔结晶分子筛的方法需要包含X 2 O 3源（X为三价元素），YO源（Y为四价元素）和MOH源（M为碱金属）的含水反应混合物）。 H 2 O / MOH摩尔比在70至126的范围内，X 2 O 3和YO 2的源是含有X 2 O 3和YO 2并且YO 2 / X 2 O 3摩尔比为15或更小的无定形材料。分子筛产物可用作催化剂和/或吸收剂。具有MFI结构类型，TON结构类型或沸石β的结构类型的分子筛和涉及摩尔关系（n）YO 2：X 2 O 3的组成，其中n为2至小于15是新物质组合物。

9. 发明授权

US5827491A Process for preparing the synthetic porous crystalline material MCM-56 失效
标题翻译：制备合成多孔结晶材料MCM-56的方法
公开(公告)号：US5827491A
公开(公告)日：1998-10-27
申请号：US684664
申请日：1996-07-22
申请人： Sean C. Emerson , Shiu Lun Anthony Fung , Stephen Latham Lawton , Wieslaw Jerzy Roth
发明人： Sean C. Emerson , Shiu Lun Anthony Fung , Stephen Latham Lawton , Wieslaw Jerzy Roth
IPC分类号： C01B33/38 , C01B39/00 , B01J29/04
CPC分类号： B01J29/70 , C01B33/38
摘要： The synthetic porous crystalline material, MCM-56, is synthesized by a process comprising the steps of: a) preparing a reaction mixture containing sources of alkali or alkaline earth metal (M) cation, an oxide of an trivalent element X, an oxide of a tetravalent element Y containing at least 30 wt. % of solid YO.sub.2, a directing agent (R), and water, said reaction mixture having a composition, in terms of mole ratios of oxides, within the following ranges: YO.sub.2 /X.sub.2 O.sub.3 5 to 35 H.sub.2 O/YO.sub.2 10 to 70 OH.sup.-- /YO.sub.2 0.05 to 0.5 M/YO.sub.2 0.05 to 3.0 R/YO.sub.2 0.1 to 1.0 b) crystallizing said mixture at a temperature of about 80.degree. C. to about 225.degree. C., preferably about 125.degree. C. to about 140.degree. C., to form crystals of MCM-56, c) terminating said crystallization prior to the formation of a significant quantity of MCM-49, and d) separating the MCM-56 crystals from the reaction mixture.
摘要翻译：合成多孔结晶材料MCM-56通过包括以下步骤的方法合成：a）制备含有碱金属或碱土金属（M）阳离子，三价元素X的氧化物，含有至少30重量％的四价元素Y。％的固体YO 2，导向剂（R）和水，所述反应混合物的组成按照氧化物的摩尔比在以下范围内：YO 2 / X 2 O 3 5至35H 2 O / YO 2 10至70 OH- / YO2 0.05〜0.5M / YO2 0.05〜3.0R / YO2 0.1〜1.0 b）在约80℃至约225℃，优选约125℃至约140℃的温度下使所述混合物结晶，以形成MCM-56的晶体，c）在形成显着量的MCM-49之前终止所述结晶，以及d）从反应混合物中分离MCM-56晶体。

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