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1. 发明授权

US5449763A Preparation of alkylpolyglycosides 失效
标题翻译：烷基多糖苷的制备
公开(公告)号：US5449763A
公开(公告)日：1995-09-12
申请号：US957333
申请日：1992-10-06
申请人： Harald P. Wulff , Paul A. Siracusa , Patricia E. Bator , Barry A. Salka , Michael W. Counts , Robert A. Aleksejczyk , Patrick M. McCurry, Jr. , Robert S. McDaniel , William G. Kozak , Allen D. Urfer , Gail Howell
发明人： Harald P. Wulff , Paul A. Siracusa , Patricia E. Bator , Barry A. Salka , Michael W. Counts , Robert A. Aleksejczyk , Patrick M. McCurry, Jr. , Robert S. McDaniel , William G. Kozak , Allen D. Urfer , Gail Howell
IPC分类号： A61K8/00 , A61K8/46 , A61K8/60 , A61K8/73 , A61Q5/02 , A61Q5/12 , A61Q11/00 , A61Q19/10 , C07G3/00 , C07H1/06 , C07H15/04 , C11D1/66 , C11D1/68 , C11D3/22 , C11D17/08 , C07H15/00 , C08B37/00
CPC分类号： C11D1/662 , A61K8/604 , A61Q11/00 , A61Q19/10 , A61Q5/02 , A61Q5/12 , C07H15/04 , A61K2800/596
摘要： A process for preparing high detergency or surfactant alkyl polyglycoside compositions and a purified alkyl monoglycoside and to compositions employing the polyglycosides for various end use applications. The process involves removal of a substantial portion of the monoglycoside present in a reaction product mixture containing alkyl polyglycosides resulting from the reaction of an alcohol and saccharide at elevated temperatures in the presence of an acid catalyst. Separation of the monoglycoside from the reaction product mixture may be carried out by molecular distillation.
摘要翻译：一种制备高洗涤剂或表面活性剂烷基多糖苷组合物和纯化烷基单糖苷的方法，以及将多糖苷用于各种最终应用的组合物。该方法包括除去在酸催化剂存在下，在高温下由醇和糖反应得到的含有烷基多糖苷的反应产物混合物中存在的大部分单糖苷。从反应产物混合物中分离单糖苷可以通过分子蒸馏进行。

2. 发明授权

US5962399A Preparation of alkylpolyglycosides and cleaning compositions comprising same 失效
标题翻译：烷基多糖苷的制备和包含其的清洁组合物
公开(公告)号：US5962399A
公开(公告)日：1999-10-05
申请号：US969254
申请日：1997-11-13
申请人： Harald P. Wulff , Paul A. Siracusa , Patricia E. Bator , Barry A. Salka , Michael W. Counts , Robert A. Aleksejczyk , Patrick M. McCurry, Jr. , Robert S. McDaniel , William G. Kozak , Allen D. Urfer , Gail Howell
发明人： Harald P. Wulff , Paul A. Siracusa , Patricia E. Bator , Barry A. Salka , Michael W. Counts , Robert A. Aleksejczyk , Patrick M. McCurry, Jr. , Robert S. McDaniel , William G. Kozak , Allen D. Urfer , Gail Howell
IPC分类号： A61K8/00 , A61K8/46 , A61K8/60 , A61K8/73 , A61Q5/02 , A61Q5/12 , A61Q11/00 , A61Q19/10 , C07G3/00 , C07H1/06 , C07H15/04 , C11D1/66 , C11D1/68 , C11D3/22 , C11D17/08 , C07H1/00 , C08B37/00
CPC分类号： C11D1/662 , A61K8/604 , A61Q11/00 , A61Q19/10 , A61Q5/02 , A61Q5/12 , C07H15/04 , A61K2800/596
摘要： A process for preparing high detergency or surfactant alkyl polyglycoside compositions and a purified alkyl monoglycoside and to compositions employing the polyglycosides for various end use applications. The process involves removal of a substantial portion of the monoglycoside present in a reaction product mixture containing alkyl polyglycosides resulting from the reaction of an alcohol and saccharide at elevated temperatures in the presence of an acid catalyst. Separation of the monoglycoside from the reaction product mixture may be carried out by molecular distillation.
摘要翻译：一种制备高洗涤剂或表面活性剂烷基多糖苷组合物和纯化烷基单糖苷的方法，以及将多糖苷用于各种最终应用的组合物。该方法包括除去在酸催化剂存在下，在高温下由醇和糖反应得到的含有烷基多糖苷的反应产物混合物中存在的大部分单糖苷。从反应产物混合物中分离单糖苷可以通过分子蒸馏进行。

3. 发明授权

US5859218A Preparation of alkylpolyglycosides 失效
公开(公告)号：US5859218A
公开(公告)日：1999-01-12
申请号：US458391
申请日：1995-06-01
申请人： Harald P. Wulff , Paul A. Siracusa , Patricia E. Bator , Barry A. Salka , Michael W. Counts , Robert A. Aleksejczyk , Patrick M. McCurry, Jr. , Robert S. McDaniel , William G. Kozak , Allen D. Urfer , Gail Howell
发明人： Harald P. Wulff , Paul A. Siracusa , Patricia E. Bator , Barry A. Salka , Michael W. Counts , Robert A. Aleksejczyk , Patrick M. McCurry, Jr. , Robert S. McDaniel , William G. Kozak , Allen D. Urfer , Gail Howell
IPC分类号： A61K8/00 , A61K8/46 , A61K8/60 , A61K8/73 , A61Q5/02 , A61Q5/12 , A61Q11/00 , A61Q19/10 , C07G3/00 , C07H1/06 , C07H15/04 , C11D1/66 , C11D1/68 , C11D3/22 , C11D17/08 , C07H1/00
CPC分类号： C11D1/662 , A61K8/604 , A61Q11/00 , A61Q19/10 , A61Q5/02 , A61Q5/12 , C07H15/04 , A61K2800/596
摘要： A process for preparing high detergency or surfactant alkyl polyglycoside compositions and a purified alkyl monoglycoside and to compositions employing the polyglycosides for various end use applications. The process involves removal of a substantial portion of the monoglycoside present in a reaction product mixture containing alkyl polyglycosides resulting from the reaction of an alcohol and saccharide at elevated temperatures in the presence of an acid catalyst. Separation of the monoglycoside from the reaction product mixture may be carried out by molecular distillation.

4. 发明授权

US5266690A Preparation of alkylpolyglycosides 失效
标题翻译：烷基多糖苷的制备
公开(公告)号：US5266690A
公开(公告)日：1993-11-30
申请号：US810588
申请日：1991-12-19
申请人： Patrick M. McCurry, Jr. , Robert S. McDaniel , William G. Kozak , Allen D. Urfer , Gail Howell
发明人： Patrick M. McCurry, Jr. , Robert S. McDaniel , William G. Kozak , Allen D. Urfer , Gail Howell
IPC分类号： A61K8/60 , A61Q5/02 , A61Q5/12 , A61Q19/10 , C07G3/00 , C07H1/06 , C07H15/04 , C11D1/66 , C07H15/00 , C08B37/00
CPC分类号： C11D1/662 , A61K8/604 , A61Q19/10 , A61Q5/02 , C07H15/04 , A61Q5/12
摘要： A process for preparing high detergency or surfactant alkyl polyglycoside compositions and a purified alkyl monoglycoside and to compositions employing the polyglycosides for various end use applications. The process involves removal of a substantial portion of the monoglycoside present in a reaction product mixture containing alkyl polyglycosides resulting from the reaction of an alcohol and saccharide at elevated temperatures in the presence of an acid catalyst. Separation of the monoglycoside from the reaction product mixture may be carried out by molecular distillation.
摘要翻译：一种制备高洗涤剂或表面活性剂烷基多糖苷组合物和纯化烷基单糖苷的方法，以及将多糖苷用于各种最终应用的组合物。该方法包括除去在酸催化剂存在下，在高温下由醇和糖反应得到的含有烷基多糖苷的反应产物混合物中存在的大部分单糖苷。从反应产物混合物中分离单糖苷可以通过分子蒸馏进行。

5. 发明授权

US5534500A Process for preparing surfactant mixtures having high solids content 失效
标题翻译：制备具有高固体含量的表面活性剂混合物的方法
公开(公告)号：US5534500A
公开(公告)日：1996-07-09
申请号：US293861
申请日：1994-08-22
申请人： Thomas Casamassina , Florencio Morales, Jr. , Barry A. Salka , John Fallon , Sureshchandra G. Desai , Patrick M. McCurry, Jr.
发明人： Thomas Casamassina , Florencio Morales, Jr. , Barry A. Salka , John Fallon , Sureshchandra G. Desai , Patrick M. McCurry, Jr.
IPC分类号： C07H15/04 , B01F17/00 , B01F17/52 , C11D1/10 , C11D1/12 , C11D1/14 , C11D1/22 , C11D1/28 , C11D1/29 , C11D1/32 , C11D1/66 , C11D1/83 , C11D9/26 , A61K31/70 , C07G3/00 , C07H1/00 , C11D9/00
CPC分类号： C11D1/83 , C11D1/10 , C11D1/123 , C11D1/126 , C11D1/143 , C11D1/146 , C11D1/22 , C11D1/28 , C11D1/29 , C11D1/32 , C11D1/662 , Y10S516/06 , Y10S516/07
摘要： Highly concentrated mixtures of surfactants are obtained by a method which comprises adding the acid form of a neutralizable surfactant to an aqueous composition comprised of a base and an alkyl polyglycoside.
摘要翻译：通过包括将酸形式的可中和表面活性剂加入到由碱和烷基多糖苷组成的含水组合物中的方法获得高度浓缩的表面活性剂混合物。

6. 发明授权

US5556950A Method for preparing stabilized alkyl glycosides 失效
标题翻译：稳定烷基糖苷的制备方法
公开(公告)号：US5556950A
公开(公告)日：1996-09-17
申请号：US873908
申请日：1992-04-24
申请人： Patrick M. McCurry, Jr. , Janet R. Varvil
发明人： Patrick M. McCurry, Jr. , Janet R. Varvil
IPC分类号： C07H15/04 , C07H15/08 , C07H1/06
CPC分类号： C07H15/08 , C07H15/04
摘要： Glycoside products having a propensity to discolor and/or to exhibit haze under aqueous alkaline or neutral pH conditions can be stabilized to substantially reduce the extent of discoloration and to essentially eliminate any haze which might also be present by adjusting the pH of an aqueous solution of the alkyl glycoside product to about 7 prior to treatment with a metal borohydride material which at the end of the reaction period is consumed resulting in a stabilized alkyl polyglycoside product which does not exhibit a haze in an aqueous solution at a pH of about 7.
摘要翻译：具有褪色倾向和/或在含水碱性或中性pH条件下显示雾度的糖苷产品可以被稳定化，以显着降低变色程度，并基本上消除任何可能通过调节水溶液烷基糖苷产物在用金属硼氢化物处理之前至约7，在反应结束时消耗，从而产生稳定的烷基多糖苷产物，其在约7的pH下在水溶液中不发生雾度。

7. 发明授权

US5831044A Process for preparation of glycosides 失效
标题翻译：糖苷的制备方法
公开(公告)号：US5831044A
公开(公告)日：1998-11-03
申请号：US597060
申请日：1996-02-05
申请人： Patrick M. McCurry, Jr. , John Frederick Hessel
发明人： Patrick M. McCurry, Jr. , John Frederick Hessel
IPC分类号： C07H15/04 , C11D3/22
CPC分类号： C07H15/04
摘要： A process for making glycosides having enhance color properties comprising the steps of: (a) reacting a reducing saccharide with excess fatty alcohol to obtain a glycoside reaction mixture; (b) adding an effective amount of an unsaturated aliphatic carboxylic acid, including hydroxy-substituted derivatives thereof and their salt, to the glycoside reaction mixture; and (c) evaporating excess fatty alcohol from the glycoside reaction mixture to form a glycoside mixture.
摘要翻译：一种制备具有增强色素性质的糖苷的方法，包括以下步骤：（a）使还原糖与过量脂肪醇反应得到糖苷反应混合物; （b）向糖苷反应混合物中加入有效量的包括其羟基取代的衍生物及其盐的不饱和脂肪族羧酸; 和（c）从糖苷反应混合物中蒸发过量的脂肪醇以形成糖苷混合物。

8. 发明授权

US5597406A Method of thickening aqueous formulations 失效
标题翻译：增稠水性制剂的方法
公开(公告)号：US5597406A
公开(公告)日：1997-01-28
申请号：US330353
申请日：1994-11-01
申请人： Stephen A. Fischer , Kartar S. Arora , Reuben Grinstein , Patrick M. McCurry, Jr. , Judith C. Giordan
发明人： Stephen A. Fischer , Kartar S. Arora , Reuben Grinstein , Patrick M. McCurry, Jr. , Judith C. Giordan
IPC分类号： A61K8/39 , A61K8/60 , A61K8/86 , A61Q5/02 , A61Q19/10 , C09D7/00 , C11D1/29 , C11D1/34 , C11D1/66 , C11D1/72 , C11D1/83 , C11D3/06 , C11D3/20 , G05D24/00 , C11D1/74
CPC分类号： A61Q19/10 , A61K8/39 , A61K8/604 , A61K8/86 , A61Q5/02 , C09D7/002 , C11D1/83 , C11D3/2044 , C11D3/2055 , C11D3/2068 , A61K2800/596 , C08L67/00 , C11D1/29 , C11D1/345 , C11D1/662 , C11D1/72 , C11D3/2048 , C11D3/2051
摘要： A composition for thickening aqueous based personal care products is comprised of a cosolvent selected from the group consisting of a diol, the mono alkyl ether of a diol, a salt of a sulfated ethoxylated alcohol, a salt of a sulfated ethoxylated alkyl phenol, and a complex organic phosphate ester; water; a nonionic surfactant and, a complex ester.
摘要翻译：用于增稠水性个人护理产品的组合物由选自二醇，二醇的单烷基醚，硫酸化乙氧基化醇的盐，硫酸化乙氧基化烷基酚的盐和复合有机磷酸酯; 水; 非离子表面活性剂和复合酯。

9. 发明授权

US5432275A Continuous bleaching of alkylpolyglycosides 失效
标题翻译：连续漂白烷基聚糖苷
公开(公告)号：US5432275A
公开(公告)日：1995-07-11
申请号：US202293
申请日：1994-02-25
申请人： Patrick M. McCurry, Jr. , James D. Beaulieu
发明人： Patrick M. McCurry, Jr. , James D. Beaulieu
IPC分类号： C07H1/06 , C07H15/04 , C08B37/00 , C07H15/00
CPC分类号： C07H15/04 , C08B37/0003
摘要： A continuous method of bleaching an alkylpolyglycoside, substantially free of alcohol, with peroxy compounds, preferably hydrogen peroxide, which is highly efficient to provide an unexpected high degree of color reduction from a dark brown to a light, which product, from an extinction coefficient color respectively of about 10 to about 15 to about 0.025 to about 0.15. The bleaching is carried out at controlled pH and temperature, under pressure preferably in the presence of Mg. The use of a prebleached heel or feed prior to introduction of the unbleached material to be bleached results in a faster approach to equilibrium, steady state, bleaching conditions which results in minimum chemical usage and more rapid production of low color.
摘要翻译：使用过氧化合物（优选过氧化氢）漂白基本上不含醇的烷基多糖苷的连续方法，该方法高效地提供从暗棕色到光的意想不到的高度的颜色还原，该消光系数颜色分别为约10至约15至约0.025至约0.15。在控制的pH和温度下，优选在Mg存在下，在压力下进行漂白。在引入待漂白的未漂白材料之前使用预先漂白的脚后跟或饲料导致更快的平衡，稳定状态，漂白条件的方法，这导致最少的化学使用和更快的低颜色生产。

10. 发明授权

US06429320B1 Processes for the purification of tocopherol and/or sterol compounds and compositions containing orthoborate ester mixtures 有权
标题翻译：纯化生育酚和/或固醇化合物和含有原硼酸酯混合物的组合物的方法
公开(公告)号：US06429320B1
公开(公告)日：2002-08-06
申请号：US09922208
申请日：2001-08-03
申请人： Patrick M. McCurry, Jr. , Stephen W. Turner , Carl Pickens
发明人： Patrick M. McCurry, Jr. , Stephen W. Turner , Carl Pickens
IPC分类号： C07D31176
CPC分类号： C07D311/72
摘要： Processes for purifying compounds are disclosed which include reacting (i) a mixture of at least one tocopherol compound or sterol compound, and an alcohol having from about 10 to 30 carbons with (i) one or more boron-containing compounds to form a second mixture of orthoborate esters, wherein the mole ratio of tocopherol, sterol and alcohol to boron is at least about 2.5:1; heating the second mixture to form a residue containing the orthoborate esters; contacting the residue with a compound capable of solvolyzing the orthoborate esters to form a third mixture including the boron-containing compound(s), the alcohol and the tocopherol and/or sterol compound(s); and recovering the tocopherol and/or sterol compound(s). Another process for purifying such compounds includes an activated carbon treatment, which may alternatively follow the other process steps; formation of borate esters; heating to remove low boiling point components; formation of a residue comprising the borate esters; contacting the residue with a compound capable of solvolyzing the borate esters; and separation of the remaining components. Compositions including mixtures of alkyl/tocopherol/sterol orthoborate esters are also disclosed.
摘要翻译：公开了用于纯化化合物的方法，其包括使（i）至少一种生育酚化合物或固醇化合物的混合物与具有约10至30个碳的醇与（i）一种或多种含硼化合物反应以形成第二混合物的正硼酸酯，其中生育酚，固醇和醇与硼的摩尔比为至少约2.5:1; 加热第二混合物以形成含有原硼酸酯的残余物; 使残余物与能够使原硼酸酯溶剂化的化合物接触以形成包含含硼化合物，醇和生育酚和/或固醇化合物的第三混合物; 并回收生育酚和/或固醇化合物。净化这些化合物的另一种方法包括活性炭处理，其可以替代地遵循其它工艺步骤; 形成硼酸酯; 加热去除低沸点组分; 形成含有硼酸酯的残渣; 使残余物与能够溶解硼酸酯的化合物接触; 并分离其余组分。还公开了包括烷基/生育酚/正硼酸甾醇酯的混合物的组合物。

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