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1. 发明申请

US20110034625A1 METHOD FOR INITIATING RADICAL POLYMERIZATIONS 有权
标题翻译：用于启动放射性聚合物的方法
公开(公告)号：US20110034625A1
公开(公告)日：2011-02-10
申请号：US12934528
申请日：2009-03-12
申请人： Harald Grassl , Jochen Mezger , Alexander Kraus , Gerhard Albrecht
发明人： Harald Grassl , Jochen Mezger , Alexander Kraus , Gerhard Albrecht
IPC分类号： C08L33/08 , C08L33/12 , C08L33/02
CPC分类号： C08F2/58
摘要： The invention relates to a process for the preparation of polymers by free radical polymerization of monomers in the presence of water, electrochemically produced free radicals being used for initiating the free radical polymerization.
摘要翻译：本发明涉及通过在水存在下自由基聚合单体制备聚合物的方法，电化学产生的自由基用于引发自由基聚合。

2. 发明授权

US08361302B2 Method for initiating radical polymerizations 有权
标题翻译：引发自由基聚合的方法
公开(公告)号：US08361302B2
公开(公告)日：2013-01-29
申请号：US12934528
申请日：2009-03-12
申请人： Harald Grassl , Jochen Mezger , Alexander Kraus , Gerhard Albrecht
发明人： Harald Grassl , Jochen Mezger , Alexander Kraus , Gerhard Albrecht
IPC分类号： C25B3/00
CPC分类号： C08F2/58
摘要： The invention relates to a process for the preparation of polymers by free radical polymerization of monomers in the presence of water, electrochemically produced free radicals being used for initiating the free radical polymerization.
摘要翻译：本发明涉及通过在水存在下自由基聚合单体制备聚合物的方法，电化学产生的自由基用于引发自由基聚合。

3. 发明授权

US07425596B2 Use of block copolymers as dispersants for aqueous suspensions of solids 失效
标题翻译：使用嵌段共聚物作为固体含水悬浮液的分散剂
公开(公告)号：US07425596B2
公开(公告)日：2008-09-16
申请号：US10525299
申请日：2003-08-13
申请人： Alexander Kraus , Christian Hübsch , Gerhard Albrecht , Harald Grassl , Angelika Hartl , Stefanie Scheul , Alfred Kern
发明人： Alexander Kraus , Christian Hübsch , Gerhard Albrecht , Harald Grassl , Angelika Hartl , Stefanie Scheul , Alfred Kern
IPC分类号： C08F20/02
CPC分类号： C08L53/00 , C04B24/2647 , C04B28/02 , C04B2103/0061 , C08F293/005
摘要： The use of block copolymers which were prepared by polymerization of a poly(alkylene oxide) compound (A) with at least one ethylenically unsaturated monomer compound (B), as dispersants for aqueous suspensions of solids, in particular based on hydraulic binders, such as, for example, cement, lime, gypsum or anhydrite, is described. Surprisingly, these block copolymers have a substantially better water-reducing power at the same dose in comparison with conventional superplasticizers based on comb polymers. Moreover, the slump loss can also be reduced in comparison with conventional superplasticizers by modification of the adhesive block.
摘要翻译：使用通过将聚（环氧烷）化合物（A）与至少一种烯属不饱和单体化合物（B）聚合制备的嵌段共聚物作为固体的水悬浮液的分散剂，特别是基于水硬性粘合剂，例如，例如，水泥，石灰，石膏或无水石膏。令人惊奇的是，与基于梳形聚合物的常规超增塑剂相比，这些嵌段共聚物在相同剂量下具有显着更好的降水功能。此外，与传统的超增塑剂相比，通过修改粘合剂块，也可以减少坍落度损失。

4. 发明授权

US08299192B2 Statistic comb polymers, method for producing the same and their use 失效
标题翻译：统计梳形聚合物，其制备方法及其用途
公开(公告)号：US08299192B2
公开(公告)日：2012-10-30
申请号：US10567260
申请日：2004-08-17
申请人： Alexander Kraus , Gerhard Albrecht , Christian Hübsch , Harald Grassl , Angelika Hartl
发明人： Alexander Kraus , Gerhard Albrecht , Christian Hübsch , Harald Grassl , Angelika Hartl
IPC分类号： C08F16/16
CPC分类号： C08F220/28 , C04B24/2647 , C04B24/267 , C04B2103/006 , C08F290/062 , C08F2438/00
摘要： Statistic comb polymers obtainable by the radical copolymerization of a vinylic poly(alkylenoxide) compound (A) with an ethylenically unsaturated monomer compound (B) according to the catalytic chain transfer method (CCT). The comb polymers are extremely suitable for hydraulic binder suspensions based on cement, lime, gypsum and anhydrite as they have, for the same dosage, an improved water reducing power over conventional flow agents. The corresponding building material mixtures are characterized by a substantially reduced stickiness and plastic viscosity once said comb polymers are added, which dramatically improves the plasticity of very cement-rich building material mixtures, such as concretes. The building material mixtures using the inventive flow agents have a considerably increased slump flow and an increased shear-thinning behavior as compared to conventional concretes without the tendency to segregate.
摘要翻译：通过乙烯基聚（亚烷基氧化物）化合物（A）与烯属不饱和单体化合物（B）根据催化链转移法（CCT）自由基共聚得到的统计梳形聚合物。梳状聚合物非常适用于基于水泥，石灰，石膏和无水石膏的水硬性粘合剂悬浮液，因为它们具有相同的剂量，比常规流动剂具有更好的减水能力。相应的建筑材料混合物的特征在于一旦所述梳状聚合物被加入时，其粘度和塑性粘度显着降低，这显着地改善了非常水泥的建筑材料混合物如混凝土的可塑性。使用本发明的流动剂的建筑材料混合物与常规混凝土相比具有显着增加的坍落度流动和增加的剪切稀化行为，而没有倾向于分离。

5. 发明授权

US07910640B2 Polycondensation product based on aromatic or heteroaromatic compounds, method for the production thereof, and use thereof 有权
标题翻译：基于芳族或杂芳族化合物的缩聚产物，其制备方法及其用途
公开(公告)号：US07910640B2
公开(公告)日：2011-03-22
申请号：US11665424
申请日：2005-10-14
申请人： Philipp Wieland , Alexander Kraus , Gerhard Albrecht , Kerstin Becher , Harald Grassl
发明人： Philipp Wieland , Alexander Kraus , Gerhard Albrecht , Kerstin Becher , Harald Grassl
IPC分类号： C04B24/12 , C04B24/28 , C08G8/18
CPC分类号： C08G12/40 , C04B24/243 , C04B24/30 , C04B24/32 , C04B2103/30 , C08G8/28
摘要： Disclosed is a polycondensation product that is a reaction product of A) an aromatic or heteroaromatic compound containing 5 to 10 C atoms or heteroatoms and is provided with an average of 1 to 300 oxyethylene groups and/or oxypropylene groups per molecule which are linked to the aromatic or heteroaromatic compound via an O atom or N atoms, and B) an aromatic compound and C) an aldehyde selected among the group of formaldehyde, glyoxylic acid, and benzaldehyde or mixtures thereof. Surprisingly, the inventive polycondensation product causes very good liquefaction of hydraulic binding agents, eg. Cement, resulting in substantially improved liquefaction of the construction material at a lower dose while pourability can be maintained over a longer period of time as opposed to naphthalene sulfonates or melamine sulfonates.
摘要翻译：公开了一种缩聚产物，其是A）含有5至10个C原子或杂原子的芳族或杂芳族化合物与每个分子平均具有1至300个氧化乙烯基团和/或氧代丙烯基团的反应产物，芳族或杂芳族化合物，以及B）芳族化合物和C）选自甲醛，乙醛酸和苯甲醛或其混合物的醛。令人惊奇的是，本发明的缩聚产物导致非常好的液压粘合剂的液化，例如。水泥，导致较低剂量的建筑材料的液化显着改善，而与萘磺酸盐或三聚氰胺磺酸盐相比，可以在更长的时间内保持可倾倒性。

6. 发明授权

US08053498B2 Pulverulent polycondensation products 有权
标题翻译：粉末缩聚产物
公开(公告)号：US08053498B2
公开(公告)日：2011-11-08
申请号：US12084212
申请日：2006-12-18
申请人： Philipp Wieland , Alexander Kraus , Gerhard Albrecht , Harald Grassl , Kerstin Becher
发明人： Philipp Wieland , Alexander Kraus , Gerhard Albrecht , Harald Grassl , Kerstin Becher
IPC分类号： C04B24/26
CPC分类号： C04B40/0042 , C04B24/166 , C04B24/246 , C04B24/30 , C04B35/63476 , C04B35/63488 , C04B2235/3217 , C04B2235/3418 , C04B2235/5409 , C04B2235/5436 , Y02W30/97 , C04B7/00 , C04B14/02 , C04B16/06 , C04B40/0028 , C04B18/24
摘要： Pulverulent polycondensation products are described, consisting of a) 5 to 95% by weight of a polycondensation product based on an aromatic or heteroaromatic compound (A) having 5 to 10 C atoms or heteroatoms having at least one oxyethylene or oxypropylene radical and one aldehyde (C) selected from the group consisting of formaldehyde, glyoxylic acid and benzaldehyde or mixtures thereof, and b) 5 to 95% by weight of a finely divided mineral carrier material having a specific surface area of 0.5 to 500 m2/g (according to BET as specified in DIN 66 131). The pulverulent polycondensation products according to the invention are outstandingly suitable in construction material mixtures in an amount of from 0.1 to 5% by weight, based on the weight of the construction material. The pulverulent polycondensation products have a number of advantages here, such as, for example, excellent storage stability, good liquefying action at low dosage and industrially simple production.
摘要翻译：描述了由以下组成的粉末缩聚产物：a）5至95重量％的基于具有5至10个碳原子的芳族或杂芳族化合物（A）的缩聚产物或具有至少一个氧乙烯或氧丙烯基和一个醛的杂原子（ C）选自甲醛，乙醛酸和苯甲醛或其混合物，和b）5至95重量％的细分矿物载体材料，其比表面积为0.5-500m2 / g（根据BET 如DIN 66 131中所规定）。根据本发明的粉状缩聚产物，以建筑材料的重量为基准，优选为0.1-5重量％的建筑材料混合物。粉状缩聚产物在这里具有许多优点，例如，优异的储存稳定性，低剂量的液化作用和工业上简单的生产。

7. 发明申请

US20090054558A1 Pulverulent Polycondensation Products 有权
标题翻译：粉末缩聚产品
公开(公告)号：US20090054558A1
公开(公告)日：2009-02-26
申请号：US12084212
申请日：2006-12-18
申请人： Philipp Wieland , Alexander Kraus , Gerhard Albrecht , Harald Grassl , Kerstin Becher
发明人： Philipp Wieland , Alexander Kraus , Gerhard Albrecht , Harald Grassl , Kerstin Becher
IPC分类号： C08L61/00 , C08L61/06 , C08K5/13 , C04B14/00 , C04B16/00 , C08K5/521 , C08K3/00 , C08K5/17 , C08K5/42 , C08K5/18 , C08K5/20 , C08K5/1535 , C08K5/3492 , C08K5/21 , C08K3/26 , C08K3/34 , C08K3/22 , C08K3/30
CPC分类号： C04B40/0042 , C04B24/166 , C04B24/246 , C04B24/30 , C04B35/63476 , C04B35/63488 , C04B2235/3217 , C04B2235/3418 , C04B2235/5409 , C04B2235/5436 , Y02W30/97 , C04B7/00 , C04B14/02 , C04B16/06 , C04B40/0028 , C04B18/24
摘要： Pulverulent polycondensation products are described, consisting of a) 5 to 95% by weight of a polycondensation product based on an aromatic or heteroaromatic compound (A) having 5 to 10 C atoms or heteroatoms having at least one oxyethylene or oxypropylene radical and one aldehyde (C) selected from the group consisting of formaldehyde, glyoxylic acid and benzaldehyde or mixtures thereof, and b) 5 to 95% by weight of a finely divided mineral carrier material having a specific surface area of 0.5 to 500 m2/g (according to BET as specified in DIN 66 131). The pulverulent polycondensation products according to the invention are outstandingly suitable in construction material mixtures in an amount of from 0.1 to 5% by weight, based on the weight of the construction material. The pulverulent polycondensation products have a number of advantages here, such as, for example, excellent storage stability, good liquefying action at low dosage and industrially simple production.
摘要翻译：描述了由以下组成的粉末缩聚产物：a）5至95重量％的基于具有5至10个碳原子的芳族或杂芳族化合物（A）的缩聚产物或具有至少一个氧乙烯或氧丙烯基和一个醛的杂原子（ C）选自甲醛，乙醛酸和苯甲醛或其混合物，和b）5至95重量％的细分矿物载体材料，其比表面积为0.5-500m2 / g（根据BET 如DIN 66 131中所规定）。根据本发明的粉状缩聚产物，以建筑材料的重量为基准，优选为0.1-5重量％的建筑材料混合物。粉状缩聚产物在这里具有许多优点，例如，优异的储存稳定性，低剂量的液化作用和工业上简单的生产。

8. 发明申请

US20080108732A1 Polycondensation Product Base on Aromatic or Heteroaromatic Compounds, Method for the Production Thereof, and Use Thereof 有权
标题翻译：芳基或杂芳族化合物的缩聚产物，其生产方法及其用途
公开(公告)号：US20080108732A1
公开(公告)日：2008-05-08
申请号：US11665424
申请日：2005-10-14
申请人： Philipp Wieland , Alexander Kraus , Gerhard Albrecht , Kerstin Becher , Harald Grassl
发明人： Philipp Wieland , Alexander Kraus , Gerhard Albrecht , Kerstin Becher , Harald Grassl
IPC分类号： C08K3/26
CPC分类号： C08G12/40 , C04B24/243 , C04B24/30 , C04B24/32 , C04B2103/30 , C08G8/28
摘要： Disclosed is a polycondensation product comprising A) an aromatic or heteroaromatic compound containing 5 to 10 C atoms or heteroatoms, said compound being provided with an average of 1 to 300 oxyethylene groups and/or oxypropylene groups per molecule which are linked to the aromatic or heteroaromatic compound via an O atom or N atom, and optionally B) an aromatic compound selected among the group comprising phenols, phenol ether, naphthols, naphthol ether, anilines, furfuryl alcohols, and/or an aminoplast former selected among the group comprising melamine (derivatives), urea (derivatives), and carboxylic acid amides, and C) an aldehyde selected among the group comprising formaldehyde, glyoxylic acid, and benzaldehyde or mixtures thereof, the benzaldehyde optionally containing acid groups in the form of COOMa, SO3Ma, and PO3Ma, wherein M=H, akali metal or alkaline earth metal, ammonium, or organic amine radicals and a=½, 1, or 2. Surprisingly, the inventive polycondensation product causes very good liquefaction of hydraulic binding agents, e.g. cement, resulting in substantially improved liquefaction of the construction material at a lower dose while pourability can be maintained over a longer period of time as opposed to naphthalene sulfonates or melamine sulfonates.
摘要翻译：公开了一种缩聚产物，其包含A）含有5至10个C原子的芳族或杂芳族化合物或杂原子，所述化合物每分子平均提供1至300个氧化乙烯基团和/或氧代丙烯基团，其与芳族或杂芳族化合物通过O原子或N原子的化合物，以及任选地B）选自苯酚，酚醚，萘酚，萘酚醚，苯胺，糠醇和/或选自三聚氰胺（衍生物）），脲（衍生物）和羧酸酰胺，和C）选自包括甲醛，乙醛酸和苯甲醛或其混合物的组中的醛，所述苯甲醛任选地含有COOM的形式的酸基，其中M = H，碱金属或碱土金属，或者其中M = H，碱金属或碱土金属，铵或有机胺基，a =½，1或2。令人惊奇的是，本发明的缩聚产物导致非常好的液压粘合剂的液化，例如水泥，导致较低剂量的建筑材料的液化显着改善，而与萘磺酸盐或三聚氰胺磺酸盐相比，可以在更长的时间内保持可倾倒性。

9. 发明申请

US20070043190A1 Statistic comb polymers, method for producing the same and their use 失效
标题翻译：统计梳形聚合物，其制备方法及其用途
公开(公告)号：US20070043190A1
公开(公告)日：2007-02-22
申请号：US10567260
申请日：2004-08-17
申请人： Alexander Kraus , Gerhard Albrecht , Christian Hubsch , Harald Grassl , Angelika Hartl
发明人： Alexander Kraus , Gerhard Albrecht , Christian Hubsch , Harald Grassl , Angelika Hartl
IPC分类号： C08F118/02
CPC分类号： C08F220/28 , C04B24/2647 , C04B24/267 , C04B2103/006 , C08F290/062 , C08F2438/00
摘要： Statistic comb polymers obtainable by the radical copolymerization of a vinylic poly(alkylenoxide) compound (A) with an ethylenically unsaturated monomer compound (B) according to the catalytic chain transfer method (CCT). The comb polymers are extremely suitable for hydraulic binder suspensions based on cement, lime, gypsum and anhydrite as they have, for the same dosage, an improved water reducing power over conventional flow agents. The corresponding building material mixtures are characterized by a substantially reduced stickiness and plastic viscosity once said comb polymers are added, which dramatically improves the plasticity of very cement-rich building material mixtures, such as concretes. The building material mixtures using the inventive flow agents have a considerably increased slump flow and an increased shear-thinning behavior as compared to conventional concretes without the tendency to segregate.
摘要翻译：通过乙烯基聚（亚烷基氧化物）化合物（A）与烯属不饱和单体化合物（B）根据催化链转移法（CCT）自由基共聚得到的统计梳形聚合物。梳状聚合物非常适用于基于水泥，石灰，石膏和无水石膏的水硬性粘合剂悬浮液，因为它们具有相同的剂量，比常规流动剂具有更好的减水能力。相应的建筑材料混合物的特征在于一旦所述梳状聚合物被加入时，其粘度和塑性粘度显着降低，这显着地改善了非常水泥的建筑材料混合物如混凝土的可塑性。使用本发明的流动剂的建筑材料混合物与常规混凝土相比具有显着增加的坍落度流动和增加的剪切稀化行为，而没有倾向于分离。

10. 发明申请

US20050228142A1 Use of block copolymers as dispersants for aqueous suspensions of solids 失效
标题翻译：使用嵌段共聚物作为固体含水悬浮液的分散剂
公开(公告)号：US20050228142A1
公开(公告)日：2005-10-13
申请号：US10525299
申请日：2003-08-13
申请人： Alexander Kraus , Christian Hubsch , Gerhard Albrecht , Harald Grassl , Angelika Hartl , Stefanie Scheul , Alfred Kern
发明人： Alexander Kraus , Christian Hubsch , Gerhard Albrecht , Harald Grassl , Angelika Hartl , Stefanie Scheul , Alfred Kern
IPC分类号： C04B24/26 , C04B24/32 , C04B103/40 , C08F293/00 , C08L53/00 , C08F20/02
CPC分类号： C08L53/00 , C04B24/2647 , C04B28/02 , C04B2103/0061 , C08F293/005
摘要： The use of block copolymers which were prepared by polymerization of a poly(alkylene oxide) compound (A) with at least one ethylenically unsaturated monomer compound (B), as dispersants for aqueous suspensions of solids, in particular based on hydraulic binders, such as, for example, cement, lime, gypsum or anhydrite, is described. Surprisingly, these block copolymers have a substantially better water-reducing power at the same dose in comparison with conventional superplasticizers based on comb polymers. Moreover, the slump loss can also be reduced in comparison with conventional superplasticizers by modification of the adhesive block.
摘要翻译：使用通过将聚（环氧烷）化合物（A）与至少一种烯属不饱和单体化合物（B）聚合制备的嵌段共聚物作为固体的水悬浮液的分散剂，特别是基于水硬性粘合剂，例如，例如，水泥，石灰，石膏或无水石膏。令人惊奇的是，与基于梳形聚合物的常规超增塑剂相比，这些嵌段共聚物在相同剂量下具有显着更好的降水功能。此外，与传统的超增塑剂相比，通过修改粘合剂块，也可以减少坍落度损失。

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