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1. 发明授权

US08828288B2 Porous, low density nanoclay composite 有权
标题翻译：多孔，低密度纳米复合材料
公开(公告)号：US08828288B2
公开(公告)日：2014-09-09
申请号：US13484322
申请日：2012-05-31
申请人： Qi Liao , Walter A. Scrivens , Philip T. Wilson , Darin L. Dotson , Hao Zhou
发明人： Qi Liao , Walter A. Scrivens , Philip T. Wilson , Darin L. Dotson , Hao Zhou
IPC分类号： B29C35/16
CPC分类号： C08K3/346 , C04B33/04 , C04B38/0045 , C04B2111/2046 , C04B2111/52 , C04B2235/349 , C04B2235/5454 , C04B2235/606 , C08J3/075 , C08J9/008 , C08J9/28 , C08J2201/0484 , C08J2305/00 , C08J2305/12 , C08J2329/04 , C08J2361/28 , C08J2389/00 , C08J2405/12 , C08K5/053 , C08L5/12 , C08L29/04 , Y10T442/2861 , C04B38/0054 , C04B38/0605
摘要： Disclosed are porous, low density nanoclay composites that exhibit highly homogeneous microcellular morphology and methods for forming the nanocomposites. The nanocomposites include a three-dimensional matrix having a non-lamellar, generally isotropic cellular structure with little or no macroscopic pores. The nanocomposites also include a gel that may be a noncovalently cross-linked, thermoreversible gel. The nanocomposites may include a binder and/or fibrous reinforcement materials. The nanocomposites may be formed according to a freeze-drying process in which ice crystal growth is controlled to prevent formation of macroscopic pores in the composite materials.
摘要翻译：公开了多孔，低密度纳米粘土复合材料，其表现出高度均匀的微孔形态和形成纳米复合材料的方法。纳米复合材料包括具有非层状，通常各向同性的细胞结构，具有很少或不具有宏观孔的三维基质。纳米复合材料还包括可以是非共价交联的热可逆凝胶的凝胶。纳米复合材料可以包括粘合剂和/或纤维增强材料。可以根据冷冻干燥方法形成纳米复合材料，其中控制冰晶生长以防止在复合材料中形成宏观孔。

2. 发明申请

US20120077015A1 Multi-Layer Nano-Composites 审中-公开
标题翻译：多层纳米复合材料
公开(公告)号：US20120077015A1
公开(公告)日：2012-03-29
申请号：US12893030
申请日：2010-09-29
申请人： Hao Zhou , Walter A. Scrivens
发明人： Hao Zhou , Walter A. Scrivens
IPC分类号： B32B5/26 , B32B27/04 , B29C47/06 , B32B27/02
CPC分类号： B32B5/26 , B29C48/05 , B29C48/08 , B29C48/21 , Y10T428/249949 , Y10T428/249952
摘要： A nano-composite article containing a nanofiber layer and a supporting layer. The nanofiber layer has a first outer boundary adjacent the supporting layer, a second outer boundary on the side of the nanofiber layer opposite the supporting layer and an inner boundary located at the mid-point between the first outer boundary and the second outer boundary and parallel to the first outer boundary. The nanofiber layer contains a matrix and a plurality of nanofibers, where at least 70% of the nanofibers are bonded to other nanofibers. The supporting layer contains a thermoplastic polymer. The concentration of nanofibers is substantially uniform in the nanofiber layer from the inner boundary to the first boundary layer.
摘要翻译：一种含纳米纤维层和支撑层的纳米复合制品。纳米纤维层具有与支撑层相邻的第一外边界，在与支撑层相对的纳米纤维层侧的第二外边界和位于第一外边界和第二外边界之间的中点处的内边界，并且平行到第一个外边界。纳米纤维层包含基质和多个纳米纤维，其中至少70％的纳米纤维结合到其他纳米纤维上。支撑层含有热塑性聚合物。纳米纤维层从内边界到第一边界层的纳米纤维的浓度基本一致。

3. 发明申请

US20120076972A1 Nanofiber Non-Woven Composite 审中-公开
标题翻译：纳米纤维无纺布复合材料
公开(公告)号：US20120076972A1
公开(公告)日：2012-03-29
申请号：US12893035
申请日：2010-09-29
申请人： Hao Zhou , Walter A. Scrivens
发明人： Hao Zhou , Walter A. Scrivens
IPC分类号： B32B5/26 , B29C47/88 , B32B3/02 , B82Y30/00
CPC分类号： B82Y30/00 , B29C48/04 , B29C48/05 , B29C48/21 , B29C48/919 , B29K2313/00 , B29K2913/00 , B32B5/022 , B32B5/26 , D04H1/559 , D04H1/64 , Y10T428/23914
摘要： A nanofiber non-woven composite containing a nanofiber non-woven layer and a textile layer. The nanofiber non-woven layer has a first side and a second side and a plurality of nanofibers. At least 70% of the nanofibers are bonded to other nanofibers. The textile layer has a textile layer thickness and is located on the first side of the nanofiber non-woven layer. At least a portion of the nanofibers of the nanofiber non-woven layer are penetrated at least partially into the textile layer thickness.
摘要翻译：一种含有纳米纤维无纺布层和织物层的纳米纤维无纺布复合材料。纳米纤维无纺布层具有第一面和第二面以及多个纳米纤维。至少70％的纳米纤维结合到其他纳米纤维上。纺织层具有织物层厚度，并且位于纳米纤维无纺布层的第一面上。纳米纤维无纺层的纳米纤维的至少一部分至少部分地渗入织物层的厚度。

4. 发明申请

US20120074612A1 Process of Forming a Nanofiber Non-Woven Containing Particles 有权
标题翻译：形成纳米纤维无纺布颗粒的工艺
公开(公告)号：US20120074612A1
公开(公告)日：2012-03-29
申请号：US12893041
申请日：2010-09-29
申请人： Walter A. Scrivens , Hao Zhou
发明人： Walter A. Scrivens , Hao Zhou
IPC分类号： B29C51/04
CPC分类号： D04H1/413 , B29C47/0004 , B29C47/0014 , D01D5/082 , D04H1/541 , D04H1/544 , D04H1/549 , D04H1/55 , D04H3/005
摘要： A process for forming a nanofiber non-woven includes mixing a first and second thermoplastic polymer and a plurality of particles, then subjecting the mixture to elongational forces when the first and second polymers are in a softened condition forming nanofibers of the first polymer. Next, the mixture is brought to a condition where the temperature is below the softening temperature of the first polymer forming a first intermediate. The first intermediate is consolidated forming the second intermediate where at least 70% of the nanofibers are fused to other nanofibers. Next, at least a portion of the second polymer is removed and at least 50% of the particles are positioned adjacent a surface of the nanofibers.
摘要翻译：形成纳米纤维无纺布的方法包括混合第一和第二热塑性聚合物和多个颗粒，然后当第一和第二聚合物处于形成第一聚合物的纳米纤维的软化状态时，对混合物进行拉伸力。接下来，使混合物达到温度低于形成第一中间体的第一聚合物的软化温度的条件。将第一中间体固结形成第二中间体，其中至少70％的纳米纤维与其它纳米纤维融合。接下来，除去至少一部分第二聚合物，并且至少50％的颗粒位于纳米纤维的表面附近。

5. 发明申请

US20120077405A1 Core/Shell Nanofiber Non-Woven 审中-公开
标题翻译：核/壳纳米纤维无纺布
公开(公告)号：US20120077405A1
公开(公告)日：2012-03-29
申请号：US12893046
申请日：2010-09-29
申请人： Hao Zhou , Walter A. Scrivens
发明人： Hao Zhou , Walter A. Scrivens
IPC分类号： B32B5/02 , D01D5/34 , D04H13/00
CPC分类号： D01D5/34 , D01D5/00 , D04H1/4391 , D04H3/016 , D04H3/018 , Y10T442/621 , Y10T442/622 , Y10T442/641
摘要： A core/shell nanofiber non-woven containing a plurality of core/shell nanofibers where at least 70% of the nanofibers are bonded to other nanofibers. The core of the nanofiber contains a core polymer and the shell of the nanofiber contains a shell polymer. At least a portion of the core polymer interpenetrates the shell of the nanofiber and at least a portion of the shell polymer interpenetrates the core of the nanofiber. The process for forming a core/shell nanofiber non-woven is also disclosed.
摘要翻译：含有多个核/壳纳米纤维的核/壳纳米纤维无纺布，其中至少70％的纳米纤维结合到其他纳米纤维上。纳米纤维的核心含有核心聚合物，纳米纤维的外壳含有壳聚合物。核心聚合物的至少一部分互穿纳米纤维的外壳，并且壳聚合物的至少一部分互穿纳米纤维的核心。还公开了形成核/壳纳米纤维无纺布的方法。

6. 发明授权

US08889572B2 Gradient nanofiber non-woven 有权
标题翻译：梯度纳米纤维无纺布
公开(公告)号：US08889572B2
公开(公告)日：2014-11-18
申请号：US12893010
申请日：2010-09-29
申请人： Walter A. Scrivens , Hao Zhou
发明人： Walter A. Scrivens , Hao Zhou
IPC分类号： D04H3/005 , D04H3/016 , D04H3/147 , D01D5/40 , B32B5/02 , D01F6/44 , D01F6/88 , D04H1/4391 , D04H3/018
CPC分类号： D01D5/40 , B32B5/022 , D01F6/44 , D01F6/88 , D04H1/4391 , D04H3/016 , D04H3/018 , Y10T442/614 , Y10T442/619 , Y10T442/622 , Y10T442/641 , Y10T442/69
摘要： A gradient nanofiber non-woven contains a plurality of nanofibers where at least 70% of the nanofibers are bonded to other nanofibers. The nanofibers each have a surface and a center and contain a bulk polymer and a third component. The majority by weight at the surface of the nanofiber is the third component and the majority by weight at the center of the nanofiber is the bulk polymer and there is a concentration gradient from most concentrated to least from the surface of the nanofiber to the center of the nanofiber. The process for forming a gradient nanofiber non-woven is also disclosed.
摘要翻译：梯度纳米纤维无纺布含有多个纳米纤维，其中至少70％的纳米纤维结合到其他纳米纤维上。纳米纤维各自具有表面和中心并且包含本体聚合物和第三组分。在纳米纤维表面的重量百分比是第三组分，并且在纳米纤维中心的重量百分比是本体聚合物，并且存在从最浓缩到最小从纳米纤维表面到中心的浓度梯度纳米纤维还公开了形成梯度纳米纤维无纺布的方法。

7. 发明申请

US20120077406A1 Nanofiber Non-Wovens Containing Particles 审中-公开
标题翻译：纳米非织造布包含颗粒
公开(公告)号：US20120077406A1
公开(公告)日：2012-03-29
申请号：US12893028
申请日：2010-09-29
申请人： Walter A. Scrivens , Hao Zhou
发明人： Walter A. Scrivens , Hao Zhou
IPC分类号： D04H13/00
CPC分类号： D04H3/016 , B32B5/022 , B32B5/26 , B32B2262/02 , B32B2264/02 , B32B2264/10 , B32B2307/724 , B32B2307/7265 , D04H1/413 , D04H1/4382 , D04H3/007 , D04H3/009 , D04H3/011 , Y10T442/626 , Y10T442/698 , Y10T442/699
摘要： A nano-fiber non-woven comprising a plurality of thermoplastic nano-fibers and a plurality of particles. At least 50% of the particles are positioned adjacent a surface of the nanofibers and at least 70% of the nanofibers are fused to other nanofibers within the nano-fiber non-woven. A process for making the nano-fiber non-woven is also disclosed.
摘要翻译：一种包含多个热塑性纳米纤维和多个颗粒的纳米纤维无纺布。至少50％的颗粒位于纳米纤维的表面附近，并且至少70％的纳米纤维与纳米纤维无纺布中的其它纳米纤维融合。还公开了制备纳米纤维无纺布的方法。

8. 发明申请

US20120074611A1 Process of Forming Nano-Composites and Nano-Porous Non-Wovens 审中-公开
标题翻译：形成纳米复合材料和纳米多孔无纺布的工艺
公开(公告)号：US20120074611A1
公开(公告)日：2012-03-29
申请号：US12893021
申请日：2010-09-29
申请人： Hao Zhou , Walter A. Scrivens
发明人： Hao Zhou , Walter A. Scrivens
IPC分类号： B29C51/04
CPC分类号： C08J3/005 , B29C43/003 , B29C55/00 , B29K2105/0088 , B32B5/022 , B32B7/03 , B32B27/08 , B32B27/286 , B32B27/32 , B32B2262/14 , B32B2270/00 , B82Y30/00 , C08J5/005 , C08J5/046 , D01F6/46 , D01F6/56 , D04H13/02
摘要： A process for forming a nano-composite including mixing a first and second thermoplastic polymer in a molten state forming a molten polymer blend. The second polymer is soluble in a first solvent and the first polymer is insoluble in the first solvent. The first polymer forms discontinuous regions in the second polymer. Next, the polymer blend is subjected to extensional flow, shear stress, and heat forming nanofibers where less than about 30% by volume of the nanofibers are bonded to other nanofibers.Next the polymer blend with nanofibers is cooled and the first intermediate is formed into a pre-consolidation formation. The pre-consolidation formation is then consolidated causing nanofiber movement, randomization, and at least 70% by volume of the nanofibers to fuse to other nanofibers. According to one aspect, the second intermediate is then subjected to the first solvent to the dissolving away at least a portion of the second polymer.
摘要翻译：一种形成纳米复合材料的方法，包括在形成熔融聚合物共混物的熔融状态下混合第一和第二热塑性聚合物。第二聚合物可溶于第一溶剂，第一聚合物不溶于第一溶剂。第一聚合物在第二聚合物中形成不连续区域。接下来，聚合物共混物经受拉伸流动，剪切应力和热成型纳米纤维，其中少于约30体积％的纳米纤维结合到其他纳米纤维。接下来，将具有纳米纤维的聚合物共混物冷却，并将第一中间体形成预固化地层。然后固化预固化形成，导致纳米纤维运动，随机化，以及至少70体积％的纳米纤维与其他纳米纤维融合。根据一个方面，然后使第二中间体经受第一溶剂以溶解至少部分第二聚合物。

9. 发明授权

US08795561B2 Process of forming a nanofiber non-woven containing particles 有权
标题翻译：形成纳米纤维无纺布的颗粒的方法
公开(公告)号：US08795561B2
公开(公告)日：2014-08-05
申请号：US12893041
申请日：2010-09-29
申请人： Walter A. Scrivens , Hao Zhou
发明人： Walter A. Scrivens , Hao Zhou
IPC分类号： D01F1/02 , D04H1/413 , D04H3/005 , D01D5/08 , D04H1/541 , D04H1/544 , D04H1/549 , D04H1/55 , B29C47/00
CPC分类号： D04H1/413 , B29C47/0004 , B29C47/0014 , D01D5/082 , D04H1/541 , D04H1/544 , D04H1/549 , D04H1/55 , D04H3/005
摘要： A process for forming a nanofiber non-woven includes mixing a first and second thermoplastic polymer and a plurality of particles, then subjecting the mixture to elongational forces when the first and second polymers are in a softened condition forming nanofibers of the first polymer. Next, the mixture is brought to a condition where the temperature is below the softening temperature of the first polymer forming a first intermediate. The first intermediate is consolidated forming the second intermediate where at least 70% of the nanofibers are fused to other nanofibers. Next, at least a portion of the second polymer is removed and at least 50% of the particles are positioned adjacent a surface of the nanofibers.
摘要翻译：形成纳米纤维无纺布的方法包括混合第一和第二热塑性聚合物和多个颗粒，然后当第一和第二聚合物处于形成第一聚合物的纳米纤维的软化状态时，对混合物进行拉伸力。接下来，使混合物达到温度低于形成第一中间体的第一聚合物的软化温度的条件。将第一中间体固结形成第二中间体，其中至少70％的纳米纤维与其它纳米纤维融合。接下来，除去至少一部分第二聚合物，并且至少50％的颗粒位于纳米纤维的表面附近。

10. 发明申请

US20120077404A1 Gradient Nanofiber Non-Woven 有权
标题翻译：梯度纳米纤维无纺布
公开(公告)号：US20120077404A1
公开(公告)日：2012-03-29
申请号：US12893010
申请日：2010-09-29
申请人： Walter A. Scrivens , Hao Zhou
发明人： Walter A. Scrivens , Hao Zhou
IPC分类号： D04H13/00 , D01D5/06 , B32B5/02
CPC分类号： D01D5/40 , B32B5/022 , D01F6/44 , D01F6/88 , D04H1/4391 , D04H3/016 , D04H3/018 , Y10T442/614 , Y10T442/619 , Y10T442/622 , Y10T442/641 , Y10T442/69
摘要： A gradient nanofiber non-woven contains a plurality of nanofibers where at least 70% of the nanofibers are bonded to other nanofibers. The nanofibers each have a surface and a center and contain a bulk polymer and a third component. The majority by weight at the surface of the nanofiber is the third component and the majority by weight at the center of the nanofiber is the bulk polymer and there is a concentration gradient from most concentrated to least from the surface of the nanofiber to the center of the nanofiber. The process for forming a gradient nanofiber non-woven is also disclosed.
摘要翻译：梯度纳米纤维无纺布含有多个纳米纤维，其中至少70％的纳米纤维结合到其他纳米纤维上。纳米纤维各自具有表面和中心并且包含本体聚合物和第三组分。在纳米纤维表面的重量百分比是第三组分，并且在纳米纤维中心的重量百分比是本体聚合物，并且存在从最浓缩到最小从纳米纤维表面到中心的浓度梯度纳米纤维还公开了形成梯度纳米纤维无纺布的方法。

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