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1. 发明授权

US5814282A High surface intermeshing profile reactor 失效
标题翻译：高表面啮合轮廓反应器
公开(公告)号：US5814282A
公开(公告)日：1998-09-29
申请号：US784167
申请日：1997-01-15
申请人： Hans Lohe , Hartmut Hey , Gordon Shaw , W. Jeffrey Stikeleather
发明人： Hans Lohe , Hartmut Hey , Gordon Shaw , W. Jeffrey Stikeleather
IPC分类号： B01J19/18 , C08F5/02 , B32B19/02 , C08G63/02
CPC分类号： B01J19/1887 , B01J2219/182
摘要： A polycondensation reactor for polyesters, polyamides or polyarylates, for example, in which a low viscosity material is introduced into the reactor and a relative high viscosity polymer exits the reactor. The reactor has at least two longitudinally intersecting cylindrical interior chambers, each with a rotating shaft through its length. Each shaft has a plurality of stirrers and spacers designed to wipe all interior surfaces of the reactor. The stirrers can be shaped as a cycloid or involute profile, for example. Generally the stirrers on each shaft are indexed from one another preferably by 90.degree. and intermesh with stirrers on the adjacent shaft. Stirring the low viscosity material by rotating the stirrers (on the shafts) spreads the material into a plurality of thin films. At the temperature and vacuum conditions of the reactor, a volatile component is removed, thus causing the material to polymerize, by condensation, forming a relatively high viscosity polymer.
摘要翻译：用于聚酯，聚酰胺或多芳基化合物的缩聚反应器，例如其中将低粘度材料引入反应器和相对较高粘度的聚合物离开反应器。反应器具有至少两个纵向相交的圆柱形内部室，每个室具有通过其长度的旋转轴。每个轴具有多个搅拌器和间隔物，其被设计成擦拭反应器的所有内表面。例如，搅拌器可以成形为摆线或渐开线轮廓。通常，每个轴上的搅拌器彼此优选地相差90°，并且在相邻的轴上与搅拌器相互啮合。通过旋转搅拌器（在轴上）搅拌低粘度材料将材料铺展成多个薄膜。在反应器的温度和真空条件下，除去挥发性组分，从而使材料通过冷凝聚合形成相对高粘度的聚合物。

2. 发明授权

US5599507A Reactor apparatus for preparing a polymeric material 失效
标题翻译：用于制备聚合物材料的反应器装置
公开(公告)号：US5599507A
公开(公告)日：1997-02-04
申请号：US336446
申请日：1994-11-09
申请人： Gordon Shaw , Rainer A. Schaller , W. Jeffrey Stikeleather , Michael D. Melton , Harmut Hey , Roland Schmidt , Rolf Hartmann , Hans Lohe
发明人： Gordon Shaw , Rainer A. Schaller , W. Jeffrey Stikeleather , Michael D. Melton , Harmut Hey , Roland Schmidt , Rolf Hartmann , Hans Lohe
IPC分类号： B01F7/00 , B01F7/10 , B01F15/00 , B01J19/00 , B01J19/18 , C08G63/78 , C08G85/00
CPC分类号： B01F7/00216 , B01F7/10 , B01J19/0006 , B01J19/18 , C08G63/785 , B01J2219/00058 , B01J2219/182
摘要： A polycondensation reactor for processing low viscosity polyester or another polymer into relatively highly viscosity polymer comprises a substantially cylindrical horizontal reactor vessel with a polymer inlet and a polymer outlet adjacent its opposite ends and a vapor exhaust opening in the upper side of the vessel at its outlet end. A polymer agitator is rotated axially within the chamber and includes plural alternating annular overflow and underflow baffles and multiple perforated film-forming screens disposed therebetween in parallel spaced relation to one another. The overflow baffles are in peripheral polymer-sealing relation to the vessel while the underflow baffles have multiple underflow recesses in their outer peripheries, whereby the baffles define a tortuous polymer flow path alternately through their respective polymer overflow and underflow openings to control residence time, distribution and viscosity growth as the polymer flows between the baffles. The baffles and screens are integrally fixed coaxially at their outer peripheries by axially extending wiper bars. Aligned openings in the baffles and screens along the rotational axis of the agitator provide for free flow of volatiles to the exhaust opening.
摘要翻译：用于将低粘度聚酯或另一种聚合物加工成相对高粘度的聚合物的缩聚反应器包括基本上圆柱形的水平反应器容器，其具有邻近其相对端的聚合物入口和聚合物出口以及在其出口处的容器的上侧中的蒸汽排气口结束。聚合物搅拌器在室内轴向旋转并且包括多个交替的环形溢流和下溢挡板以及以彼此间隔开的平行间隔设置的多个穿孔膜形成屏。溢流挡板与容器处于外围聚合物密封关系，而底流挡板在其外周具有多个下溢凹槽，由此挡板通过其各自的聚合物溢流和下溢开口交替地限定弯曲的聚合物流动路径，以控制停留时间，分布并且当聚合物在挡板之间流动时的粘度增长。挡板和筛网通过轴向延伸的刮水条在其外周部同轴地固定。沿着搅拌器的旋转轴线的挡板和筛网中的对准开口提供挥发物自由流动到排气口。

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