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    • 2. 发明授权
    • High surface intermeshing profile reactor
    • 高表面啮合轮廓反应器
    • US5814282A
    • 1998-09-29
    • US784167
    • 1997-01-15
    • Hans LoheHartmut HeyGordon ShawW. Jeffrey Stikeleather
    • Hans LoheHartmut HeyGordon ShawW. Jeffrey Stikeleather
    • B01J19/18C08F5/02B32B19/02C08G63/02
    • B01J19/1887B01J2219/182
    • A polycondensation reactor for polyesters, polyamides or polyarylates, for example, in which a low viscosity material is introduced into the reactor and a relative high viscosity polymer exits the reactor. The reactor has at least two longitudinally intersecting cylindrical interior chambers, each with a rotating shaft through its length. Each shaft has a plurality of stirrers and spacers designed to wipe all interior surfaces of the reactor. The stirrers can be shaped as a cycloid or involute profile, for example. Generally the stirrers on each shaft are indexed from one another preferably by 90.degree. and intermesh with stirrers on the adjacent shaft. Stirring the low viscosity material by rotating the stirrers (on the shafts) spreads the material into a plurality of thin films. At the temperature and vacuum conditions of the reactor, a volatile component is removed, thus causing the material to polymerize, by condensation, forming a relatively high viscosity polymer.
    • 用于聚酯,聚酰胺或多芳基化合物的缩聚反应器,例如其中将低粘度材料引入反应器和相对较高粘度的聚合物离开反应器。 反应器具有至少两个纵向相交的圆柱形内部室,每个室具有通过其长度的旋转轴。 每个轴具有多个搅拌器和间隔物,其被设计成擦拭反应器的所有内表面。 例如,搅拌器可以成形为摆线或渐开线轮廓。 通常,每个轴上的搅拌器彼此优选地相差90°,并且在相邻的轴上与搅拌器相互啮合。 通过旋转搅拌器(在轴上)搅拌低粘度材料将材料铺展成多个薄膜。 在反应器的温度和真空条件下,除去挥发性组分,从而使材料通过冷凝聚合形成相对高粘度的聚合物。