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1. 发明授权

US06454913B1 Process for deposition of sputtered shape memory alloy films 失效
标题翻译：溅射形状记忆合金膜沉积工艺
公开(公告)号：US06454913B1
公开(公告)日：2002-09-24
申请号：US09904072
申请日：2001-07-12
申请人： Gregory K. Rasmussen , Fenglian Chang , Terry J. Gold , Maryann G. Seibert , Jinping Zhang
发明人： Gregory K. Rasmussen , Fenglian Chang , Terry J. Gold , Maryann G. Seibert , Jinping Zhang
IPC分类号： C23C1434
CPC分类号： C22C27/00 , C22C30/00 , C22F1/006 , C23C14/165 , C23C14/3414
摘要： A process is provided for forming a thin film deposit of a Ni—Ti—Hf ternary shape memory alloy on a substrate by magnetron sputtering deposition having high transformation temperatures and good shape-memory and mechanical properties. The method of forming a thin film deposit of a ternary shape memory alloy on a substrate by sputtering deposition comprises arranging a Ni—Ti—Hf target and a substrate within a deposition chamber, maintaining a working distance from the target to the substrate of about 83 mm to 95 mm; heating the substrate to a temperature high enough to induce in-situ crystallization; introducing a krypton working gas into the deposition chamber; applying appropriate level of deposition power so that the deposition rate is from about 6 Å per second to about 120 Å per second; and, depositing a Ni—Ti—Hf shape memory alloy film having a composition ranging from about Ni48(TiHf)52 to Ni50(TiHf)50.
摘要翻译：提供了一种通过具有高转变温度和良好形状记忆和机械性能的磁控溅射沉积在基底上形成Ni-Ti-Hf三元形状记忆合金薄膜沉积的方法。通过溅射沉积在衬底上形成三元形状记忆合金的薄膜沉积的方法包括在沉积室内布置Ni-Ti-Hf靶和衬底，保持从靶到衬底的工作距离约为83 毫米至95毫米; 将基底加热到足够高的温度以引起原位结晶; 将氪工作气体引入沉积室; 施加适当水平的沉积功率，使得沉积速率为每秒约6埃至约120埃; 并且沉积具有约Ni48（TiHf）52至Ni50（TiHf）50的组成的Ni-Ti-Hf形状记忆合金膜。

2. 发明授权

US06592724B1 Method for producing NiTiHf alloy films by sputtering 失效
标题翻译：通过溅射生产NiTiHf合金膜的方法
公开(公告)号：US06592724B1
公开(公告)日：2003-07-15
申请号：US09400589
申请日：1999-09-22
申请人： Gregory Keller Rasmussen , Fenglian Chang , Jinping Zhang , Terry Jack Gold
发明人： Gregory Keller Rasmussen , Fenglian Chang , Jinping Zhang , Terry Jack Gold
IPC分类号： C23C1434
CPC分类号： C23C14/165 , C23C14/34
摘要： Disclosed is a method for producing ternary shape-memory alloy films employing sputtering process techniques using krypton as a process gas.
摘要翻译：公开了一种使用氪作为工艺气体的溅射工艺技术制备三元形状记忆合金膜的方法。

3. 发明授权

US06358380B1 Production of binary shape-memory alloy films by sputtering using a hot pressed target 失效
标题翻译：使用热压靶通过溅射制造二元形状记忆合金膜
公开(公告)号：US06358380B1
公开(公告)日：2002-03-19
申请号：US09401085
申请日：1999-09-22
申请人： Gamdur Singh Mann , Carlos Augusto Valdes , Terry Jack Gold , Jinping Zhang , Fenglian Chang , Gregory Keller Rasmussen
发明人： Gamdur Singh Mann , Carlos Augusto Valdes , Terry Jack Gold , Jinping Zhang , Fenglian Chang , Gregory Keller Rasmussen
IPC分类号： C23C1434
CPC分类号： C23C14/3414 , C23C14/16
摘要： A method for producing thin film deposits of binary shape-memory alloys using an ion sputtering deposition process comprising using a hot pressed metal powder composition target.
摘要翻译：一种使用使用热压金属粉末组合物靶的离子溅射沉积工艺制造二元形状记忆合金的薄膜沉积物的方法。

4. 发明申请

US20090260987A1 METHOD OF MAKING GAS SENSOR ELEMENT, AND GAS SENSOR DERIVED THEREFROM 审中-公开
标题翻译：制造气体传感器元件的方法，以及气体传感器
公开(公告)号：US20090260987A1
公开(公告)日：2009-10-22
申请号：US12105539
申请日：2008-04-18
申请人： Carlos A. Valdes , Jinping Zhang , Raymond L. Bloink , Fenglian Chang , Da Yu Wang , Walter T. Symons , Sheng Yao
发明人： Carlos A. Valdes , Jinping Zhang , Raymond L. Bloink , Fenglian Chang , Da Yu Wang , Walter T. Symons , Sheng Yao
IPC分类号： G01N27/26
CPC分类号： G01N27/4073
摘要： Disclosed herein is a method of making a gas sensor element, comprising calcining a NOx sensor electrode material at a NOx sensor electrode material calcination temperature of about 1200 to about 1600° C. to form a calcined NOx sensor electrode material, disposing the calcined NOx sensor electrode material on a substrate to form a substrate comprising a NOx sensor electrode, and firing the substrate comprising the NOx sensor electrode at a gas sensor element firing temperature to form a gas sensor element comprising a NOx sensor electrode. Also disclosed is a gas sensor comprising the gas sensor element.
摘要翻译：本发明公开了一种制造气体传感器元件的方法，包括在约1200至约1600℃的NOx传感器电极材料煅烧温度下煅烧NOx传感器电极材料，以形成经煅烧的NOx传感器电极材料，将煅烧的NOx传感器电极材料，以形成包括NOx传感器电极的基板，并且在气体传感器元件点火温度下烧制包含NOx传感器电极的基板，以形成包括NOx传感器电极的气体传感器元件。还公开了一种包括气体传感器元件的气体传感器。

5. 发明授权

US06596132B1 Production of ternary shape-memory alloy films by sputtering using a hot pressed target 失效
标题翻译：使用热压靶通过溅射制造三元形状记忆合金膜
公开(公告)号：US06596132B1
公开(公告)日：2003-07-22
申请号：US09400581
申请日：1999-09-22
申请人： Gregory Keller Rasmussen , Fenglian Chang , Jinping Zhang , Terry Jack Gold
发明人： Gregory Keller Rasmussen , Fenglian Chang , Jinping Zhang , Terry Jack Gold
IPC分类号： C23C1432
CPC分类号： C23C14/165 , C23C14/3414
摘要： A method for producing thin film deposits of ternary shape-memory alloys using an ion sputtering deposition process comprising using a hot pressed metal powder composition target.
摘要翻译：一种使用离子溅射沉积工艺制造三元形状记忆合金薄膜沉积物的方法，该方法包括使用热压金属粉末组合物靶。

6. 发明申请

US20070108047A1 Sensing element and method of making the same 审中-公开
标题翻译：感应元件及其制作方法
公开(公告)号：US20070108047A1
公开(公告)日：2007-05-17
申请号：US11281056
申请日：2005-11-16
申请人： Fenglian Chang , Kerry Kruske , Rick Kerr
发明人： Fenglian Chang , Kerry Kruske , Rick Kerr
IPC分类号： G01N27/26
CPC分类号： G01N27/4071 , G01N27/4075
摘要： Disclosed herein is a sensing element comprising: an electrochemical cell; wherein the sensing element comprises a metal selected from the group consisting of Pd and alloys and combinations comprising at least one of the foregoing; and wherein the electrically conductive element is thermally stable at temperatures of greater than or equal to about 1,200° C.
摘要翻译：本文公开了一种感测元件，包括：电化学电池; 其中所述感测元件包括选自Pd和合金的金属和包含前述中的至少一种的组合; 并且其中所述导电元件在大于或等于约1200℃的温度下是热稳定的。

7. 发明授权

US08545684B2 Sensing element and method of making the same 有权
标题翻译：感应元件及其制作方法
公开(公告)号：US08545684B2
公开(公告)日：2013-10-01
申请号：US12899919
申请日：2010-10-07
申请人： Fenglian Chang , Kerry J. Kruske , Rick D. Kerr
发明人： Fenglian Chang , Kerry J. Kruske , Rick D. Kerr
IPC分类号： B05D5/12 , G01N9/00
CPC分类号： G01N27/4071 , G01N27/4075
摘要： Disclosed herein is a method of making a sensing element comprising forming an electrically conductive element, wherein the sensing element comprises a metal selected from the group consisting of Pd and alloys and combinations comprising Pd; and wherein the electrically conductive element is thermally stable at temperatures as high as 1,200° C.
摘要翻译：本文公开了一种制造感测元件的方法，包括形成导电元件，其中感测元件包括选自Pd和合金的金属以及包含Pd的组合; 并且其中导电元件在高达1,200℃的温度下是热稳定的。

8. 发明授权

US07241477B2 Methods of treating electrodes and gas sensors comprising the electrodes 失效
标题翻译：处理包括电极的电极和气体传感器的方法
公开(公告)号：US07241477B2
公开(公告)日：2007-07-10
申请号：US10626128
申请日：2003-07-21
申请人： Fenglian Chang , Rick D. Kerr , Earl Lankheet , David A. Thompson
发明人： Fenglian Chang , Rick D. Kerr , Earl Lankheet , David A. Thompson
IPC分类号： B01D3/00
CPC分类号： G01N27/4074 , G01N27/4071 , G01N27/4075
摘要： A method for forming an electrode comprises: combining a platinum precursor with a gold precursor to form an electrode ink; forming the electrode ink into an electrode precursor; firing the electrode precursor to form the electrode; treating the electrode in an environment having an oxygen partial pressure of less than or equal to 500 ppm oxygen for a period of time sufficient produce an electrode with an exposed surface gold concentration of greater than or equal to about 6 times a bulk gold concentration in the electrode.
摘要翻译：一种形成电极的方法包括：将铂前体与金前体组合以形成电极墨; 将电极油墨形成电极前体; 焙烧电极前体以形成电极; 在氧分压小于或等于500ppm氧的环境中处理电极足够长的时间产生暴露表面金浓度大于或等于约6倍于本体金浓度的电极电极。

9. 发明申请

US20050016841A1 Methods of treating electrodes and gas sensors comprising the electrodes 失效
标题翻译：处理包括电极的电极和气体传感器的方法
公开(公告)号：US20050016841A1
公开(公告)日：2005-01-27
申请号：US10626128
申请日：2003-07-21
申请人： Fenglian Chang , Rick Kerr , Earl Lankheet , David Thompson
发明人： Fenglian Chang , Rick Kerr , Earl Lankheet , David Thompson
IPC分类号： G01N27/407 , B05D5/12
CPC分类号： G01N27/4074 , G01N27/4071 , G01N27/4075
摘要： A method for forming an electrode comprises: combining a platinum precursor with a gold precursor to form an electrode ink; forming the electrode ink into an electrode precursor; firing the electrode precursor to form the electrode; treating the electrode in an environment having an oxygen partial pressure of less than or equal to 500 ppm oxygen for a period of time sufficient produce an electrode with an exposed surface gold concentration of greater than or equal to about 6 times a bulk gold concentration in the electrode.
摘要翻译：一种形成电极的方法包括：将铂前体与金前体组合以形成电极墨; 将电极油墨形成电极前体; 焙烧电极前体以形成电极; 在氧分压小于或等于500ppm氧的环境中处理电极足够长的时间产生暴露表面金浓度大于或等于约6倍于本体金浓度的电极电极。

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