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1. 发明授权

US4586986A Method of recovering pure aromatic substances 失效
标题翻译：纯芳香物质回收方法
公开(公告)号：US4586986A
公开(公告)日：1986-05-06
申请号：US652161
申请日：1984-09-18
申请人： Gerhard Preusser , Martin Schulze , Gerd Emmrich , Hans-Christoph Schneider
发明人： Gerhard Preusser , Martin Schulze , Gerd Emmrich , Hans-Christoph Schneider
IPC分类号： C07C7/08 , C07C1/00 , C07C7/00 , C07C7/04 , C07C7/10 , C07C15/02 , C07C15/04 , C07C67/00 , C10G7/08 , C10G21/00 , B01D3/40
CPC分类号： C10G21/00 , C07C7/005 , C07C7/04 , C10G7/08
摘要： Disclosed is a method for recovering pure aromatic substances from a mixture of hydrocarbons containing both aromatic and non-aromatic fractions. The input mixture is fed through an extractive stage provided with a preliminary distillation column. In the preliminary stage the aromatics-containing product is treated at a pressure up to 20 bar and a temperature up to 300.degree. C. The pressure is adjusted to a value at which the operational temperature of the preliminary stage is higher than the pressure and temperature in the extractive stage and the heat of the vapors discharged from the preliminary stage is used for heating the extractive stage.
摘要翻译：公开了一种从包含芳族和非芳香级分的烃的混合物中回收纯芳族物质的方法。输入混合物通过提供有预蒸馏塔的萃取阶段进料。在初级阶段，含芳族化合物的产物在最高达20巴的压力和高达300℃的温度下进行处理。将压力调节到初级阶段的工作温度高于压力和温度的值在萃取阶段，从初级排出的蒸汽的热量用于加热萃取阶段。

2. 发明授权

US4925535A Process for the production of an aromate concentrate suitable for use as blending component for gasification fuel 失效
标题翻译：用于生产适合用作气化燃料的混合组分的芳香浓缩物的方法
公开(公告)号：US4925535A
公开(公告)日：1990-05-15
申请号：US230187
申请日：1988-08-08
申请人： Gerhard Preusser , Gerd Emmrich , Martin Schulze
发明人： Gerhard Preusser , Gerd Emmrich , Martin Schulze
IPC分类号： B01D3/40 , C07C1/00 , C07C7/08 , C07C15/00 , C07C67/00 , C10G7/08 , C10G53/04 , C10L1/06
CPC分类号： C10G7/08 , C10L1/06
摘要： The process for production of an aromate concentrate for use as a blending component for gasification fuel includes subjecting another feed hydrocarbon mixture to an extractive distillation using N-substituted morpholines as selective solvent in a extractive distillation column. Low-boiling non-aromates with a boiling range up to about 105.degree. C. practically completely and higher-boiling non-aromates with a boiling range between about 105.degree. and 160.degree. C. to a substantial extent are discharged as a raffinate from the top of the extractive distillation column. The extract bottoms from the extractive distillation are fed to a solvent stripping column where the solvent is at least partially recovered from other hydrocarbons. To eliminate condensation and polymerization products due to components with a boiling point over 170.degree. C. from the feed hydrocarbon mixture which can impair the process, a feed hydrocarbon mixture which contains those high boiling components is predistilled prior to extractive distillation to remove them. The top product from the predistillation column is fed to the extractive distillation column for extractive distillation. The predistillation residue can then be added to other hydrocarbons to form the aromate concentrate.
摘要翻译：生产用作气化燃料的共混组分的芳香族浓缩物的方法包括在萃取蒸馏塔中使用N-取代的吗啉作为选择性溶剂对另一种进料烃混合物进行萃取蒸馏。沸点范围高达约105℃的低沸点非芳族化合物，实际上完全沸点高的沸点非常高的沸点在大约105℃至160℃之间的非芳族化合物，作为萃余液从萃取蒸馏塔顶部。来自萃取蒸馏的提取物底部物质进料到溶剂汽提塔，其中溶剂至少部分地从其它烃回收。为了消除来自可能损害该方法的原料烃混合物的沸点超过170℃的组分的冷凝和聚合产物，在萃取蒸馏之前将含有这些高沸点组分的进料烃混合物预先除去，以除去它们。将来自预蒸馏塔的顶部产物进料到萃取蒸馏塔进行萃取蒸馏。然后将预蒸馏残余物加入到其它烃中以形成芳族化合物浓缩物。

3. 发明授权

US4664783A Method for the separation of aromates from hydrocarbon mixtures containing aromatics 失效
标题翻译：芳烃与含芳族烃混合物分离的方法
公开(公告)号：US4664783A
公开(公告)日：1987-05-12
申请号：US708331
申请日：1985-03-05
申请人： Gerhard Preusser , Martin Schulze
发明人： Gerhard Preusser , Martin Schulze
IPC分类号： C07C1/00 , C07C7/08 , C07C15/02 , C07C67/00 , C10G7/08 , C10G21/20 , C10G21/28
CPC分类号： C10G21/28 , C07C7/08 , C10G21/20 , C10G7/08
摘要： A method is disclosed for the separation of aromates from hydrocarbon mixtures employed as entry products, by means of extractive distillation, employing as selective solvent N-substituted morpholine, the substitutions of which display no more than 7 C atoms. The raffinate produced as top product of the extractive distillation is subjected to a distillation, whereby the produced sump product with a solvent content between 20-75% by weight and a temperature between 20.degree.-70.degree. C., is led into a separation container and there separated into a heavy and a light phase. The heavy phase is then recycled into the extractive distillation column, whereas the light phase is recycled into the raffinate distillation column.
摘要翻译：公开了一种用于通过萃取蒸馏将作为进料产物的烃混合物中的芳族化合物分离的方法，采用选择性溶剂N-取代的吗啉，其取代不超过7个C原子。将作为萃取蒸馏的顶部产物生产的残液进行蒸馏，由此将溶剂含量在20-75重量％和温度在20-70℃之间的所生产的油槽产物引入分离容器并分离成一个沉重而轻的阶段。然后将重相循环到萃取蒸馏塔中，而轻相循环到萃余塔蒸馏塔中。

4. 发明授权

US4488936A Heat input control of an extractive distillation column 失效
标题翻译：萃取蒸馏塔的热输入控制
公开(公告)号：US4488936A
公开(公告)日：1984-12-18
申请号：US474315
申请日：1983-03-10
申请人： Gerhard Preusser , Klaus Richter , Martin Schulze
发明人： Gerhard Preusser , Klaus Richter , Martin Schulze
IPC分类号： B01D3/40 , B01D3/42 , C07C7/08
CPC分类号： B01D3/425 , Y10S203/09
摘要： A process and apparatus are provided controlling the heat input of an extractive distillation column. The bottom of the column is heated with a major stream of thermal energy which is either slowly varying in time or controlled by the amount of starting material mixture and with a minor stream of thermal energy which is controlled by sensing the thermodynamic state in the upper half of the column during the process. The major stream can provide about 90 percent and the minor stream about 10 percent of the heat fed to the column. The minor stream can be controlled by the temperature at one point in the upper half of the column, by the temperature difference at two points in the upper half of the column or by gas chromatographic analysis of the extract material concentration near the top of the column. The process allows one to keep a low concentration of the extract material in the raffinate.
摘要翻译：提供了控制萃取蒸馏塔的热输入的方法和装置。柱的底部用主要的热能流加热，该热能流在时间上缓慢变化或受起始材料混合物的量控制，并且具有通过感测上半部分的热力学状态控制的少量热能在该过程中。主流可以提供约90％的次流，约为进料塔热量的10％。小流量可以通过塔上半部分的温度，塔的上半部分两点的温度差或通过柱顶部提取物质浓度的气相色谱分析来控制。该方法允许将提取物材料的低浓度保持在萃余液中。

5. 发明授权

US4410400A Extractive distilling with reworking of residue 失效
标题翻译：萃取蒸馏残留物的再加工
公开(公告)号：US4410400A
公开(公告)日：1983-10-18
申请号：US289718
申请日：1981-08-03
申请人： Gerhard Preusser , Martin Schulze
发明人： Gerhard Preusser , Martin Schulze
IPC分类号： B01D3/40 , B01D3/42 , C07C1/00 , C07C7/08 , C07C67/00 , C10G7/08 , C10G7/12
CPC分类号： C07C7/08 , B01D3/4238 , C10G7/08 , C10G7/12 , Y02P20/124 , Y02P20/57 , Y10S203/20
摘要： A method for working up residues of an extractive distilling process for obtaining pure hydrocarbons. The residue from an extractive distilling column is fed to the about middle part of a distilling column. The hydrocarbons are distilled and removed at the head of the distilling column and the solvent is removed at the bottom of the distilling column. A sidestream is removed from the distilling column at a position above the feed plate for the residue from the extractive distilling column via a so-called reflux evaporator plate having an elevated level of liquid. The sidestream is heated by indirect heat exchange with the solvent flowing from the distilling column. The heated-up sidestream is fed back into the distilling column at a level at or above the reflux evaporator plate. The concentration of the solvent at the reflux evaporator plate is controlled by the amount of reflux at the head of the distilling column.The heating of the side stream reduces the heat requirement of the bottom boiler of the distilling column by about 35 percent.
摘要翻译：一种处理萃取蒸馏工艺残渣的方法，用于获得纯烃。来自萃取蒸馏塔的残余物进料到蒸馏塔的大约中间部分。在蒸馏塔的头部蒸馏并除去烃，并在蒸馏塔的底部除去溶剂。通过所谓的具有升高液体水平的回流蒸发器板，在进料塔上方的馏出塔中从脱萃塔中除去来自萃取蒸馏塔的残余物的侧流。通过与从蒸馏塔流出的溶剂进行间接热交换来加热侧流。加热的侧流在回流蒸发器板上或上方的水平反馈回蒸馏塔。回流蒸发器板上溶剂的浓度由蒸馏塔头部的回流量控制。侧流的加热将蒸馏塔的底部锅炉的热量需求降低约35％。

6. 发明授权

US4081355A Process for recovering highly pure aromatics from a mixture of aromatics and non-aromatics 失效
标题翻译：从芳烃和非芳族化合物的混合物中回收高纯度芳烃的方法
公开(公告)号：US4081355A
公开(公告)日：1978-03-28
申请号：US736151
申请日：1976-10-27
申请人： Gerhard Preusser , Martin Schulze , Klaus Richter , Wilhelm Huwels
发明人： Gerhard Preusser , Martin Schulze , Klaus Richter , Wilhelm Huwels
IPC分类号： B01D11/04 , C07C7/00 , C07C7/08 , C07C7/10 , C10G21/00 , C10G21/20 , B01D3/40 , C10G7/00
CPC分类号： C10G21/20 , B01D11/0426 , B01D11/0488 , C07C7/005 , C07C7/08 , C07C7/10 , C10G21/00
摘要： Process for recovering highly pure aromatic substances from mixtures of hydrocarbons which contain in addition to the aromatic substances, large amounts of non-aromatic substances by liquid-liquid extraction in combination with an after arranged extractive distillation whereby the liquid-liquid extraction of the starting hydrocarbon mixture is carried out under such conditions that the resulting extract contains substantially the total amount of the aromatic substances and a portion of the non-aromatic substances, introducing this extract into an after arranged extractive distillation for further separating said extract whereby the sump product (extract phase) formed is drawn off and introduced into an after arranged distillation column where it is separated into an aromatic and a solvent fraction, while the head product of the extractive distillation (raffinate phase) is reintroduced into the bottom of the extractor for liquid-liquid extraction thereof, wherein there is used in both of the extracting stages, as selective solvent, morpholine and/or N-substituted morpholine in admixture with water whereby the water content of the solvent for the liquid-liquid extraction amounts to between 2-15 weight percent and for the extractive distillation amounts to between 0 and 8 weight percent.
摘要翻译：从芳族物质除外含有烃的混合物中回收高纯度芳族物质的方法，通过液 - 液萃取与大量非芳香族物质的混合萃取后再进行萃取蒸馏，由此液 - 液萃取原料烃混合物在所得提取物基本上含有大量芳族物质和一部分非芳香族物质的条件下进行，将该提取物引入后置的萃取蒸馏中，以进一步分离所述提取物，从而将贮槽产物（提取物相）被引出并引入后排列的蒸馏塔中，其中它被分离成芳族和溶剂馏分，而萃取蒸馏（萃余相）的头部产物被重新引入液体提取器的底部其提取，其中在o中使用 f提取阶段，作为选择性溶剂，吗啉和/或N-取代的吗啉与水混合，其中用于液 - 液萃取的溶剂的水含量为2-15重量％，萃取蒸馏之间为 0和8重量％。

7. 发明授权

US4997547A Method for the production of an aromate concentrate suitable for use as blending component for fuel 失效
标题翻译：用于生产适合用作燃料混合组分的芳香浓缩物的方法
公开(公告)号：US4997547A
公开(公告)日：1991-03-05
申请号：US316911
申请日：1989-02-21
申请人： Gerd Emmrich , Bernhard Firnhaber , Martin Schulze
发明人： Gerd Emmrich , Bernhard Firnhaber , Martin Schulze
IPC分类号： B01D3/40 , C10G7/08 , C10L1/16
CPC分类号： B01D3/40 , C10G7/08
摘要： In the method for the production of an aromate concentrate suitable for use as blending component for gasifier fuel, feed hydrocarbon mixtures having boiling ranges substantially between 40.degree. and 170.degree. C., are subjected, without any previous separation into individual fractions, to an extractive distillation employing N-substituted morpholine, substituents of which display no more than seven C-atoms, as selective solvent. Herewith, the lower boiling non-aromates with a boiling range up to about 105.degree. C., practically completely, and most of the higher boiling non-aromates with a boiling range between about 105.degree. and 160.degree. C., are recovered as raffinate, whereas the aromates, which are to be employed in whole or in part as blending component, come down in the extract of the extractive distillation. In order to separate heavy aromates from solvent, a partial stream of the circulating solvent is mixed with water, and the heavy aromates are separated as a light phase from the solvent-water mixture. The solvent-water mixture is then separated into its components, which are re-utilized.
摘要翻译：在生产适合用作气化器燃料的共混组分的芳香族浓缩物的方法中，将沸点范围基本上在40℃和170℃之间的原料烃混合物在没有任何先前分离成单独馏分的条件下进行萃取作为选择性溶剂，使用取代基不超过7个C原子的N-取代吗啉进行蒸馏。因此，沸点高达约105℃，几乎完全沸腾的沸点非常高的沸点非常高的芳族化合物，沸点约为105-160℃的大部分较高沸点的非芳香化合物作为萃余液回收而将全部或部分作为共混组分使用的芳香剂在萃取蒸馏的提取物中降低。为了将重质芳族化合物与溶剂分离，将循环溶剂的一部分流与水混合，重溶剂与溶剂 - 水混合物分离为轻质相。然后将溶剂 - 水混合物分离成其组分，其被再利用。

8. 发明授权

US4191615A Process for operating extraction or extractive distillation _apparatus 失效
标题翻译：操作萃取或萃取蒸馏工艺
公开(公告)号：US4191615A
公开(公告)日：1980-03-04
申请号：US863733
申请日：1977-12-23
申请人： Martin Schulze , Gerhard Preusser
发明人： Martin Schulze , Gerhard Preusser
IPC分类号： B01D3/40 , C07C7/08 , C07C7/10 , C23F11/06 , C23F11/00
CPC分类号： B01D3/40 , C07C7/08 , C07C7/10 , C23F11/06
摘要： In order to prevent corrosion of the apparatus in extraction and extractive distillation processes where N-substituted morpholine is employed as the selective solvent an additive is added to the solvent which additive consists of (a) phosphoric acid, (b) a salt thereof, (c) a vanadium compound, (d) a molybdenum compound or (e) a mixture of two or more of these compounds, the addition being effected in an amount of about 0.005 to 0.02% by weight of the morpholine solvent.
摘要翻译：为了防止在采用N-取代的吗啉作为选择性溶剂的萃取和萃取蒸馏方法中装置的腐蚀，添加剂加入到溶剂中，该添加剂由（a）磷酸，（b）其盐，（ c）钒化合物，（d）钼化合物或（e）这些化合物中的两种或更多种的混合物，所述添加量以所述吗啉溶剂的约0.005至0.02重量％的量进行。

9. 发明授权

US3944483A Distillative recovery of aromatics with water addition in azeotropic proportions 失效
标题翻译：采用共沸比例加水添加芳烃的蒸馏回收率
公开(公告)号：US3944483A
公开(公告)日：1976-03-16
申请号：US426790
申请日：1973-12-20
申请人： Fritz Schwall , Gerhard Preusser , Martin Schulze
发明人： Fritz Schwall , Gerhard Preusser , Martin Schulze
IPC分类号： B01D3/40 , B01D11/04 , C07C1/00 , C07C7/08 , C07C7/10 , C07C11/04 , C07C15/02 , C07C67/00 , C10G21/28
CPC分类号： C07C7/08 , B01D11/0488 , C07C7/10
摘要： A hydrocarbon mixture consisting of an aromatic and a non-aromatic component is subjected to a liquid-liquid extraction and/or an extractive distillation. A solvent is used which selectively dissolves the aromatic component so as to form an extract phase. The extract phase is introduced into a distillation column for separating the solvent and the aromatic component. The column is provided with trays and the extract phase is introduced into the column at about the middle thereof from where the solvent flows downwardly and the aromatic component flows upwardly. Sufficient water is introduced into the sump of the column to insure that the trays above the location at which the extract phase enters the column are filled with water during the separation. This improves the operation of the distillation column. An arrangement for carrying out the above process is also disclosed.
摘要翻译：将由芳族组分和非芳族组分组成的烃混合物进行液 - 液萃取和/或萃取蒸馏。使用选择性溶解芳族组分以形成提取相的溶剂。将萃取相引入用于分离溶剂和芳族组分的蒸馏塔中。该塔具有托盘，并且提取相在其中部从塔中引入塔中，其中溶剂向下流动，芳族成分向上流动。将足够的水引入塔的贮槽中，以确保在分离期间在提取相进入塔的位置上的塔填充有水。这改善了蒸馏塔的操作。还公开了用于执行上述过程的装置。

10. 发明授权

US5857112A System for achieving enhanced performance and data availability in a unified redundant array of disk drives by using user defined partitioning and level of redundancy 失效
标题翻译：通过使用用户定义的分区和冗余级别，在统一的磁盘驱动器冗余阵列中实现增强性能和数据可用性的系统
公开(公告)号：US5857112A
公开(公告)日：1999-01-05
申请号：US943410
申请日：1992-09-09
申请人： Ebrahim Hashemi , Martin Schulze , Jim Morris , Bob Harper , Swami Nathan , Paul Boulay , Dave Scheffey
发明人： Ebrahim Hashemi , Martin Schulze , Jim Morris , Bob Harper , Swami Nathan , Paul Boulay , Dave Scheffey
IPC分类号： G06F11/20 , G06F11/00 , G06F11/16
CPC分类号： G06F11/1096 , G06F11/2053 , G06F2211/103
摘要： The present invention provides a system of hardware and software that combine to efficiently integrate the various requirements for system performance and system reliability in a RAID system. A user of the present invention is able to select from a range of system performance and reliability configurations, independently of each other. From user specifications, the present invention initially constructs a user space which must be mapped onto the physical storage space in the array of disk drives. The present invention preserves the orthogonality of performance and reliability concepts through a series of mappings that relate to these concepts independently as it transforms user space into the physical space of the disk array.
摘要翻译：本发明提供了一种硬件和软件系统，其组合以在RAID系统中有效地整合系统性能和系统可靠性的各种要求。本发明的用户能够彼此独立地从一系列系统性能和可靠性配置中进行选择。根据用户规范，本发明最初构建了必须映射到磁盘驱动器阵列中的物理存储空间上的用户空间。本发明通过与这些概念相关联的一系列映射来保持性能和可靠性概念的正交性，因为它将用户空间转换成磁盘阵列的物理空间。

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