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1. 发明授权

US06689710B2 Method for producing multimetal cyanide compounds 失效
标题翻译：多金属氰化物的制备方法
公开(公告)号：US06689710B2
公开(公告)日：2004-02-10
申请号：US10204367
申请日：2002-08-20
申请人： Georg Heinrich Grosch , Dirk Franke , Manfred Munzinger , Kathrin Harre , Eva Baum , Michael Stösser
发明人： Georg Heinrich Grosch , Dirk Franke , Manfred Munzinger , Kathrin Harre , Eva Baum , Michael Stösser
IPC分类号： B01J2726
CPC分类号： C08G65/2663 , B01J27/26
摘要： A process for preparing multimetal cyanide compounds by reacting a metal salt with a cyanometalate compound comprises the steps a) precipitation of the multimetal cyanide compound by reaction of a metal salt with a cyanometalate compound and b) recrystallization of the multimetal cyanide compound precipitated in step a).
摘要翻译：通过使金属盐与氰基金属化合物反应制备多金属氰化合物的方法包括以下步骤：通过金属盐与氰基金属化合物的反应沉淀多金属氰化合物，和b）在步骤a）中沉淀的多金属氰化物化合物的重结晶。

2. 发明授权

US07015364B2 Process for preparing polyether polyols 失效
标题翻译：制备聚醚多元醇的方法
公开(公告)号：US07015364B2
公开(公告)日：2006-03-21
申请号：US10745136
申请日：2003-12-22
申请人： Georg Heinrich Grosch , Dirk Franke , Manfred Munzinger , Kathrin Harre , Eva Baum , Michael Stösser
发明人： Georg Heinrich Grosch , Dirk Franke , Manfred Munzinger , Kathrin Harre , Eva Baum , Michael Stösser
IPC分类号： C07C41/03
CPC分类号： C08G65/2663 , B01J27/26
摘要： A process for preparing polyether polyols includes a precipitation step, a recrystallization step, and a reaction step. In the precipitation step, a multimetal cyanide compound is precipitated by reaction of a metal salt with a cyanometalate compound. In the recrystallization step, the multimetal cyanide compound precipitated above is recrystallized by adding further metal salt and/or further cyanometalate compound. The recrystallization forms a multimetal cyanide catalyst compound. In the reaction step, an initiator and one or more alkylene oxide are reacted in the presence of the multimetal cyanide catalyst compound.
摘要翻译：制备聚醚多元醇的方法包括沉淀步骤，重结晶步骤和反应步骤。在沉淀步骤中，通过金属盐与氰基金属化合物的反应使多金属氰化物化合物沉淀。在重结晶步骤中，通过添加另外的金属盐和/或其他氰基金属化合物，使上述析出的多金属氰化物化合物重结晶。重结晶形成多金属氰化物催化剂化合物。在反应步骤中，引发剂和一种或多种烯化氧在多金属氰化物催化剂化合物的存在下反应。

3. 发明申请

US20050203274A1 Dmc catalysts, polyether alcohols, and method for the production thereof 审中-公开
标题翻译： Dmc催化剂，聚醚醇及其制备方法
公开(公告)号：US20050203274A1
公开(公告)日：2005-09-15
申请号：US10514714
申请日：2003-06-18
申请人： Edward Bohres , Dirk Franke , Michael Stosser , Raimund Ruppel , Eva Baum , Kathrin Harre
发明人： Edward Bohres , Dirk Franke , Michael Stosser , Raimund Ruppel , Eva Baum , Kathrin Harre
IPC分类号： C08G65/12 , B01J27/26 , B01J37/03 , C08G18/48 , C08G65/26 , C08G65/04
CPC分类号： B01J27/26 , B01J37/03 , C08G18/4866 , C08G65/2663
摘要： The invention relates to a process for preparing polyether alcohols by addition of alkylene oxides onto H-functional starter substances using multimetal cyanide compounds as catalysts, wherein the multimetal cyanide compound is prepared by a process comprising the steps: a) adding a metal salt solution to a cyanometalate solution at a specific stirring power ε in the range from 0.05 to 10 W/l, preferably from 0.4 to 4 W/l, a temperature in the range from 0° C. to 100° C., preferably from 20° C. to 60° C., and an addition time of from 5 to 120 minutes, b) reducing the specific stirring power ε to a value in the range from 0.03 to 0.8 W/l and at the same time adding a surface-active agent, c) heating the solution while stirring at a specific stirring power ε of from 0.03 to 0.8 W/l, to a temperature of not more than 100° C., preferably in the range from 55° C. to 75° C., d) adding further metal salt solution while stirring at a specific stirring power ε of from 0.03 to 0.8 W/l, e) when the conductivity begins to drop, dispersing the solid, for example by stirring while increasing the specific stirring power ε to >0.7 W/l or by installation of a pumped circuit with an appropriate pump or by means of a high-speed stirrer, f) stirring at the specific stirring power ε of step e) until the conductivity or the pH remains constant, g) separating off the multimetal cyanide compound and washing it with water and, if desired, h) drying the catalyst.
摘要翻译：本发明涉及通过使用多金属氰化物作为催化剂将烯化氧加成到H官能起始物质上制备聚醚醇的方法，其中所述多金属氰化合物通过包括以下步骤的方法制备：a）将金属盐溶液加入到在特定搅拌功率ε为0.05至10W / l，优选0.4至4W / l的范围内的氰酸金属盐溶液，温度范围为0℃至100℃，优选为20℃ 至60℃，加入时间为5至120分钟，b）将比重搅拌功率ε3降低至0.03-0.8W / l的范围内，同时加入表面活性剂，c）在0.03-0.8W / l的特定搅拌功率ε的搅拌下将溶液加热至不超过100℃，优选在55℃至75℃的温度， d）在搅拌下以特定搅拌功率ε加入另外的金属盐溶液从0.03至0.8W / l，e）当电导率开始下降时，例如通过搅拌分散固体，同时将特定搅拌功率ε提高至> 0.7W / l或通过用合适的泵安装泵浦回路或通过高速搅拌器，f）在步骤e）的特定搅拌功率ε下搅拌，直到导电率或pH保持恒定，g）分离多金属氰化合物并用水洗涤，如果需要，h ）干燥催化剂。

4. 发明授权

US07511170B2 Process for liquid/solid reaction 失效
标题翻译：液/固反应方法
公开(公告)号：US07511170B2
公开(公告)日：2009-03-31
申请号：US10487214
申请日：2002-08-29
申请人： Ingo Klopp , Thomas Bogenstätter , Dirk Franke , Manfred Munzinger
发明人： Ingo Klopp , Thomas Bogenstätter , Dirk Franke , Manfred Munzinger
IPC分类号： C07C63/06
CPC分类号： C07F9/1417 , B01J8/006 , B01J8/007 , B01J8/008 , B01J8/06 , B01J8/20 , B01J2208/00548 , B01J2208/0069 , B01J2219/00164 , B01J2219/00189 , C07F9/3813
摘要： A process for carrying out a liquid/solid reaction comprises a) preparing a reaction suspension in which a first reactant is present in suspended form and a second reactant is present in dissolved form in a suspension medium, where one of the reaction products is insoluble in the suspension medium, b) passing the reaction suspension through an elongated reaction zone so that the Reynolds number of the stream is less than 20,000 and c) separating off the insoluble reaction product formed. The process has the advantage that the insoluble reaction product is obtained in a readily filterable form.
摘要翻译：进行液/固反应的方法包括：a）制备其中第一反应物以悬浮形式存在的反应悬浮液，第二反应物以溶解形式存在于悬浮介质中，其中一种反应产物不溶于悬浮介质，b）使反应悬浮液通过细长的反应区，使得流的雷诺数小于20,000，和c）分离形成的不溶性反应产物。该方法具有以易于过滤的形式获得不溶性反应产物的优点。

5. 发明授权

US06693191B2 Method for the production of a particle-containing preparation of tetrahydro-3,5-dimethyl-1,3,5-thiadiazin-2-thione 有权
标题翻译：制备四氢-3,5-二甲基-1,3,5-噻二嗪-2-硫酮的含颗粒制剂的方法
公开(公告)号：US06693191B2
公开(公告)日：2004-02-17
申请号：US10343973
申请日：2003-02-06
申请人： Heinz Isak , Norbert Sendhoff , Franz Schütz , Jörg Therre , Michael Drögemüller , Dirk Franke , Manfred Munzinger , Alexander Weck , Kirsten Burkart
发明人： Heinz Isak , Norbert Sendhoff , Franz Schütz , Jörg Therre , Michael Drögemüller , Dirk Franke , Manfred Munzinger , Alexander Weck , Kirsten Burkart
IPC分类号： C07D28534
CPC分类号： C07D285/34
摘要： Described is a process for the preparation of a particulate tetrahydro-3,5-dimethyl-1,3,5-thiadiazine-2-thione product by combining a first aqueous solution comprising methylammonium N-methyldithiocarbamate with a second aqueous solution comprising formaldehyde, followed by separation and drying of the resulting solid, which comprises combining the first and the second aqueous solutions in such a way that the ratio between the concentrations of dithiocarbamate functions and of formaldehyde is essentially constant in the reaction mixture over time during the duration of the reaction.
摘要翻译：描述了通过将包含N-甲基二硫代氨基甲酸铵的第一水溶液与包含甲醛的第二水溶液组合来制备四氢-3,5-二甲基-1,3,5-噻二嗪-2-硫酮颗粒的产物的方法，随后通过分离和干燥所得固体，其包括将第一和第二水溶液组合，使得二甲氨基甲酸酯官能团和甲醛的浓度之间的比例在反应期间随着时间的推移在反应混合物中基本上恒定。

6. 发明授权

US6066761A Method for isolating 3-[2-chloro-4-(trifluoromethyl)-phenoxy]-benzoic acid 失效
标题翻译：分离3- [2-氯-4-（三氟甲基） - 苯氧基] - 苯甲酸的方法
公开(公告)号：US6066761A
公开(公告)日：2000-05-23
申请号：US355277
申请日：1999-07-28
申请人： Hans Rupert Merkle , Ronald R. Eva , Dirk Franke , Simon A. Jones , Wolfgang Mattmann , Manfred Munzinger
发明人： Hans Rupert Merkle , Ronald R. Eva , Dirk Franke , Simon A. Jones , Wolfgang Mattmann , Manfred Munzinger
IPC分类号： C07C51/48 , C07C51/02 , C07C65/03 , C07C65/21 , C07C65/24
CPC分类号： C07C65/24 , C07C51/02
摘要： A process for the isolation of 3-[2-chloro-4-(trifluoromethyl)phenoxy]benzoic acid of the formula I ##STR1## from an aqueous solution of its metal salt comprises a) reacting the metal salt of 3-[2-chloro-4-(trifluoromethyl)phenoxy]benzoic acid with an organic or inorganic acid;b) heating the reaction mixture until a liquid two-phase system of organic and aqueous phase has formed; andc) separating the organic phase from the aqueous phase.
摘要翻译： PCT No.PCT / EP98 / 00705 Sec。 371日期1999年7月28日第 102（e）日期1999年7月28日PCT提交1998年2月9日PCT公布。第WO98 / 37054号公报日期1998年8月27日从其金属盐水溶液中分离式I的3- [2-氯-4-（三氟甲基）苯氧基]苯甲酸的方法包括：a）使3- [ 2-氯-4-（三氟甲基）苯氧基]苯甲酸与有机或无机酸反应; b）加热反应混合物直到形成有机相和水相的液体两相体系; 和c）从水相中分离有机相。

7. 发明授权

US07717460B2 Airbag 有权
标题翻译：安全气囊
公开(公告)号：US07717460B2
公开(公告)日：2010-05-18
申请号：US11667240
申请日：2005-11-30
申请人： Dirk Franke , Lutz Eichner , Günter Zähle , Andreas Terlunen
发明人： Dirk Franke , Lutz Eichner , Günter Zähle , Andreas Terlunen
IPC分类号： B60R21/16
CPC分类号： B60R21/2342 , B60R21/237 , B60R2021/23169 , B60R2021/23316
摘要： The disclosed airbag for a motor vehicle for supporting the knees of a vehicle occupant in the event of a crash, comprises an inflatable portion, a first fastening region for fastening the airbag to a motor vehicle part, at least one second, detachable fastening region for fastening the airbag to the same or different motor vehicle part, and a connection located between the second, detachable fastening region and the inflatable portion. The second, detachable fastening region is configured to detach from the inflatable portion if a force exceeding a predetermined value acts on the connection between the second, detachable fastening region and the inflatable portion.
摘要翻译：所公开的用于在碰撞的情况下用于支撑车辆乘员的膝盖的机动车辆的气囊包括可充气部分，用于将气囊紧固到机动车辆部分的第一紧固区域，至少一个第二可拆卸紧固区域将气囊紧固到相同或不同的机动车辆部件上，以及位于第二可拆卸紧固区域和可充气部分之间的连接。如果超过预定值的力作用在第二可拆卸紧固区域和可充气部分之间的连接处，第二可拆卸紧固区域构造成从可膨胀部分脱离。

8. 发明授权

US06965047B2 Method for producing ethers, esters or acid anhydrides 失效
标题翻译：生产醚，酯或酸酐的方法
公开(公告)号：US06965047B2
公开(公告)日：2005-11-15
申请号：US10511161
申请日：2003-04-14
申请人： Ingo Klopp , Thomas Bogenstätter , Dirk Franke
发明人： Ingo Klopp , Thomas Bogenstätter , Dirk Franke
IPC分类号： C07F9/06 , C07C51/02 , C07C51/41 , C07F9/141 , C07C69/76
CPC分类号： C07F9/1417 , C07C51/02 , C07C51/412 , C07C63/06 , C07C63/08
摘要： Ethers, esters or acid anhydrides are advantageously obtained when a cake of a first reactant selected from salts of organic or oxygen-containing inorganic acids or alkoxides disposed on a filter element is flowed through by a solution of a second reactant selected from inorganic or organic acid halides and alkyl halides, so that the insoluble halide salt formed remains on the filter element. The halide salt can thus be removed substantially quantitatively in a simple manner.
摘要翻译：当选自设置在过滤元件上的有机或含氧无机酸或醇盐的第一反应物的滤饼通过选自无机或有机酸的第二反应物的溶液流过时，有利地获得醚，酯或酸酐卤化物和烷基卤，使得形成的不溶性卤化物盐保留在过滤元件上。卤化物盐因此可以以简单的方式基本上定量地去除。

9. 发明授权

US08337377B2 Method and device for folding an airbag for an airbag module 有权
标题翻译：用于折叠安全气囊模块的气囊的方法和装置
公开(公告)号：US08337377B2
公开(公告)日：2012-12-25
申请号：US13022932
申请日：2011-02-08
申请人： Andre Buchholz , Dirk Franke
发明人： Andre Buchholz , Dirk Franke
IPC分类号： B31F1/00
CPC分类号： B60R21/237 , B60R2021/2375
摘要： A method for folding an airbag for an airbag module in which the airbag is disposed on a support is provided. At least one piling element for folding the airbag is provided next to the exterior edge of the airbag disposed on the support. The airbag is folded together using the at least one piling element in that the piling element is moved along the support in the direction toward the interior of the airbag disposed on the support. A retainer protrudes from the at least one piling element and moving together with the piling element during the movement thereof and reaching over or under an edge area of the airbag. The at least one retainer acts on an edge area of the airbag in such a way that an undercut is formed in the airbag through the effect of the retainer.
摘要翻译：提供了一种折叠安全气囊的安全气囊的方法，其中气囊设置在支撑件上。至少一个用于折叠气囊的打桩元件设置在安置在支撑件上的气囊的外边缘的旁边。使用至少一个打桩元件将气囊折叠在一起，因为打桩元件沿着朝着安装在支撑件上的气囊内部的方向沿着支撑件移动。保持架从至少一个打桩元件突出并且在其运动期间与打桩元件一起移动并且到达气囊的边缘区域的上方或下方。至少一个保持器作用在气囊的边缘区域上，使得通过保持器的作用在气囊中形成底切。

10. 发明授权

US07329748B2 Method for the production of riboflavin of modification b/c in granular form 失效
标题翻译：用于生产颗粒形式的改性b / c的核黄素的方法
公开(公告)号：US07329748B2
公开(公告)日：2008-02-12
申请号：US10552137
申请日：2004-04-07
申请人： Dirk Franke , Friedrich Hill , Christoph Martin , Thomas Knebel
发明人： Dirk Franke , Friedrich Hill , Christoph Martin , Thomas Knebel
IPC分类号： C07D487/04
CPC分类号： C07D475/14 , A23L33/15
摘要： The present invention relates to an improved process for preparing riboflavin of the B/C modification in granule form. Furthermore, the invention relates to the riboflavin preparation process wherein riboflavin of the A modification is (a) dissolved in aqueous mineral acid without treating the resulting riboflavin solution with activated carbon, (b) precipitated directly afterwards, steps (a) and (b) being carried out at a temperature in the range from 5 to 15° C., and (c) dried by fluidized bed granulation; and wherein the riboflavin does not come into contact with the aqueous mineral acid solvent for longer than on average 4 hours.
摘要翻译：本发明涉及一种制备颗粒形式的B / C改性核黄素的改进方法。此外，本发明涉及核黄素制备方法，其中A修饰的核黄素是（a）溶解在无机酸水溶液中，而不用活性炭处理所得的核黄素溶液，（b）直接沉淀，步骤（a）和（b）在5至15℃的温度下进行，（c）通过流化床造粒干燥; 并且其中所述核黄素不与无机酸水溶液接触长于平均4小时。

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