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1. 发明授权

US06299994B1 Process for providing a pure hydrogen stream for use with fuel cells 失效
标题翻译：提供用于燃料电池的纯氢气流的方法
公开(公告)号：US06299994B1
公开(公告)日：2001-10-09
申请号：US09335620
申请日：1999-06-18
申请人： Gavin P. Towler , Kishore J. Doshi , Kurt M. Vanden Bussche , John J. Senetar
发明人： Gavin P. Towler , Kishore J. Doshi , Kurt M. Vanden Bussche , John J. Senetar
IPC分类号： H01M804
CPC分类号： H01M8/0625 , B01J8/0453 , B01J8/0465 , B01J8/0469 , B01J8/048 , B01J8/0496 , B01J2208/00309 , B01J2208/00504 , B01J2208/00522 , B01J2208/0053 , B01J2219/1946 , C01B3/382 , C01B3/48 , C01B2203/0233 , C01B2203/0244 , C01B2203/0283 , C01B2203/044 , C01B2203/0445 , C01B2203/047 , C01B2203/066 , C01B2203/0811 , C01B2203/0822 , C01B2203/0827 , C01B2203/0844 , C01B2203/1241 , C01B2203/127 , C01B2203/143 , C01B2203/82 , H01M8/04022 , H01M8/0631 , H01M8/0662 , H01M8/0668 , H01M8/0687 , Y02P20/128
摘要： Hydrogen generation and fuel cell operation are integrated through the use of a low-cost hydrogen generation zone which comprises a pre-reforming zone, a partial oxidation zone, a reforming zone, and a water gas shift zone. Anode waste gas from the fuel cell is burned to provide heat to pre-reform the feed to the hydrogen generation zone while the burner exit temperature and the reforming zone exit temperatures are controlled to eliminate thermal cycling in the hydrogenation zone. This simplified control of the hot side temperatures in the hydrogen generation zone below about 700° C. combined with use of the pre-reforming zone, surprisingly permits the use of carbon steel and/or stainless steel for construction of the hydrogenation zone while providing an efficient system which does not require external fuel and offers a high degree of feedstock flexibility at low cost.
摘要翻译：通过使用包括预重整区，部分氧化区，重整区和水煤气换挡区的低成本氢生成区来集成氢气和燃料电池操作。燃料电池的阳极废气被燃烧以提供热量以将进料转化为氢气产生区域，同时控制燃烧器出口温度和重整区出口温度以消除氢化区域中的热循环。在低于约700℃的氢气生成区域中的热侧温度的简化控制以及使用预重整区域令人惊讶地允许使用碳钢和/或不锈钢来构建氢化区，同时提供高效的系统，不需要外部燃料，并以低成本提供高度的原料灵活性。

2. 发明授权

US06280864B1 Control system for providing hydrogen for use with fuel cells 失效
标题翻译：用于提供用于燃料电池的氢的控制系统
公开(公告)号：US06280864B1
公开(公告)日：2001-08-28
申请号：US09336084
申请日：1999-06-18
申请人： Gavin P. Towler , Kishore J. Doshi , Kurt M. Vanden Bussche , John J. Senetar
发明人： Gavin P. Towler , Kishore J. Doshi , Kurt M. Vanden Bussche , John J. Senetar
IPC分类号： H01M804
CPC分类号： H01M8/0625 , B01J8/0453 , B01J2208/00309 , B01J2208/00495 , B01J2208/00504 , B01J2208/00522 , B01J2208/0053 , B01J2219/00006 , C01B3/382 , C01B3/48 , C01B2203/0233 , C01B2203/0244 , C01B2203/0283 , C01B2203/0288 , C01B2203/043 , C01B2203/044 , C01B2203/0445 , C01B2203/047 , C01B2203/066 , C01B2203/0811 , C01B2203/0822 , C01B2203/0827 , C01B2203/0844 , C01B2203/085 , C01B2203/0855 , C01B2203/0866 , C01B2203/0883 , C01B2203/0894 , C01B2203/1011 , C01B2203/1041 , C01B2203/1047 , C01B2203/1052 , C01B2203/1064 , C01B2203/1076 , C01B2203/1082 , C01B2203/1241 , C01B2203/1247 , C01B2203/127 , C01B2203/143 , C01B2203/145 , C01B2203/1604 , C01B2203/1619 , C01B2203/169 , C01B2203/1695 , C01B2203/82 , H01M8/04022 , H01M8/0618 , H01M8/0662 , Y02P20/128
摘要： Hydrogen generation and fuel cell operation are integrated through the use of a low-cost hydrogen generation zone which comprises a pre-reforming zone, a partial oxidation zone, a reforming zone, and a water gas shift zone. Anode waste gas from the fuel cell is burned to provide heat to pre-reform the feed to the hydrogen generation zone while the burner exit temperature and the reforming zone exit temperatures are controlled using a simplified control system to eliminate thermal cycling in the hydrogenation zone. This simplified control of the hot side temperatures in the hydrogen generation zone below about 700° C. combined with use of the pre-reforming zone, surprisingly permits the use of carbon steel and/or stainless steel for construction of the hydrogenation zone while providing an efficient system which does not require external fuel and offers a high degree of feedstock flexibility at low cost.
摘要翻译：通过使用包括预重整区，部分氧化区，重整区和水煤气换挡区的低成本氢生成区来集成氢气和燃料电池操作。燃料电池的阳极废气被燃烧以提供热量以将进料预改性为氢气产生区，同时使用简化的控制系统控制燃烧器出口温度和重整区出口温度以消除氢化区中的热循环。在低于约700℃的氢气生成区域中的热侧温度的简化控制以及使用预重整区域令人惊讶地允许使用碳钢和/或不锈钢来构建氢化区，同时提供高效的系统，不需要外部燃料，并以低成本提供高度的原料灵活性。

3. 发明授权

US06190623B1 Apparatus for providing a pure hydrogen stream for use with fuel cells 失效
标题翻译：用于提供用于燃料电池的纯氢气流的装置
公开(公告)号：US06190623B1
公开(公告)日：2001-02-20
申请号：US09336106
申请日：1999-06-18
申请人： Robert J. Sanger , Gavin P. Towler , Kishore J. Doshi , Kurt M. Vanden Bussche , John J. Senetar
发明人： Robert J. Sanger , Gavin P. Towler , Kishore J. Doshi , Kurt M. Vanden Bussche , John J. Senetar
IPC分类号： B01J804
CPC分类号： H01M8/0631 , B01J8/04 , B01J8/048 , B01J8/0496 , B01J2208/00309 , B01J2208/00504 , B01J2208/00513 , B01J2208/0053 , B01J2219/00006 , C01B3/323 , C01B3/382 , C01B3/48 , C01B3/583 , C01B3/586 , C01B2203/0233 , C01B2203/0244 , C01B2203/0283 , C01B2203/0288 , C01B2203/0405 , C01B2203/043 , C01B2203/044 , C01B2203/0445 , C01B2203/046 , C01B2203/047 , C01B2203/066 , C01B2203/0811 , C01B2203/0822 , C01B2203/0827 , C01B2203/0844 , C01B2203/0855 , C01B2203/0866 , C01B2203/0877 , C01B2203/0883 , C01B2203/0894 , C01B2203/1011 , C01B2203/1041 , C01B2203/1047 , C01B2203/1052 , C01B2203/1064 , C01B2203/107 , C01B2203/1076 , C01B2203/1082 , C01B2203/1217 , C01B2203/1241 , C01B2203/1247 , C01B2203/1258 , C01B2203/127 , C01B2203/1294 , C01B2203/143 , C01B2203/145 , C01B2203/148 , C01B2203/1604 , C01B2203/1619 , C01B2203/169 , C01B2203/82 , H01M8/04022 , H01M8/0612 , H01M8/0618 , H01M8/0625 , H01M8/0662 , H01M8/0668 , Y02P20/128
摘要： An apparatus is provided which comprises two burner zones using a single igniter separated by a heat transfer zone for use in low-cost hydrogen generation units. When used in conjunction with a control system which limits the effluent temperature to less than about 700° C., the apparatus can be constructed of materials such as carbon steel and stainless steel rather than more exotic materials. This simplified structure and the use of less exotic materials provides an efficient, low-cost combined partial oxidation reactor for small-scale hydrogen production systems, especially for hydrogen production systems associated with fuel cell operation for the production of electricity.
摘要翻译：提供了一种装置，其包括使用由用于低成本氢气发生单元的传热区分开的单个点火器的两个燃烧器区域。当与将流出物温度限制在低于约700℃的控制系统结合使用时，该设备可以由诸如碳钢和不锈钢的材料构成，而不是更外来的材料。这种简化的结构和使用不太外来的材料为小规模氢气生产系统提供了一种高效，低成本的组合部分氧化反应器，特别是与用于生产电力的燃料电池操作相关的氢气生产系统。

4. 发明授权

US07192458B1 Process, control system and apparatus for the distribution of air in a fuel cell/fuel processor system 失效
标题翻译：用于在燃料电池/燃料处理器系统中分配空气的过程，控制系统和装置
公开(公告)号：US07192458B1
公开(公告)日：2007-03-20
申请号：US10347926
申请日：2003-01-17
申请人： John R. Harness , Gavin P. Towler , Kurt M. Vanden Bussche , John J. Senetar , Daniel R. Sioui
发明人： John R. Harness , Gavin P. Towler , Kurt M. Vanden Bussche , John J. Senetar , Daniel R. Sioui
IPC分类号： B01J3/24
CPC分类号： H01M8/0618 , C01B3/382 , C01B3/48 , C01B2203/0233 , C01B2203/0244 , C01B2203/0261 , C01B2203/0283 , C01B2203/044 , C01B2203/047 , C01B2203/066 , C01B2203/1211 , C01B2203/1235 , C01B2203/1241 , C01B2203/141 , C01B2203/142 , C01B2203/1604 , C01B2203/1619 , C01B2203/1623 , C01B2203/1685 , C01B2203/169 , H01M8/04022 , H01M8/0662
摘要： A process, control system and apparatus for controlling the air side flows to the major components of a fuel processor apparatus are provided. The control system employs a multi-capacity blower provides process air to a partial oxidation reactor and a preferential oxidation reactor. The multi-capacity blower preferably provides a portion of the process air through a control valve to the partial oxidation reactor and the remaining portion of the process air is passed through a flow restrictor to supply process air to the preferential oxidation reactor. The control system of the present invention is simple, low cost and reliable.
摘要翻译：提供了用于控制空气侧的处理，控制系统和装置流向燃料处理器装置的主要部件。控制系统采用多容量鼓风机向部分氧化反应器和优先氧化反应器提供工艺空气。多容量鼓风机优选通过控制阀将一部分工艺空气提供给部分氧化反应器，并且其余部分的工艺空气通过限流器以将工艺空气供应到优先氧化反应器。本发明的控制系统简单，成本低，可靠。

5. 发明授权

US07288411B2 Process for simultaneously evaluating a plurality of catalysts 有权
标题翻译：同时评估多种催化剂的方法
公开(公告)号：US07288411B2
公开(公告)日：2007-10-30
申请号：US10649438
申请日：2003-08-27
申请人： Duncan E. Akporiaye , Arne Karlsson , Ivar M. Dahl , Rune Wendelbo , Kurt M. Vanden Bussche , Gavin P. Towler , Ralph D. Gillespie
发明人： Duncan E. Akporiaye , Arne Karlsson , Ivar M. Dahl , Rune Wendelbo , Kurt M. Vanden Bussche , Gavin P. Towler , Ralph D. Gillespie
IPC分类号： G01N31/10
CPC分类号： G01N31/10 , B01J19/0046 , B01J2219/00283 , B01J2219/00286 , B01J2219/00299 , B01J2219/00308 , B01J2219/00351 , B01J2219/00423 , B01J2219/00495 , B01J2219/00585 , B01J2219/00698 , B01J2219/00702 , B01J2219/00704 , B01J2219/00745 , B01J2219/00747 , C40B30/08 , C40B40/18 , Y10T436/24
摘要： A process for simultaneously testing a plurality of catalysts using combinatorial chemistry has been developed. The process involves containing the plurality of catalysts in an array of parallel reactors with each reactor containing a bed of catalyst. Each bed of catalyst is then simultaneously contacted, at reaction conditions, with a reactant to form an effluent of each reactor. The reactant or an inert fluid is at a space velocity sufficient to fluidize the catalyst beds. Each of the effluents is analyzed.
摘要翻译：已经开发了使用组合化学同时测试多种催化剂的方法。该方法包括在平行反应器阵列中包含多个催化剂，每个反应器含有催化剂床。然后每个催化剂床在反应条件下与反应物同时接触以形成每个反应器的流出物。反应物或惰性流体处于足以使催化剂床流化的空间速度。分析每个废水。

6. 发明授权

US06548029B1 Apparatus for providing a pure hydrogen stream for use with fuel cells 失效
标题翻译：用于提供用于燃料电池的纯氢气流的装置
公开(公告)号：US06548029B1
公开(公告)日：2003-04-15
申请号：US09442612
申请日：1999-11-18
申请人： Gavin P. Towler , Kurt M. Vanden Bussche
发明人： Gavin P. Towler , Kurt M. Vanden Bussche
IPC分类号： B01J802
CPC分类号： H01M8/0631 , B01J8/0453 , B01J8/0496 , B01J2208/0015 , B01J2208/00176 , B01J2208/00212 , B01J2208/0084 , B01J2208/025 , C01B3/16 , C01B2203/0283 , C01B2203/066 , C01B2203/0894
摘要： An apparatus is provided which comprises a thermosiphon shift reactor for the conversion of carbon monoxide and the generation of steam for use in a fuel processor for the conversion of hydrocarbon fuels into hydrogen and employs the hydrogen in a fuel cell. The thermosiphon shift reactor comprises a vertically extended shell defining an interior volume containing a vertical axis defining a catalyst zone. The vertically extended shell contains a catalyst zone comprising a shift catalyst wherein a high temperature shift catalyst is disposed in successively tapering layers relative to a low temperature shift catalyst and the catalyst zone is at least partially surrounded by an external jacket which defines a flow passage between the vertically extended shell and the external jacket. A fluid reservoir is located above the vertically extended shell at a height effective to establish a thermosiphon effect between the flow passage and the reservoir which generates steam and provides an essentially uniform temperature at the shell wall.
摘要翻译：提供了一种装置，其包括用于转化一氧化碳的热虹吸变换反应器和用于在燃料处理器中用于将烃燃料转化为氢气并在燃料电池中使用氢气的蒸汽的产生。热虹吸变换反应器包括垂直延伸的壳体，其限定包含限定催化剂区域的垂直轴线的内部容积。垂直延伸的壳体包含催化剂区域，其包括换档催化剂，其中相对于低温变换催化剂将高温变换催化剂设置在相继逐渐变细的层中，并且催化剂区域至少部分地被外部护套包围，该外部套管限定了垂直延伸的外壳和外套。流体储存器位于垂直延伸的壳体上方，其高度有效地在流动通道和储存器之间建立热虹吸效应，其产生蒸汽并且在壳壁处提供基本均匀的温度。

7. 发明授权

US06368865B1 Combinatorial process for performing catalytic chemical reactions 有权
标题翻译：进行催化化学反应的组合方法
公开(公告)号：US06368865B1
公开(公告)日：2002-04-09
申请号：US09464306
申请日：1999-12-15
申请人： Ivar M. Dahl , Arne Karlsson , Duncan E. Akporiaye , Rune Wendelbo , Kurt M. Vanden Bussche , Gavin P. Towler
发明人： Ivar M. Dahl , Arne Karlsson , Duncan E. Akporiaye , Rune Wendelbo , Kurt M. Vanden Bussche , Gavin P. Towler
IPC分类号： G01N3110
CPC分类号： G01N31/10 , B01J19/0046 , Y10T436/24
摘要： A combinatorial process for simultaneously conducting multiple catalytic chemical reactions in parallel has been developed. At least one catalyst is contained in the reaction zones of a plurality of reactors, each reactor having a reactor insert placed within a sleeve and inserted into a well, the reaction zone of each reactor being formed between a fluid permeable structure attached to the sleeve and a fluid permeable end of the corresponding reactor insert. A fluid reactant is flowed through each reactor where it is contacted with the catalyst contained in the reaction zone to form an effluent. The effluents are removed from the effluent from the reactor and are analyzed.
摘要翻译：已经开发了同时进行多个催化化学反应并联的组合方法。在多个反应器的反应区域中包含至少一种催化剂，每个反应器具有置于套管内的反应器插入件并插入到井中，每个反应器的反应区域形成在附接到套筒的流体可渗透结构和相应的反应器插入物的流体可渗透的端部。流体反应物流过每个反应器，在那里与包含在反应区中的催化剂接触以形成流出物。将废水从反应器的流出物中除去并进行分析。

8. 发明授权

US06375924B1 Water gas shift process for purifying hydrogen for use with fuel cells 失效
标题翻译：用于净化用于燃料电池的氢气的水煤气变换过程
公开(公告)号：US06375924B1
公开(公告)日：2002-04-23
申请号：US09608118
申请日：2000-06-30
申请人： Gavin P. Towler , Kurt M. Vanden Bussche
发明人： Gavin P. Towler , Kurt M. Vanden Bussche
IPC分类号： C01B316
CPC分类号： C01B3/16 , B01J23/78 , B01J23/80 , B01J23/862 , C01B3/384 , C01B3/48 , C01B2203/0233 , C01B2203/0244 , C01B2203/0288 , C01B2203/066 , C01B2203/0822 , C01B2203/0827 , C01B2203/0877 , C01B2203/1017 , C01B2203/1052 , C01B2203/1058 , C01B2203/1064 , C01B2203/107 , Y02P20/128 , Y02P20/52
摘要： A process and apparatus are disclosed for the operation of a compact water gas shift reactor for use in conjunction with fuel cell to generate electric power from a feedstream comprising a hydrocarbon or an alcohol. The fuel cell comprises a proton exchange membrane which produces electric power from a hydrogen product stream which comprises essentially no carbon monoxide. The hydrogen product stream may be produced from the feedstream in a steam reforming of autothermal reforming zone. The compact water gas shift reactor comprises a vertically aligned vessel having a top end, a bottom end opposite, which defines an interior space. The interior space contains a first water spray zone for contacting a reforming effluent stream comprising hydrogen with a first water stream. A first dispersion zone is disposed below the first water spray zone and above a high temperature shift zone. The high temperature shift zone contains a high temperature shift catalyst to produce a high temperature shift effluent stream. A second water spray zone is disposed below the high temperature shift zone and above a second dispersion zone. A low temperature shift zone is disposed below the second dispersion zone. The low temperature shift zone contains a low temperature shift catalyst to produce a water-saturated hydrogen product stream which comprises less than 50 ppm-mol carbon monoxide. The water dispersion zones simplify the overall shift reaction zone and provide protection for the shift catalysts from temperature shock.
摘要翻译：公开了用于与燃料电池结合使用以从包含烃或醇的进料流产生电力的紧凑型水煤气变换反应器的操作的方法和设备。燃料电池包括质子交换膜，其从基本上不含一氧化碳的氢产物流产生电力。氢气产物流可以在自热重整区域的蒸汽重整中由进料流产生。紧凑型水煤气变换反应堆包括垂直排列的容器，其具有顶端，底端相对，其限定内部空间。内部空间包含用于使包含氢气的重整流出物流与第一水流接触的第一喷水区。第一分散区设置在第一喷水区下方和高温移位区之上。高温位移区包含高温变换催化剂，以产生高温漂移流出物流。第二喷水区设置在高温移位区下方和第二分散区之上。低温移位区设置在第二分散区的下方。低温变换区包含低温变换催化剂，以产生包含小于50ppm摩尔一氧化碳的水饱和氢产物流。水分散区简化了整体转移反应区，为转移催化剂提供了对温度冲击的保护。

9. 发明授权

US06342185B1 Combinatorial catalytic reactor 有权
标题翻译：组合催化反应器
公开(公告)号：US06342185B1
公开(公告)日：2002-01-29
申请号：US09464171
申请日：1999-12-15
申请人： Ivar M. Dahl , Arne Karlsson , Duncan E. Akporiaye , Kurt M. Vanden Bussche , Gavin P. Towler
发明人： Ivar M. Dahl , Arne Karlsson , Duncan E. Akporiaye , Kurt M. Vanden Bussche , Gavin P. Towler
IPC分类号： G01N3110
CPC分类号： G01N31/10 , B01J19/0046 , B01J35/0006 , B01J2219/00283 , B01J2219/00286 , B01J2219/00299 , B01J2219/00308 , B01J2219/00351 , B01J2219/00423 , B01J2219/00495 , B01J2219/00585 , B01J2219/00698 , B01J2219/00702 , B01J2219/00745 , B01J2219/00747 , C40B30/08 , C40B40/18 , C40B60/14
摘要： A reactor for conducting catalytic chemical reactions has been developed. The reactor has a well having an open end and a closed end. The reactor also has a sleeve having a top end and a bottom end. The bottom end of the sleeve is inserted within the open end of the well. A fluid permeable structure is attached to the sleeve spanning the cross-section thereby defining a chamber between the closed end of the well and the fluid permeable structure. The reactor also has a reactor insert having a fluid permeable end and a top end containing a first and a second fluid conduit. The fluid permeable end of the reactor is inserted within the open end of the sleeve. The first fluid conduit is in fluid communication with the chamber, and the second fluid conduit is in fluid communication with the fluid permeable end of the reactor insert.
摘要翻译：已经开发了用于进行催化化学反应的反应器。反应器具有开口端和封闭端的阱。反应器还具有具有顶端和底端的套筒。套筒的底端插入孔的开口端。流体可渗透结构连接到横跨横截面的套筒上，从而在井的封闭端和流体可渗透结构之间限定一个室。反应器还具有反应器插入物，其具有流体可渗透的端部，顶端包含第一和第二流体导管。反应器的流体可渗透的端部插入到套筒的开口端内。第一流体导管与腔室流体连通，第二流体导管与反应器插入物的流体可渗透的端部流体连通。

10. 发明授权

US07422676B2 Apparatus and process for the synthesis of hydrogen peroxide directly from hydrogen and oxygen 失效
标题翻译：用于直接从氢和氧合成过氧化氢的装置和方法
公开(公告)号：US07422676B2
公开(公告)日：2008-09-09
申请号：US11313201
申请日：2005-12-20
申请人： Kurt M. Vanden Bussche , Anil R. Oroskar , Jeffery C. Bricker , Laszlo T. Nemeth , Gavin P. Towler
发明人： Kurt M. Vanden Bussche , Anil R. Oroskar , Jeffery C. Bricker , Laszlo T. Nemeth , Gavin P. Towler
IPC分类号： C25B1/30 , C25B1/04 , C01B15/029
CPC分类号： B01J8/025 , B01F5/0057 , B01F15/0201 , B01J10/007 , B01J19/002 , B01J2219/00013 , B01J2219/00263 , B01J2219/00889 , C01B15/029 , C07D223/10 , C07D301/12 , C07D313/04
摘要： A device is disclosed for the generation of hydrogen peroxide. The device produces hydrogen peroxide on an as-needed basis through the use of electrolysis of water, remixing hydrogen and oxygen in an appropriate ratio, and reacting the hydrogen and oxygen in water in a reactor.
摘要翻译：公开了用于产生过氧化氢的装置。该设备通过使用水的电解，以适当的比例重新混合氢气和氧气，并在反应器中使氢气和氧气在水中反应，根据需要生产过氧化氢。

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