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1. 发明授权

US06288286B1 Method for producing hexanediol-1,6 失效
标题翻译：己二醇-1,6-
公开(公告)号：US06288286B1
公开(公告)日：2001-09-11
申请号：US09700366
申请日：2000-11-15
申请人： Frank Stein , Thomas Krug , Martin Gall , Gabriele Iffland
发明人： Frank Stein , Thomas Krug , Martin Gall , Gabriele Iffland
IPC分类号： C07C2700
CPC分类号： C07C29/149 , C07C2601/14 , C07C31/20 , C07C35/08
摘要： A process for preparing 1,6-hexanediol from a carboxylic acid mixture obtained as by-product in the oxidation of cyclohexane to cyclohexanone/cyclohexanol with oxygen or oxygen-comprising gases and by aqueous extraction of the reaction mixture and comprising adipic acid, 6-hydroxycaproic acid and small amounts of 1,4-cyclohexanediols by esterification of the acids and hydrogenation, by a) reacting the mono- and dicarboxylic acids in the aqueous dicarboxylic acid mixture with a low molecular weight alcohol to form the corresponding carboxylic esters, b) conducting a first distillation to remove excess alcohol and low boilers from the esterification mixture obtained, c) conducting a second distillation to separate the bottom product into an ester fraction which is essentially free from 1,4-cyclohexanediols and a fraction which includes at least the larger proportion of the 1,4-cyclohexanediols, d) subjecting the ester fraction essentially free from 1,4-cyclohexanediols to a catalytic hydrogenation, and e) subjecting the hydrogenation effluent to a distillation to recover 1,6-hexanediol in a conventional manner, comprises using an aqueous dicarboxylic acid mixture comprising more than 20 ppm of cobalt and more than 40 ppm of phosphorus in the form of phosphate and passing this aqueous dicarboxylic acid mixture through a cation exchanger and after the esterification of step (a) through an anion exchanger.
摘要翻译：从环己烷氧化成环己酮/环己醇与氧气或含氧气体的副产物得到的羧酸混合物中制备1,6-己二醇的方法，并通过水提取反应混合物，并包含己二酸，6- 羟基己酸和少量的1,4-环己烷二醇通过酸的酯化和氢化，a）使二羧酸二羧酸混合物与低分子量醇反应形成相应的羧酸酯，b）导电从所得到的酯化混合物中除去多余的醇和低沸点物的第一次蒸馏，c）进行第二次蒸馏以将底部产物分离成基本上不含1,4-环己烷二醇的酯馏分和至少包括较大的 1,4-环己烷二醇的比例，d）将基本上不含1,4-环己烷二醇的酯馏分进行催化水解国家和地区）使氢化流出物以常规方式进行蒸馏以回收1,6-己二醇，包括使用包含大于20ppm钴的多余二羧酸混合物和大于40ppm磷酸盐形式的磷，使该含水二羧酸混合物通过阳离子交换剂，并且在步骤（a）通过阴离子交换剂酯化之后。

2. 发明授权

US08772547B2 Method for producing 1-adamantyl trimethylammonium hydroxide 有权
标题翻译： 1-金刚烷基三甲基氢氧化铵的制备方法
公开(公告)号：US08772547B2
公开(公告)日：2014-07-08
申请号：US13255805
申请日：2010-03-11
申请人： Christof Wilhelm Wigbers , Martin Ernst , Laszlo Szarvas , Giovanni D'Andola , Ellen Dahlhoff , Gabriele Iffland , Peter Raatz , Falk Simon , Matthias Frauenkron
发明人： Christof Wilhelm Wigbers , Martin Ernst , Laszlo Szarvas , Giovanni D'Andola , Ellen Dahlhoff , Gabriele Iffland , Peter Raatz , Falk Simon , Matthias Frauenkron
IPC分类号： C07C211/00
CPC分类号： C07C211/63 , C07C209/00 , C07C209/26 , C07C2603/74
摘要： The present invention relates to a process for preparing 1-adamantyltrimethylammonium hydroxide, by A) reacting 1-adamantyldimethylamine with dimethyl sulfate to give 1-adamantyltrimethylammonium sulfate; and B) subjecting the 1-adamantyltrimethylammonium sulfate obtained in A) to anion exchange with an ion exchanger loaded with OH ions.
摘要翻译：本发明涉及一种制备1-金刚烷基三甲基氢氧化铵的方法，通过A）使1-金刚烷基二甲胺与硫酸二甲酯反应得到1-金刚烷基三甲基硫酸铵; 和B）在A）中获得的1-金刚烷基三甲基硫酸铵与负载有OH离子的离子交换剂进行阴离子交换。

3. 发明授权

US09670415B2 Synthesis of zeolitic materials using N,N-dimethyl organotemplates 有权
公开(公告)号：US09670415B2
公开(公告)日：2017-06-06
申请号：US13605701
申请日：2012-09-06
申请人： Bilge Yilmaz , Ulrich Berens , Vijay Narayanan Swaminathan , Ulrich Müller , Gabriele Iffland , Laszlo Szarvas
发明人： Bilge Yilmaz , Ulrich Berens , Vijay Narayanan Swaminathan , Ulrich Müller , Gabriele Iffland , Laszlo Szarvas
IPC分类号： C01B39/54 , C01B39/48 , B01J29/70 , B01J29/85 , B01J29/86 , B01J29/87 , C10G3/00 , C10G11/05 , C07C1/20 , C10G25/03 , C10G11/18 , B01D53/94
CPC分类号： C10G3/49 , B01D53/9413 , B01D53/9436 , B01D2255/50 , B01J29/70 , B01J29/7015 , B01J29/85 , B01J29/86 , B01J29/87 , B01J2229/183 , C01B39/48 , C01B39/54 , C07C1/20 , C07C2529/70 , C10G11/05 , C10G11/18 , C10G25/03 , C10G2300/405 , Y02C20/10 , C07C11/02
摘要： The present invention relates to a process for the preparation of a zeolitic material having a structure comprising YO2 and optionally comprising X2O3, preferably comprising YO2 and X2O3, wherein said process comprises the steps of (1) providing a mixture comprising one or more ammonium compounds of which the ammonium cation has the formula (I): [R1R2NR3R4]+ (I) and further comprising one or more sources for YO2 and one or more sources for X2O3; (2) crystallizing the mixture provided in (1); wherein Y is a tetravalent element, and X is a trivalent element, and wherein in formula (I) R1 and R2 are independently from one another derivatized or underivatized methyl, and R3 and R4 are independently from one another derivatized or underivatized (C3-C5)alkyl, and wherein the molar ratio of ammonium cation having the formula (I) to Y in the mixture provided in step (1) and crystallized in step (2) is equal to or greater than 0.25.

4. 发明申请

US20110033361A1 METHOD FOR REMOVING HALOGEN FROM LIQUID AMMONIA 有权
标题翻译：从液体氨去除卤素的方法
公开(公告)号：US20110033361A1
公开(公告)日：2011-02-10
申请号：US12936375
申请日：2009-03-26
申请人： Roland Bou Chedid , Gabriele Iffland , Jürgen Ciprian , Johann-Peter Melder , Frank-Friedrich Pape
发明人： Roland Bou Chedid , Gabriele Iffland , Jürgen Ciprian , Johann-Peter Melder , Frank-Friedrich Pape
IPC分类号： C01C1/00 , C01B21/087
CPC分类号： C01C1/024 , B01J41/05
摘要： The present invention relates to a method for depleting halide ions from liquid ammonia, wherein the liquid ammonia is brought into contact with a strongly basic ion exchanger, where the basic structure of the strongly basic ion exchanger is a covalently crosslinked polymer matrix. Furthermore, the present invention relates to the use of an ammonia obtainable according to the invention as starting material in the production of amines.
摘要翻译：本发明涉及从液氨中消耗卤离子的方法，其中液态氨与强碱性离子交换剂接触，其中强碱性离子交换剂的基本结构是共价交联的聚合物基体。此外，本发明涉及根据本发明可获得的氨作为制备胺的原料的用途。

5. 发明授权

US06827858B2 Method for separating alkali metal ions from alkoxylates 有权
标题翻译：从烷氧基化物中分离碱金属离子的方法
公开(公告)号：US06827858B2
公开(公告)日：2004-12-07
申请号：US10275942
申请日：2002-11-14
申请人： Joachim Bader , Hans-Heinrich Bechtolsheimer , Armin Brucker , Toni Dockner , Gabriele Iffland , Hans Klink , Stefan Martin , Jürgen Mohr , Hans-Martin Mugrauer
发明人： Joachim Bader , Hans-Heinrich Bechtolsheimer , Armin Brucker , Toni Dockner , Gabriele Iffland , Hans Klink , Stefan Martin , Jürgen Mohr , Hans-Martin Mugrauer
IPC分类号： C02F142
CPC分类号： C08G65/30 , B01J39/04 , B01J49/06 , B01J49/53
摘要： Alkali metal ions are separated off from alkoxylates containing alkali metal ions by a process comprising: a) dilution of the alkali metal-containing alkoxylate with an inert solvent, b) treatment of the alkali metal-containing solution of the alkoxylate with a cationic exchanger in order to obtain a substantially alkali metal-free solution of the alkoxylate, and c) removal of the solvent from the substantially alkali metal-free solution of the alkoxylate in order to obtain a substantially alkali metal-free and substantially solvent-free alkoxylate.
摘要翻译：碱金属离子与含有碱金属离子的烷氧基离子分离，其方法包括：a）用惰性溶剂稀释含碱金属的烷氧基化物，b）用阳离子交换剂处理含烷氧基化物的碱金属的溶液以获得基本上不含碱金属的烷氧基化物溶液，和c）从基本上不含碱金属的烷氧基化物溶液中除去溶剂，以获得基本上无碱金属和基本上无溶剂的烷氧基化物。

6. 发明授权

US5883288A Continuous preparation of alkyl esters of (meth)acrylic acid 失效
标题翻译：连续制备（甲基）丙烯酸的烷基酯
公开(公告)号：US5883288A
公开(公告)日：1999-03-16
申请号：US791052
申请日：1997-01-28
申请人： Gabriele Iffland , Albrecht Dams , Alexander Weck , Heinrich Aichinger , Holger Herbst , Gerhard Nestler , Herbert Exner , Willi Schmidt , Matthias Geisendorfer , Toni Dockner
发明人： Gabriele Iffland , Albrecht Dams , Alexander Weck , Heinrich Aichinger , Holger Herbst , Gerhard Nestler , Herbert Exner , Willi Schmidt , Matthias Geisendorfer , Toni Dockner
IPC分类号： B01J27/02 , B01J31/02 , C07B61/00 , C07C67/08 , C07C67/54 , C07C69/54 , C07C69/52
CPC分类号： C07C67/08
摘要： In the process for the continuous preparation of alkyl esters of (meth)acrylic acid by reacting (meth)acrylic acid with monohydric alkanols having from 1 to 8 carbon atoms in the presence of an acid esterification catalyst in a reaction zone, there is discharged from the reaction zone a product mixture which comprises the alkyl (meth)acrylate formed, the catalyst and the by-products formed during the course of the esterification having boiling points higher than that of the alkyl (meth)acrylate, and from which the alkyl (meth)acrylate is separated by distillation in a separation zone. The product mixture discharged from the reaction zone is fed to a rectification unit (I), in this unit the product mixture discharged is separated by rectification into at least one product (I) comprising the alkyl ester of (meth)acrylic acid and a product (II) comprising the catalyst, the product (I) is fed to a further rectification unit (II) and in this the alkyl ester of (meth)acrylic acid is separated off by rectification.
摘要翻译：在反应区酸性酯化催化剂存在下，使（甲基）丙烯酸与具有1〜8个碳原子的一元链烷醇反应连续制备（甲基）丙烯酸烷基酯的方法中，所述反应区包含形成的（甲基）丙烯酸烷基酯，在酯化过程中形成的催化剂和副产物的沸点高于（甲基）丙烯酸烷基酯的产物混合物，并且烷基（甲基）丙烯酸酯在分离区中蒸馏分离。将从反应区排出的产物混合物供给到精馏单元（I），在该单元中，排出的产物混合物通过精馏分离成至少一种包含（甲基）丙烯酸的烷基酯的产物（I）和产物（II），将产物（I）进料到另一精馏单元（II）中，通过精馏分离（甲基）丙烯酸的烷基酯。

7. 发明申请

US20130059723A1 Synthesis of Zeolitic Materials using N,N-Dimethyl Organotemplates 有权
标题翻译：使用N，N-二甲基有机模板合成沸石材料
公开(公告)号：US20130059723A1
公开(公告)日：2013-03-07
申请号：US13605701
申请日：2012-09-06
申请人： Bilge Yilmaz , Ulrich Berens , Vijay Narayanan Swaminathan , Ulrich Müller , Gabriele Iffland , Laszlo Szarvas
发明人： Bilge Yilmaz , Ulrich Berens , Vijay Narayanan Swaminathan , Ulrich Müller , Gabriele Iffland , Laszlo Szarvas
IPC分类号： C01B39/00 , B01D53/94 , C01B39/54 , B01J29/04 , C10G11/05 , C07C1/22
CPC分类号： C10G3/49 , B01D53/9413 , B01D53/9436 , B01D2255/50 , B01J29/70 , B01J29/7015 , B01J29/85 , B01J29/86 , B01J29/87 , B01J2229/183 , C01B39/48 , C01B39/54 , C07C1/20 , C07C2529/70 , C10G11/05 , C10G11/18 , C10G25/03 , C10G2300/405 , Y02C20/10 , C07C11/02
摘要： The present invention relates to a process for the preparation of a zeolitic material having a structure comprising YO2 and optionally comprising X2O3, preferably comprising YO2 and X2O3, wherein said process comprises the steps of (1) providing a mixture comprising one or more ammonium compounds of which the ammonium cation has the formula (I): [R1R2NR3R4]+ (I) and further comprising one or more sources for YO2 and one or more sources for X2O3; (2) crystallizing the mixture provided in (1); wherein Y is a tetravalent element, and X is a trivalent element, and wherein in formula (I) R1 and R2 are independently from one another derivatized or underivatized methyl, and R3 and R4 are independently from one another derivatized or underivatized (C3-C5)alkyl, and wherein the molar ratio of ammonium cation having the formula (I) to Y in the mixture provided in step (1) and crystallized in step (2) is equal to or greater than 0.25.
摘要翻译：本发明涉及一种制备具有包含YO 2和任选地包含X 2 O 3，优选包含YO 2和X 2 O 3的结构的沸石材料的方法，其中所述方法包括以下步骤：（1）提供包含一种或多种铵化合物其中铵阳离子具有式（I）：[R 1 R 2 NR 3 R 4] +（I），并且还包含一种或多种YO源和一种或多种X 2 O 3源; （2）使（1）中提供的混合物结晶; 其中Y是四价元素，X是三价元素，并且其中在式（I）中，R 1和R 2彼此独立地是衍生的或未衍生的甲基，并且R 3和R 4彼此独立地是衍生的或未衍生的（C 3 -C 5 ）烷基，并且其中在步骤（1）中提供并在步骤（2）中结晶的混合物中具有式（I）的铵阳离子与Y的摩尔比等于或大于0.25。

8. 发明申请

US20120010431A1 METHOD FOR PRODUCING 1-ADAMANTYL TRIMETHYLAMMONIUM HYDROXIDE 有权
标题翻译： 1-ADAMANTYL TRIMETHYLAMMONIUM HYDROXIDE的生产方法
公开(公告)号：US20120010431A1
公开(公告)日：2012-01-12
申请号：US13255805
申请日：2010-03-11
申请人： Christof Wilhelm Wigbers , Martin Ernst , Laszlo Szarvas , Giovanni D'Andola , Ellen Dahlhoff , Gabriele Iffland , Peter Raatz , Falk Simon , Matthias Frauenkron
发明人： Christof Wilhelm Wigbers , Martin Ernst , Laszlo Szarvas , Giovanni D'Andola , Ellen Dahlhoff , Gabriele Iffland , Peter Raatz , Falk Simon , Matthias Frauenkron
IPC分类号： C07C211/33
CPC分类号： C07C211/63 , C07C209/00 , C07C209/26 , C07C2603/74
摘要： The present invention relates to a process for preparing 1-adamantyltrimethyl-ammonium hydroxide.
摘要翻译：本发明涉及一种制备1-金刚烷基三甲基氢氧化铵的方法。

9. 发明授权

US06300467B1 Production of polytetrahydrofuran with terminal hydroxyl groups by changing the continuous and dispersed phase 有权
标题翻译：通过改变连续和分散相来生产具有末端羟基的聚四氢呋喃
公开(公告)号：US06300467B1
公开(公告)日：2001-10-09
申请号：US09445993
申请日：2000-03-29
申请人： Heinz Auer , Jürgen Ciprian , Lothar Franz , Wolfgang Franzischka , Gabriele Iffland , Alexander Weck , Werner Weinle
发明人： Heinz Auer , Jürgen Ciprian , Lothar Franz , Wolfgang Franzischka , Gabriele Iffland , Alexander Weck , Werner Weinle
IPC分类号： C08F600
CPC分类号： C08G65/30 , C08G65/20 , C08G65/3312
摘要： The present invention relates to a process for preparing hydroxyl-containing polymers, in particular for preparing polytetrahydrofuran with terminal hydroxyl groups, from the corresponding acyloxy-containing polymers by transesterification with alcohols in the presence of an alkali metal- or alkaline earth metal-containing catalyst, which entails the appropriate acyloxy-containing polymer being introduced together with the alcohol and the catalyst into a first prereactor (I) and converted therein at least partly to the hydroxyl-containing polymer, and the reaction solution being fed into the upper zone (IIa) of a distillation column (II) into whose lower zone (IIb) alcohol in vapor phase is additionally fed. This involves a phase exchange at the coherent and the disperse phase at the transition from the prereactor to the distillation column. Preferably, in addition to the first prereactor, a further 3 prereactors are used which serve as holdup reactors.
摘要翻译：本发明涉及一种制备含羟基聚合物的方法，特别是通过在含碱金属或碱土金属的催化剂存在下与醇进行酯交换从相应的含酰氧基的聚合物制备具有末端羟基的聚四氢呋喃，其使得适当的含酰氧基的聚合物与醇和催化剂一起引入第一预反应器（I）中并在其中至少部分地转化为含羟基聚合物，并将反应溶液进料到上部区域（IIa ）蒸馏塔（II），其中进一步加入气相中的低级（IIb）醇。这涉及在从预反应器到蒸馏塔的过渡处的相干和分散相的相交换。优选地，除了第一预反应器之外，还使用用作保持反应器的另外3个预反应器。

10. 发明授权

US08536376B2 Method for removing halogen from liquid ammonia 有权
标题翻译：从液氨中除去卤素的方法
公开(公告)号：US08536376B2
公开(公告)日：2013-09-17
申请号：US12936375
申请日：2009-03-26
申请人： Roland Bou Chedid , Gabriele Iffland , Jürgen Ciprian , Johann-Peter Melder , Frank-Friedrich Pape
发明人： Roland Bou Chedid , Gabriele Iffland , Jürgen Ciprian , Johann-Peter Melder , Frank-Friedrich Pape
IPC分类号： C01C1/02 , C07C211/00
CPC分类号： C01C1/024 , B01J41/05
摘要： A method for depleting halide ions from liquid ammonia, which comprises bringing the liquid ammonia into contact with a strongly basic ion exchanger, where the basic structure of the strongly basic ion exchanger is a covalently crosslinked polymer matrix and the content of ammonia in the liquid ammonia is more than 98% by weight.
摘要翻译：一种用于从液氨中消耗卤离子的方法，其包括使液氨与强碱性离子交换剂接触，其中强碱性离子交换剂的基本结构是共价交联的聚合物基质，液氨中的氨含量超过98重量％。

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