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1. 发明申请

US20050197417A1 Optical fiber coatings 有权
标题翻译：光纤涂层
公开(公告)号：US20050197417A1
公开(公告)日：2005-09-08
申请号：US10928541
申请日：2004-08-26
申请人： Eugene Sitzmann , Jean-Pierre Wolf , David Bramer , Greg Losapio
发明人： Eugene Sitzmann , Jean-Pierre Wolf , David Bramer , Greg Losapio
IPC分类号： C08F2/48 , C08F2/50 , C08F290/06 , C08G2/00 , C09D4/00
CPC分类号： C09D4/00 , C03C25/106 , C08F2/50 , C08F290/06 , C08F290/062 , C08F290/067
摘要： Optical fiber coating compositions which comprise at least one ethylenically unsaturated polymerizable compound and a photoinitiator blend, wherein the blend comprises (a) bis(2,4,6-trimethylbenzoyl)phenylphosphine oxide and (b) 2,4,6,-trimethylbenzoylethoxyphenylphosphine oxide in an (a):(b) weight:weight ratio of between about 1:10 and about 1:8; or (c) bis(2,4,6-trimethylbenzoyl)phenylphosphine oxide, (d) 2,4,6,-trimethylbenzoylethoxyphenylphosphine oxide and (e) 2-hydroxy-2-methyl-1-phenyl-1-propanone in a (c):(d):(e) weight:weight:weight ratio between about 3:1:14 and about 4:1:16; or (f) bis(2,4,6-trimethylbenzoyl)phenylphosphine oxide and (g) 2-hydroxy-2-methyl-1-phenyl-1-propanone in a (f):(g) weight:weight ratio of between about 1:3 and about 1:5 exhibit fast photospeed, very low color and fast photobleaching. The photoinitiator blends have low volatility, high shelf life stability and high compatibility with resins and monomers. The photoinitiator blends are for example liquid and easy to use.
摘要翻译：包含至少一种烯属不饱和可聚合化合物和光引发剂共混物的光纤涂料组合物，其中所述共混物包含（a）双（2,4,6-三甲基苯甲酰基）苯基氧化膦和（b）2,4,6-三甲基苯甲酰基乙氧基苯基氧化膦（a）：（b）重量：约1:10至约1:8之间的重量比; 或（c）双（2,4,6-三甲基苯甲酰基）苯基氧化膦，（d）2,4,6-三甲基苯甲酰乙氧基苯基氧化膦和（e）2-羟基-2-甲基-1-苯基-1-丙酮（c）:( d）:( e）重量：重量：约3：1：14和4：1：16之间的重量比; 或（f）双（2,4,6-三甲基苯甲酰基）苯基氧化膦和（g）2-羟基-2-甲基-1-苯基-1-丙酮：（f）:( g）重量：约1：3和约1：5显示快速的速度，非常低的颜色和快速的漂白。光引发剂共混物具有低挥发性，高保质期稳定性和与树脂和单体的高相容性。光引发剂共混物例如是液体且易于使用。

2. 发明授权

US07169826B2 Optical fiber coatings 有权
标题翻译：光纤涂层
公开(公告)号：US07169826B2
公开(公告)日：2007-01-30
申请号：US10928541
申请日：2004-08-26
申请人： Eugene V. Sitzmann , Jean-Pierre Wolf , David Bramer , Greg Losapio
发明人： Eugene V. Sitzmann , Jean-Pierre Wolf , David Bramer , Greg Losapio
IPC分类号： C08F2/50 , C09D11/00
CPC分类号： C09D4/00 , C03C25/106 , C08F2/50 , C08F290/06 , C08F290/062 , C08F290/067
摘要： Optical fiber coating compositions which compriseat least one ethylenically unsaturated polymerizable compound anda photoinitiator blend, wherein the blend comprises(a) bis(2,4,6-trimethylbenzoyl)phenylphosphine oxide and (b) 2,4,6,-trimethylbenzoylethoxyphenylphosphine oxide in an (a):(b) weight:weight ratio of between about 1:10 and about 1:8; or (c) bis(2,4,6-trimethylbenzoyl)phenylphosphine oxide, (d) 2,4,6,-trimethylbenzoylethoxyphenylphosphine oxide and (e) 2-hydroxy-2-methyl-1-phenyl-1-propanone in a (c):(d):(e) weight:weight:weight ratio between about 3:1:14 and about 4:1:16; or (f) bis(2,4,6-trimethylbenzoyl)phenylphosphine oxide and (g) 2-hydroxy-2-methyl-1-phenyl-1-propanone in a (f):(g) weight:weight ratio of between about 1:3 and about 1:5 exhibit fast photospeed, very low color and fast photobleaching. The photoinitiator blends have low volatility, high shelf life stability and high compatibility with resins and monomers. The photoinitiator blends are for example liquid and easy to use.
摘要翻译：包含至少一种烯属不饱和可聚合化合物和光引发剂共混物的光纤涂料组合物，其中所述共混物包含（a）双（2,4,6-三甲基苯甲酰基）苯基氧化膦和（b）2,4,6-三甲基苯甲酰基乙氧基苯基氧化膦（a）：（b）重量：约1:10至约1:8之间的重量比; 或（c）双（2,4,6-三甲基苯甲酰基）苯基氧化膦，（d）2,4,6-三甲基苯甲酰乙氧基苯基氧化膦和（e）2-羟基-2-甲基-1-苯基-1-丙酮（c）:( d）:( e）重量：重量：约3：1：14和4：1：16之间的重量比; 或（f）双（2,4,6-三甲基苯甲酰基）苯基氧化膦和（g）2-羟基-2-甲基-1-苯基-1-丙酮：（f）:( g）重量：约1：3和约1：5显示快速的速度，非常低的颜色和快速的漂白。光引发剂共混物具有低挥发性，高保质期稳定性和与树脂和单体的高相容性。光引发剂共混物例如是液体且易于使用。

3. 发明申请

US20050165141A1 Thermally stable cationic photocurable compositions 审中-公开
标题翻译：耐热稳定的阳离子光固化组合物
公开(公告)号：US20050165141A1
公开(公告)日：2005-07-28
申请号：US11040716
申请日：2005-01-21
申请人： Jean-Pierre Wolf , Stephen Ilg , Jean-Luc Birbaum , Eugene Sitzman , David Bramer , Greg Losapio
发明人： Jean-Pierre Wolf , Stephen Ilg , Jean-Luc Birbaum , Eugene Sitzman , David Bramer , Greg Losapio
IPC分类号： C08G59/18 , C08G59/68 , G03F7/00 , G03F7/038 , C08K5/34 , C08K5/49
CPC分类号： G03F7/0037 , C08G59/18 , C08G59/24 , C08G59/68 , G03F7/038
摘要： Disclosed are cationic photocurable compositions with improved shelf life stability. The thermally stable compositions comprise at least one cationically polymerizable compound, for example an epoxy compound, at least one onium salt photoinitiator and at least one compound selected from the group consisting of the organic phosphorus stabilizers and the hindered nitroxyl stabilizers. Also disclosed is a cationic photoinitiator composition comprising at least one onium salt photoinitiator and at least one compound selected from the group consisting of the organic phosphorus stabilizers and the hindered nitroxyl stabilizers.
摘要翻译：公开了具有改善的保质期稳定性的阳离子光固化组合物。热稳定组合物包含至少一种阳离子可聚合化合物，例如环氧化合物，至少一种鎓盐光引发剂和至少一种选自有机磷稳定剂和受阻硝酰基稳定剂的化合物。还公开了包含至少一种鎓盐光引发剂和至少一种选自有机磷稳定剂和受阻硝酰基稳定剂的化合物的阳离子光引发剂组合物。

4. 发明申请

US20070225395A1 Thermally stable cationic photocurable compositions 审中-公开
标题翻译：耐热稳定的阳离子光固化组合物
公开(公告)号：US20070225395A1
公开(公告)日：2007-09-27
申请号：US11803274
申请日：2007-05-14
申请人： Jean-Pierre Wolf , Stephen Ilg , Jean-Luc Birbaum , Eugene Sitzman , David Bramer , Greg Losapio
发明人： Jean-Pierre Wolf , Stephen Ilg , Jean-Luc Birbaum , Eugene Sitzman , David Bramer , Greg Losapio
IPC分类号： C08F2/46
CPC分类号： G03F7/0037 , C08G59/18 , C08G59/24 , C08G59/68 , G03F7/038
摘要： Disclosed are cationic photocurable compositions with improved shelf life stability. The thermally stable compositions comprise at least one cationically polymerizable compound, for example an epoxy compound, at least one onium salt photoinitiator and at least one compound selected from the group consisting of the organic phosphorus stabilizers and the hindered nitroxyl stabilizers. Also disclosed is a cationic photoinitiator composition comprising at least one onium salt photoinitiator and at least one compound selected from the group consisting of the organic phosphorus stabilizers and the hindered nitroxyl stabilizers.
摘要翻译：公开了具有改善的保质期稳定性的阳离子光固化组合物。热稳定组合物包含至少一种阳离子可聚合化合物，例如环氧化合物，至少一种鎓盐光引发剂和至少一种选自有机磷稳定剂和受阻硝酰基稳定剂的化合物。还公开了包含至少一种鎓盐光引发剂和至少一种选自有机磷稳定剂和受阻硝酰基稳定剂的化合物的阳离子光引发剂组合物。

5. 发明申请

US20140046195A1 IN VIVO BIOLUMINESCENCE MONITORING APPARATUS 有权
标题翻译：生物荧光监测装置
公开(公告)号：US20140046195A1
公开(公告)日：2014-02-13
申请号：US14112641
申请日：2012-04-17
申请人： Ueli Schibler , Andre Liani , Camille Saini , Luigi Bonacina , Jean-Pierre Wolf
发明人： Ueli Schibler , Andre Liani , Camille Saini , Luigi Bonacina , Jean-Pierre Wolf
IPC分类号： A61B5/00
CPC分类号： A61B5/0059 , A01K1/031 , A01K29/005 , G01N21/763
摘要： Apparatus for real-time in vivo bioluminescence monitoring in a conscious small animal, comprising a light-tight enclosure (4) with a base (16), side wall (19) and cover (20) configured for housing the small animal such that it may move freely, a bioluminescence detector system (6) comprising a light detector (22) for detecting the light emitted by said small animal connected to a data processing system, and a life sustaining system (8) configured for maintaining the small animal alive for a prolonged period of time spanning from a few days to a few weeks.
摘要翻译：一种用于在有意识的小动物中进行实时体内生物发光监测的装置，包括具有底座（16），侧壁（19）和盖（20）的不透光外壳（4），其被配置用于容纳小动物，可自由移动的生物发光检测器系统（6），其包括用于检测由连接到数据处理系统的所述小动物发射的光的光检测器（22），以及维持生物维持系统（8）延长的时间是从几天到几周。

6. 发明授权

US07901867B2 Sulphonium salt initiators 有权
标题翻译：锍盐引发剂
公开(公告)号：US07901867B2
公开(公告)日：2011-03-08
申请号：US11922444
申请日：2006-06-21
申请人： Jean-Pierre Wolf , Attila Latika , Jean-Luc Birbaum , Stephan Ilg , Pascal Hayoz
发明人： Jean-Pierre Wolf , Attila Latika , Jean-Luc Birbaum , Stephan Ilg , Pascal Hayoz
IPC分类号： G03F7/004 , G03F7/30 , C07C381/12
CPC分类号： C07D209/88 , B33Y70/00 , C07C309/06 , C07C381/12 , G03F7/0045 , G03F7/038 , Y10S430/122
摘要： Compounds of the formula (I), (II), (III), (IV) and wherein, R is hydrogen, C1-C20alkyl; C2-C20alkyl interrupted by one or more O; is -L-X—R2 or -L-R2; R1 has for example one of the meanings as given for R; R2 is a monovalent sensitizer or photoinitiator moiety; Ar1 and Ar2 for example independently of one another are phenyl substituted by C1-C20alkyl, halogen or OR3; or are unsubstituted naphthyl, anthryl, phenanthryl or biphenylyl; or are naphthyl, anthryl, phenanthryl or biphenylyl substituted by C1-C20alkyl, OH or OR3; or are —Ar4-A-Ar3; Ar3 is unsubstituted phenyl naphthyl, anthryl, phenanthryl or biphenylyl; or is phenyl, naphthyl, anthryl, phenanthryl or biphenylyl substituted by C1-C20alkyl, OR3 or benzoyl; Ar4 is phenylene, naphthylene, anthrylene or phenanthrylene; A is a direct bond, S, O or C1-C20alkylene; X is CO, C(O)O, OC(O), O, S or NR3; L is C1-C20alkylene or C2-C20alkylene interrupted by one or more O; R3 is C1-C20alkyl or C1-C20hydroxyalkyl; and Y is an anion, are suitable as photolatent acid generators.
摘要翻译：式（I），（II），（III），（IV）的化合物，其中R是氢，C 1 -C 20烷基; 被一个或多个O中断的C 2 -C 20烷基; 是-L-X-R2或-L-R2; R1具有例如R给出的含义之一; R2是单价敏化剂或光引发剂部分; Ar 1和Ar 2例如彼此独立地是被C 1 -C 20烷基，卤素或OR 3取代的苯基; 或未取代的萘基，蒽基，菲基或联苯基; 或被C 1 -C 20烷基，OH或OR 3取代的萘基，蒽基，菲基或联苯基; 或为-Ar4-A-Ar3; Ar 3是未取代的苯基萘基，蒽基，菲基或联苯基; 或由C 1 -C 20烷基，OR 3或苯甲酰基取代的苯基，萘基，蒽基，菲基或联苯基; Ar4是亚苯基，亚萘基，亚蒽基或菲基; A是直接键合，S，O或C1-C20亚烷基; X是CO，C（O）O，OC（O），O，S或NR 3; L是被一个或多个O中断的C 1 -C 20亚烷基或C 2 -C 20亚烷基; R3是C1-C20烷基或C1-C20羟烷基; 并且Y是阴离子，适合作为光潜酸产生剂。

7. 发明申请

US20100283992A1 METHOD OF OPTICAL TELEDETECTION OF COMPOUNDS IN A MEDIUM 有权
标题翻译：中等化合物的光学检测方法
公开(公告)号：US20100283992A1
公开(公告)日：2010-11-11
申请号：US12602245
申请日：2008-05-26
申请人： Jérôme Kasparian , Jean-Pierre Wolf
发明人： Jérôme Kasparian , Jean-Pierre Wolf
IPC分类号： G01J3/00 , G01N21/49
CPC分类号： G01J3/42 , F21S41/675 , G01J3/457 , G01N21/31 , G01N21/538 , G01N2021/1795 , G01N2021/4709 , G01S7/4802 , G01S17/95 , Y02A90/19
摘要： The invention relates to a method of optical teledetection of compounds in a medium in which: a detection measurement is carried out by emitting into the medium, short pulses of light at least 3 nm wide, and detecting a part of the light back-scattered by the medium by means of a detection unit with temporal resolution, a reference measurement in which the light emitted or the light back-scattered is filtered by virtue of addressable filtering means, simulating the optical spectrum of the light at the working wavelengths of at least one given compound to be searched for, a comparison of a detection measurement and of a reference measurement, so as to deduce therefrom the possible presence of the compound or compound(s) searched for in the medium, the addressable filtering means are modified dynamically, and a series of reference measurements and a series of corresponding comparisons are performed for a series of various compounds liable to be present in the medium, as well as a device adapted for implementing such a method.
摘要翻译：本发明涉及一种在介质中对化合物进行光电检测的方法，其中：通过向介质中发射检测测量，至少3nm宽的短脉冲光，并通过以下步骤检测部分光反向散射通过具有时间分辨率的检测单元的介质，借助于可寻址滤波装置对发射的光或光反向散射进行滤波的参考测量，模拟在至少一个工作波长处的光的光谱给定化合物进行检索，检测测量和参考测量的比较，从而推断出在介质中搜索的化合物或化合物的可能存在，可寻址过滤装置被动态修改，以及对一系列易于存在于介质中的各种化合物进行一系列参考测量和一系列相应的比较，以及一种装置适于实施这种方法。

8. 发明授权

US07588880B2 Incorporable photoinitiator 有权
标题翻译：可并入的光引发剂
公开(公告)号：US07588880B2
公开(公告)日：2009-09-15
申请号：US10512300
申请日：2003-04-17
申请人： Jean-Pierre Wolf , Rinaldo Hüsler , Wolfgang Peter , Reinhard H. Sommerlade , Souâd Boulmaâz
发明人： Jean-Pierre Wolf , Rinaldo Hüsler , Wolfgang Peter , Reinhard H. Sommerlade , Souâd Boulmaâz
IPC分类号： G03C1/73 , G03C1/735 , G03F7/028 , C08F2/50 , C07C49/12
CPC分类号： C08F2/50 , B33Y70/00
摘要： Compounds of formula I Y is, for example, C3-C12alkylene, butenylene, butynylene, or C4-C12alkylene interrupted one or more times by non-consecutive —O— or —NR2—; R1 is a reactive group selected from OH, SH, NR3R4, —(CO)—OH, —(CO)—NH2, SO3H, —C(R5)═CR6R7, oxiranyl, —O—(CO)—NH—R8—NCO and —O—(CO)—R9—(CO)—X; R2 is hydrogen, C1-C4alkyl or C2-C4hydroxyalkyl; R3 and R4 are each independently of the other hydrogen, C1-C4alkyl or C2-C4hydroxyalkyl; R5, R6 and R7 are each independently of the others hydrogen or methyl; R8 is, for example, linear or branched C4-C12alkylene, or phenylene; R9 is, for example, linear or branched C1-C16alkylene, —CH═CH—, —CH═CH—CH2—, C6-cycloalkylene, phenylene or naphthylene; and X, X1 and X2 are each independently of the others OH, Cl, OCH3 or OC2H5; are suitable as photoinitiators that can be incorporated in a formulation to be cured.
摘要翻译：式I Y的化合物是例如C 3 -C 12亚烷基，亚丁烯基，亚丁炔基或C 4 -C 12亚烷基被非连续的-O-或-NR 2 - 间隔一次或多次; R1是选自OH，SH，NR3R4， - （CO）-OH， - （CO）-NH2，SO3H，-C（R5）-CR6R7，环氧乙烷基，-O-（CO）-NH-R8- NCO和-O-（CO）-R9-（CO）-X; R2是氢，C1-C4烷基或C2-C4羟烷基; R 3和R 4各自独立地为氢，C 1 -C 4烷基或C 2 -C 4羟烷基; R5，R6和R7各自独立地为氢或甲基; R8是例如直链或支链C 4 -C 12亚烷基或亚苯基; R 9为例如直链或支链C 1 -C 16亚烷基，-CH-CH-，-CH-CH-CH 2 - ，C 6 - 亚环烷基，亚苯基或亚萘基; X，X 1和X 2各自独立地为OH，Cl，OCH 3或OC 2 H 5; 适合作为可引入待固化制剂中的光引发剂。

9. 发明申请

US20060100298A1 Storage stability of photoinitiators 有权
标题翻译：光引发剂的储存稳定性
公开(公告)号：US20060100298A1
公开(公告)日：2006-05-11
申请号：US10531482
申请日：2003-10-17
申请人： Thomas Ulrich , Thomas Bolle , Kurt Dietliker , Jean-Pierre Wolf , Andre Fuchs
发明人： Thomas Ulrich , Thomas Bolle , Kurt Dietliker , Jean-Pierre Wolf , Andre Fuchs
IPC分类号： C08F2/50
CPC分类号： C07D295/096 , B33Y70/00 , C07D295/112 , C08F2/50 , C09D11/101 , G03F7/0007 , G03F7/001 , G03F7/0037 , G03F7/031
摘要： Compounds of formula (I), wherein R1 is hydrogen or alkyl; R2 is C1-C4alkoxy or a morpholino radical; and R3 is hydrogen or C1-C4alkoxy, are suitable for improving the solubility of specific photoinitiators in formulations and accordingly enhance the storage stability of formulations comprising a photoinitiator and compounds of formula (I).
摘要翻译：式（I）化合物，其中R 1是氢或烷基; R 2是C 1 -C 4烷氧基或吗啉代基; R 3和R 3是氢或C 1 -C 4烷氧基，适用于提高特定光引发剂在制剂中的溶解度并因此增强储存包含光引发剂和式（I）化合物的制剂的稳定性。

10. 发明授权

US07026017B2 Organometallic monoacylalkylphosphines 失效
公开(公告)号：US07026017B2
公开(公告)日：2006-04-11
申请号：US10280819
申请日：2002-10-25
申请人： Jean-Pierre Wolf , Gebhard Hug
发明人： Jean-Pierre Wolf , Gebhard Hug
IPC分类号： G03F7/031 , C08F2/50 , C07F9/28 , C07F9/50 , C07F9/53
CPC分类号： G03F7/029 , A61K6/0052 , B33Y70/00 , C07F9/28 , C07F9/5036 , C07F9/5337 , C07F9/65502 , C08F2/46 , C08K5/5397 , C09D11/101 , G03F7/0045 , G03F7/038 , G03F7/0384 , G03F7/0388 , Y10T428/26 , Y10T428/31504
摘要： Compounds of the formula I in which Ar is a group or unsubstituted or substituted cyclopentyl, cyclohexyl, naphthyl, biphenylyl or an O-, S- or N-containing 5- or 6-membered heterocyclic ring; R1 and R2 are C1-C20alkyl, OR11, CF3 or halogen; R3, R4 and R5 are hydrogen, C1-C20alkyl, OR11 or halogen; R6 is unsubstituted or substituted C1-C24alkyl, C2-C24alkyl, which is interrupted by O, S or NR14 and is unsubstituted or substituted; C2-C24alkenyl, uninterrupted or interrupted by O, S or NR14 and unsubstituted or substituted; unsubstituted or substituted C7-C24arylalkyl; C4-C24cycloalkyl, uninterrupted or interrupted by O, S and/or NR14; or C8-C24arylcycloalkyl; R11 is C1-C20alkyl, C3-C8cycloalkyl, phenyl, benzyl or C2-C20alkyl, interrupted by O or S and unsubstituted or substituted; R12 and R13 are hydrogen, C1-C20alkyl, C3-C8cycloalkyl, phenyl, benzyl or C2-C20alkyl, interrupted by O atoms and unsubstituted or substituted; or R12 and R13 together are C3-C5alkylene, uninterrupted or interrupted by O, S or NR14; R14 is hydrogen, phenyl, C1-C12alkyl or C2-C12alkyl, interrupted by O or S and unsubstituted or substituted; and M is hydrogen, Li, Na or K; are valuable intermediates for the preparation of unsymmetrical bisacylphosphine oxides and monoacylphosphine oxides.

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