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1. 发明授权

US4128675A Process for treating textiles with reactive polymers 失效
标题翻译：用反应性聚合物处理纺织品的方法
公开(公告)号：US4128675A
公开(公告)日：1978-12-05
申请号：US786162
申请日：1977-04-11
申请人： Erich Rossler , Hans Deiner , Bernhard Sandner , Hans Schilling
发明人： Erich Rossler , Hans Deiner , Bernhard Sandner , Hans Schilling
IPC分类号： D06M15/29 , B05D3/02
CPC分类号： D06M15/29 , Y10T428/31663 , Y10T428/31931 , Y10T428/31935
摘要： An aqueous medium containing reactive polymers, the reactive groups being N-methylol and/or etherified N-methylol groups, preferably based on methylolated, etherified or not, unsaturated carboxylic acid amides, included by polymerization, the portion of said reactive monomers being preferably 2.5 to 20% by weight, related to the total weight of the polymers, is applied to textiles by impregnation or preferably by coating in the presence of silanes and/or siloxanes containing amino groups and organometallic compounds, preferably zinc soaps and/or dialkyl-tin dicarboxylates as hardening agents, and heated at elevated temperature. A waterproof and water-repellent finish is obtained, resistant to washing and dry cleaning.
摘要翻译：包含反应性聚合物的水性介质，反应性基团是N-羟甲基和/或醚化的N-羟甲基，优选基于聚合所包括的羟甲基化，醚化或不饱和羧酸酰胺，所述反应性单体的部分优选为2.5 相对于聚合物的总重量为20重量％，通过浸渍或优选通过在含有氨基和有机金属化合物的硅烷和/或硅氧烷的存在下，优选锌皂和/或二烷基锡二羧酸盐作为硬化剂，并在升高的温度下加热。获得防水和防水的表面，耐洗涤和干洗。

2. 发明授权

US4153640A Modified polysiloxanes and process of preparing them 失效
标题翻译：改性聚硅氧烷及其制备方法
公开(公告)号：US4153640A
公开(公告)日：1979-05-08
申请号：US774161
申请日：1977-03-03
申请人： Hans Deiner , Bernhard Sandner , Willy Bernheim
发明人： Hans Deiner , Bernhard Sandner , Willy Bernheim
IPC分类号： C09K3/18 , C08F2/00 , C08F2/44 , C08F283/12 , D06M13/02 , D06M13/322 , D06M13/325 , D06M13/345 , D06M13/51 , D06M13/513 , D06M15/263 , D06M15/643 , C08G77/12 , C08G77/20 , C08L43/04 , C08L83/04
CPC分类号： D06M15/643 , C08F283/12 , D06M15/263 , Y10T428/2933 , Y10T428/2962
摘要： A process for the production of modified polymers, preferable in organic solvents, by radical-initiated polymerization of(Ia) 70 to 99.9 parts by weight of esters of the formulaCH.sub.2 .dbd.C(R)--COOR' (Ia) in which R is --H or --CH.sub.3 and R' are 1 to 18 C-alkyl radicals, at least 50% by weight of the esters of (Ia) being those in which R' are 1 to 4 C-alkyl radicals,(Ib) 0, 1 to 20 parts by weight of .omega.-hydroxyalkyl esters of acrylic, methacrylic, maleic and/or fumaric esters, the said dicarboxylic acids are possibly etherified on the second carboxylic group with 1 to 12 C-atoms containing alcohols and(Ic) 0 to 10 parts by weight of other unsaturated monomers, the sum of (Ia), (Ib) and (Ic) amounting to 100 parts by weight, in the presence of(II) 5 to 40 parts by weight of terminal blocked alkyl-hydrogen polysiloxanes, the alkyl radicals containing 1 to 4 carbon atoms, with a viscosity of 20 to 1000 cP at 20.degree. C., the ratio of alkyl radicals to hydrogen atoms thereof being from 13 : 1 to 1 : 1, in which ratios the terminal groups are not included. Organic solvents containing the obtained modified polymers and usual curing agents for alkyl-hydrogen polysiloxanes are useful for treating fibrous material to give water-tight and water-repellent effects.
摘要翻译：通过（Ia）70至99.9重量份式CH 2 = C（R）-COOR'（Ia）的酯的自由基引发聚合制备改性聚合物的方法，优选在有机溶剂中，其中R为 -H或-CH 3和R'是1至18个C-烷基，至少50重量％的（Ia）的酯是其中R'是1至4个C-烷基，（Ib）0， 1至20重量份的丙烯酸，甲基丙烯酸，马来酸和/或富马酸的ω-羟烷基酯，所述二羧酸可能在含有1至12个碳原子的醇的第二羧基上醚化，并且（Ic）0至 10重量份的其它不饱和单体，在（II）5-40重量份末端封端的烷基 - 氢聚硅氧烷的存在下，（Ia），（Ib）和（Ic）的总和为100重量份，含有1至4个碳原子的烷基，在20℃下的粘度为20至1000cP，烷基与氢原子的比例为13:1至 1：1，其中不包括端基。含有所得改性聚合物的有机溶剂和烷基氢聚硅氧烷的常用固化剂可用于处理纤维材料以提供防水和防水效果。

3. 发明授权

US4477498A Process for the production of perfluoroalkyl residue containing condensation products, the condensation products prepared accordingly, and their use 失效
标题翻译：生产含有缩合产物的全氟烷基残基的方法，相应制备的缩合产物及其用途
公开(公告)号：US4477498A
公开(公告)日：1984-10-16
申请号：US408084
申请日：1982-08-13
申请人： Hans Deiner , Franz Mosch , Bernhard Sandner , Willy Bernheim
发明人： Hans Deiner , Franz Mosch , Bernhard Sandner , Willy Bernheim
IPC分类号： C07D251/70 , D06M13/02 , D06M13/248 , D06M13/252 , D06M13/322 , D06M13/35 , D06M13/355 , D06M13/358 , B05D3/02
CPC分类号： C07D251/70
摘要： The present invention relates to new condensation products of(A) 1 mole of a highly etherified hexamethylol melamine and(B) 3 to 6 moles of a thiol of the formulaR.sub.f --X--SH, (1) Rf standing for perfluorinated alkyl with 4 to 14 C-atoms and X for divalent ethylene or isopropylene radicals, wherein the components (A) and (B) are reacted under increasing temperature up to at least 145.degree. C. within a period of at least 40 minutes.In form of their aqueous dispersions, the condensation products are suitable for oil- and water-repellent finishing of fibrous, preferably textile materials.
摘要翻译：本发明涉及（A）1摩尔高度醚化的六羟甲基三聚氰胺和（B）3至6摩尔式Rf-X-SH的硫醇的新的缩合产物，（1）Rf代表全氟烷基与4 至14个碳原子，X为二价乙烯或异丙烯基，其中组分（A）和（B）在至少40分钟的时间内在升高的温度下反应至多至145℃。以其水分散体的形式，缩合产物适用于纤维，优选纺织材料的防油和防水整理。

4. 发明授权

US4004059A Method to make fibrous material oil and water repellent at the same time 失效
标题翻译：同时使纤维材料防油和防水的方法
公开(公告)号：US4004059A
公开(公告)日：1977-01-18
申请号：US547078
申请日：1975-02-04
申请人： Hans Deiner , Bernhard Sandner , Willy Bernheim
发明人： Hans Deiner , Bernhard Sandner , Willy Bernheim
IPC分类号： C09K3/00 , C09K3/18 , D06M15/277 , D06M15/643 , D06M13/18
CPC分类号： D06M15/643 , D06M15/277 , Y10T428/2962 , Y10T428/31544 , Y10T442/2172
摘要： While good oil-repellency can be imparted to fibre materials by treating them with polymers containing perfluoralkyl groups, it is difficult to impart water-repellency to the fibre materials at the same time and also give the treated materials a good handle. This is achieved by treating the fibre materials with, besides the perfluoralkyl group-containing polymers, an addition product of a) an unsaturated compound which is an olefin, a vinyl or allyl ester of an aliphatic straight or branched chain acid, a vinyl ether whose alkyl radical has at least 4 carbon atoms, an allyl ether whose alkyl radical has at least 4 carbon atoms and/or a vinyl halide with b) an organopolysiloxane which contains hydrogen atoms bonded to silicon atoms, the addition product containing on average more than 7 carbon atoms in the alkyl radical and at least 0.20 mole of the unsaturated component a) per gram atom of hydrogen in the siloxane component b).
摘要翻译：通过用含有全氟烷基的聚合物处理纤维材料，可以赋予纤维材料良好的拒油性，难以同时赋予纤维材料防水性，并且也使处理过的材料具有良好的手感。这是通过除含全氟烷基的聚合物以外处理纤维材料来实现的，该加成产物是a）不饱和化合物，其是烯烃，脂族直链或支链酸的乙烯基或烯丙酯，乙烯基醚，烷基具有至少4个碳原子，其烷基具有至少4个碳原子的烯丙基醚和/或乙烯基卤化物，以及b）含有与硅原子键合的氢原子的有机聚硅氧烷，该加成产物平均含有7个以上烷基中的碳原子和至少0.20摩尔不饱和组分a）在硅氧烷组分b）中每克原子的氢。

5. 发明授权

US5019428A Modified polyurethanes containing perfluoroaliphatic groups and use thereof 失效
标题翻译：含有全氟脂肪族基团的改性聚氨酯及其用途
公开(公告)号：US5019428A
公开(公告)日：1991-05-28
申请号：US301681
申请日：1989-01-25
申请人： Simpert Ludemann , Michael Bernheim , Bernhard Sandner , Erich Rossler , Hans-Burkhardt Vogel
发明人： Simpert Ludemann , Michael Bernheim , Bernhard Sandner , Erich Rossler , Hans-Burkhardt Vogel
IPC分类号： C08G18/08 , C08G18/00 , C08G18/10 , C08G18/38 , C08G18/61 , C08G18/77 , C08G18/83 , C08L75/04 , D06M15/576
CPC分类号： D06M15/576 , C08G18/10 , C08G18/387 , C08G18/837 , C08L75/04 , Y10T442/2172
摘要： Modified polyurethanes containing perfluoroaliphalic groups which are obtained by reacting oligo(poly)urethanes containing free hydroxyl or isocyanate groups and perfluoroaliphatic groups with di/polyfunctional polysiloxanes at elevated temperatures with conversion of all the reactive groups of the urethane are used for the oil- and water-repellent finishing of fiber materials, conferring on these materials thus treated not only laundering- and drycleaning-stable effects but also in particular a very soft, full hand of very good surface smoothness, these excellent hand effects being further optimized by the addition of a polyethylene dispersion and/or of further customary textile assistants, in particular water-repellent fluorocarbon compounds.
摘要翻译：通过使含有游离羟基或异氰酸酯基的低聚（聚）氨基甲酸酯和全氟脂肪族基团与二/多官能聚硅氧烷在高温下与氨基甲酸酯的所有反应性基团的转化反应而获得的改性聚氨酯用于油和水 - 对纤维材料进行精加工，赋予这些材料不仅洗涤和干洗清洁稳定的效果，而且特别是具有非常好的表面光滑度的非常柔软的全手，这些优异的手感通过加入聚乙烯分散体和/或其它常规纺织品助剂，特别是防水氟碳化合物。

6. 发明授权

US4433027A Process for finishing textiles with alkoxylation products, and compositions for this 失效
标题翻译：用烷氧基化产物制成纺织品的方法及其组合物
公开(公告)号：US4433027A
公开(公告)日：1984-02-21
申请号：US448553
申请日：1982-12-10
申请人： Hans Deiner , Bernhard Sandner
发明人： Hans Deiner , Bernhard Sandner
IPC分类号： D06M15/643 , C08G77/00 , C08G77/38 , D06M13/02 , D06M13/51 , D06M13/513 , D06M15/647 , B32B7/00 , B05D3/02
CPC分类号： C08G77/38 , D06M15/647 , Y10T442/2352 , Y10T442/273
摘要： Alkoxylation products in form of solutions in organic solvents or, preferably, in form of aqueous emulsions, stable against hydrolytic influences are used in a process for finishing textile materials to impart to these an excellent soft, superficially smooth fell connected with the improvement of tearing strength, abrasion resistance and sewability.The alkoxylation products are obtained by alkoxylation of hydrogen organopolysiloxanes, in particular of methyl hydrogen polysiloxanes with monovalent saturated and/or unsaturated alcohols having 4 to 22 C atoms.
摘要翻译：在有机溶剂中的溶液形式的烷氧基化产物，或优选以水乳液的形式，对水解影响是稳定的，用于整理纺织材料的方法，以赋予这些优异的柔软，表面光滑的下降，同时提高撕裂强度，耐磨性和缝合性。烷氧基化产物通过氢有机聚硅氧烷，特别是甲基氢聚硅氧烷与具有4至22个C原子的一价饱和和/或不饱和醇的烷氧基化而获得。

7. 发明授权

US4834764A Process for obtaining wash-and cleaning resistant textile finishes with reactive perfluoroalkyl-containing (co) polymers and/or precondensates and a blocked isocyanate compound 失效
标题翻译：具有反应性全氟烷基（共）聚合物和/或预缩合物和封端异氰酸酯化合物的洗涤和清洁抗纺织品整理剂的方法
公开(公告)号：US4834764A
公开(公告)日：1989-05-30
申请号：US124339
申请日：1987-11-20
申请人： Hans Deiner , Bernhard Sandner , Franz Mosch , Willy Bernheim
发明人： Hans Deiner , Bernhard Sandner , Franz Mosch , Willy Bernheim
IPC分类号： C08G18/62 , D06M15/295 , D06M15/576
CPC分类号： D06M15/295
摘要： The present invention relates to a process for obtaining wash- and cleaning-resistant textile finishes by impregnating with customary reactive perfluoroalkyl-containing (co)polymers and/or precondensates in aqueous dispersion and concluding heating, wherein the dispersions have NCO-containing compounds which have a molecular weight of at least 450 and/or contain a diphenylmethane-based polyisocyanate mixture in blocked form.The process according to the invention has made it possible to equip textiles with water-repellant and oil-repellant finishes which are very highly wash- and cleaning-resistant.
摘要翻译：本发明涉及一种通过在含水分散体和结束加热中用常规含反应性全氟烷基（共）聚合物和/或预缩合物浸渍来获得耐洗涤和抗清洁的纺织品整理剂的方法，其中分散体具有含有NCO的化合物，其具有至少450的分子量和/或含有封闭形式的二苯基甲烷基多异氰酸酯混合物。根据本发明的方法使得纺织品具有非常高的耐洗涤和耐清洗性的防水和防油涂层成为可能。

8. 发明授权

US3949136A Fluorine-containing organopolysiloxanes, process for their use 失效
标题翻译：含氟有机聚硅氧烷，其使用方法
公开(公告)号：US3949136A
公开(公告)日：1976-04-06
申请号：US561511
申请日：1975-03-24
申请人： Hans Deiner , Franz Mosch , Bernhard Sandner , Willy Bernheim
发明人： Hans Deiner , Franz Mosch , Bernhard Sandner , Willy Bernheim
IPC分类号： C08G77/392 , D06M15/657 , D06M13/08 , D06M15/66
CPC分类号： D06M15/657 , C08G77/392 , Y10T428/31544 , Y10T428/31663 , Y10T442/2172
摘要： New fluorine-containing organopolysiloxanes are provided which are obtained by reaction in known manner of organopolysiloxanes which contain hydrogen atoms bonded to silicon, a perfluoroalkyl compound for the formulaR.sub.f -- SO.sub.2 -- NH -- CH.sub.2 -- CH = CH.sub.2wherein R.sub.f represents perfluoroalkyl with 6 to 14 carbon atoms, and optionally a fluorine-free vinyl monomer. These new addition products are useful as oil- and water repellents for fibrous textile materials.
摘要翻译：提供新的含氟有机聚硅氧烷，其通过以已知方式与含有与硅键合的氢原子的有机聚硅氧烷反应获得，式Rf-SO 2 -NH-CH 2 -CH = CH 2的全氟烷基化合物，其中Rf表示具有6至14个全氟烷基碳原子和任选的无氟乙烯基单体。这些新添加的产品可用作纤维纺织材料的防油和防水剂。

9. 发明授权

US5112930A Modified polyurethanes containing perfluoroaliphatic groups and use thereof 失效
标题翻译：含有全氟聚醚的改性聚氨酯及其用途
公开(公告)号：US5112930A
公开(公告)日：1992-05-12
申请号：US667721
申请日：1991-03-11
申请人： Simpert Ludemann , Michael Bernheim , Bernhard Sandner , Erich Rossler , Hans-Burkhardt Vogel
发明人： Simpert Ludemann , Michael Bernheim , Bernhard Sandner , Erich Rossler , Hans-Burkhardt Vogel
IPC分类号： C08G18/08 , C08G18/00 , C08G18/10 , C08G18/38 , C08G18/61 , C08G18/77 , C08G18/83 , C08L75/04 , D06M15/576
CPC分类号： D06M15/576 , C08G18/10 , C08G18/387 , C08G18/837 , C08L75/04 , Y10T442/2172
摘要： Modified polyurethanes containing perfluoroaliphatic groups which are obtained by reacting oligo(poly)urethanes containing free hydroxyl or isocyanate groups and perfluoroaliphatic groups with di/polyfunctional polysiloxanes at elevated temperatures with conversion of all the reactive groups of the urethane are used for the oil- and water-repellent finishing of fiber materials, conferring on these materials thus treated not only laundering- and drycleaning-stable effects but also in particular a very soft, full hand of very good surface smoothness, these excellent hand effects being further optimized by the addition of a polyethylene dispersion and/or of further customary textile assistants, in particular water-repellent fluorocarbon compounds.

10. 发明申请

US20070012895A1 Highly concentrated, self-emulsifying preparations containing organopolysiloxanes and alkyl ammonium compounds and their use in aqueous systems 有权
标题翻译：含有有机聚硅氧烷和烷基铵化合物的高浓度自乳化制剂及其在含水体系中的应用
公开(公告)号：US20070012895A1
公开(公告)日：2007-01-18
申请号：US10536720
申请日：2003-12-17
申请人： Bernhard Sandner , Cristina Stanica , Longying Jiang
发明人： Bernhard Sandner , Cristina Stanica , Longying Jiang
IPC分类号： D06M13/224
CPC分类号： C11D3/3742 , C08K5/19 , C08L83/08 , C11D1/62 , D06M13/463 , D06M15/6436 , D06M2200/00 , D06M2200/25 , D06M2200/50 , Y10S8/01 , C08L83/04
摘要： This invention concerns highly concentrated self-emulsifying preparations containing organopolysiloxanes and alkylammonium compounds and use thereof in aqueous systems on textile substrates. More particularly, this invention concerns preparations consisting of fully or partially quaternized amino-functional organopolysiloxanes, quaternary alkylammonium compounds, if appropriate an organic hydrotrope and if appropriate water.
摘要翻译：本发明涉及含有有机聚硅氧烷和烷基铵化合物的高度浓缩的自乳化制剂及其在织物基底上的水性体系中的用途。更具体地，本发明涉及由完全或部分季铵化的氨基官能的有机聚硅氧烷，季烷基铵化合物，如果合适的话，有机水溶助长剂和适当的水组成的制剂。

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