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1. 发明授权

US5864002A Process for coloring polymer resins and products thereof 失效
公开(公告)号：US5864002A
公开(公告)日：1999-01-26
申请号：US733862
申请日：1996-10-18
申请人： Eric B. Stephens , Mark E. Ragsdale , David J. Moody
发明人： Eric B. Stephens , Mark E. Ragsdale , David J. Moody
IPC分类号： C08G18/48 , C08G18/38 , C08G18/50 , C09B69/00 , C09B69/10
CPC分类号： C08G18/3836 , C08G18/38 , C08G18/3872 , C08G18/50 , C08G18/5072 , C09B69/00 , C09B69/106 , C08G2101/00
摘要： A method of providing for manufacturing a colored polymer resin having the steps of:(a) blending a disazo colorant into a mixture of monomers, the colorant having a poly(oxyalkylene) substituent comprising from 2 to 200 alkylene oxide residues, bonded to each end of the disazo chromophore, the poly(oxyalkylene) substituent having a nucleophilic terminal group which is capable of reacting with at least a portion of the monomers;(b) providing conditions under which the monomers and disazo colorant polymerize to form a colored polymer resin.

2. 发明授权

US6077927A Process for coloring polymer resins and products thereof 有权
标题翻译：聚合物树脂及其制品着色方法
公开(公告)号：US6077927A
公开(公告)日：2000-06-20
申请号：US177405
申请日：1998-10-23
申请人： Eric B. Stephens , Mark E. Ragsdale , David J. Moody
发明人： Eric B. Stephens , Mark E. Ragsdale , David J. Moody
IPC分类号： C08G18/48 , C08G18/38 , C08G18/50 , C09B69/00 , C09B69/10
CPC分类号： C08G18/3836 , C08G18/38 , C08G18/3872 , C08G18/50 , C08G18/5072 , C09B69/00 , C09B69/106 , C08G2101/00
摘要： A method of providing for manufacturing a colored polymer resin having the steps of:(a) blending a disazo colorant into a mixture of monomers, the colorant having a poly(oxyalkylene) substituent comprising from 2 to 200 alkylene oxide residues, bonded to each end of the disazo chromophore, the poly(oxyalkylene) substituent having a nucleophilic terminal group which is capable of reacting with at least a portion of the monomers;(b) providing conditions under which the monomers and disazo colorant polymerize to form a colored polymer resin.
摘要翻译：一种提供制造着色聚合物树脂的方法，其具有以下步骤：（a）将双偶氮着色剂混合到单体混合物中，所述着色剂具有包含2至200个氧化烯残基的聚（氧化烯）取代基，其结合到每个末端的双（氧化烯）取代基具有能与至少一部分单体反应的亲核端基; （b）提供单体和双偶氮着色剂聚合以形成着色聚合物树脂的条件。

3. 发明授权

US5240980A Colorants for use in opacified thermoplastic resins 失效
标题翻译：用于不透明热塑性树脂的着色剂
公开(公告)号：US5240980A
公开(公告)日：1993-08-31
申请号：US890353
申请日：1992-05-22
申请人： Todd D. Danielson , David J. Moody , John W. Rekers
发明人： Todd D. Danielson , David J. Moody , John W. Rekers
IPC分类号： C08K5/00 , C08K9/08 , C09B69/00
CPC分类号： C09B69/00 , C08K5/0041 , C08K9/08
摘要： An opacified, semi-crystalline thermoplastic resin composition is provided having a poly(alkyleneoxy) substituted organic chromophore distributed throughout in an amount sufficient to color the resin. The resin composition is particularly useful for molding parts with strict dimensional tolerances as shrinkage of the molded part is minimal.
摘要翻译：提供了一种不透明的半结晶热塑性树脂组合物，其具有遍布全部的聚（亚烷氧基）取代的有机发色团，其量足以使树脂着色。树脂组合物特别适用于具有严格的尺寸公差的模制件，因为模制件的收缩是最小的。

4. 发明授权

US5544645A Combination water heating and space heating apparatus 失效
标题翻译：组合水加热和空间加热装置
公开(公告)号：US5544645A
公开(公告)日：1996-08-13
申请号：US296112
申请日：1994-08-25
申请人： David L. Armijo , Tony R. Baker , Floyd E. Cherington , Delbert S. Christopher , David J. Moody , James J. Mullen , Hugh E. Vinson , John L. Warren , Robert C. Beilfuss , John H. Wiker
发明人： David L. Armijo , Tony R. Baker , Floyd E. Cherington , Delbert S. Christopher , David J. Moody , James J. Mullen , Hugh E. Vinson , John L. Warren , Robert C. Beilfuss , John H. Wiker
IPC分类号： F24H1/18 , F24D3/00 , F24D3/08 , F24D19/10 , F24H1/20 , F24H6/00 , F24D9/00
CPC分类号： F24D19/1066 , F24H1/206 , F24H6/00
摘要： A combination water heating and space heating apparatus includes a water heating unit and a space heating unit releasably coupled with the water heating unit. The water heating unit has a water storage tank and a helically wound tubular heat exchanger inside the tank for exhausting products of combustion from a combustion chamber located in a top part of the tank and for transferring heat from the products of combustion to the surrounding water. The space heating unit is an air handler with an hydronic heat exchanger coil and a blower for blowing air over the coil. Hot water is supplied from the tank to the coil and is returned to the tank by means of a water circulation pump located in the space heating unit. Air blown over the coil is heated by the hot water flowing over the coil. The water heating unit and the space heating unit are coordinately controlled such that priority is given to the potable hot water supply over space heating in the event that sufficient hot water is not available to satisfy both demands. Further, the water heating unit anticipates the additional demand for hot water in response to a demand for space heating by raising the tank temperature setpoint so that the water heating operation is usually initiated, even if the temperature of the water in the tank was already at the original tank temperature setpoint when the demand for space heating occurred.
摘要翻译：组合式水加热和空间加热装置包括水加热单元和与水加热单元可释放地联接的空间加热单元。水加热单元在罐内具有储水箱和螺旋形管状热交换器，用于从位于罐的顶部的燃烧室排出燃烧产物，并将热量从燃烧产物传递到周围的水。空间加热单元是具有水力热交换器线圈和用于在线圈上吹空气的鼓风机的空气处理器。热水从罐供给到线圈，并通过位于空间加热单元中的水循环泵返回到罐中。吹过线圈的空气被流过线圈的热水加热。水加热单元和空间加热单元协调控制，以便在没有足够的热水不能满足这两个要求的情况下，优先考虑空间供暖时的饮用热水供应。此外，水加热单元通过提高储罐温度设定值来响应于对空间加热的需求而增加对热水的需求，使得通常开始水加热操作，即使罐中的水的温度已经在发生空间加热需求时的原始罐温度设定值。

5. 发明授权

US5270363A Poly(oxyalkylene) modified phthalocyanine colorants 失效
标题翻译：聚（氧化烯）改性酞菁着色剂
公开(公告)号：US5270363A
公开(公告)日：1993-12-14
申请号：US935567
申请日：1992-08-24
申请人： Edward W. Kluger , John W. Rekers , David J. Moody
发明人： Edward W. Kluger , John W. Rekers , David J. Moody
IPC分类号： C08K5/43 , C09B47/18 , C09B47/20 , C09B47/22 , C09B47/26 , C09B69/00 , C08K5/3417 , C08K5/04 , C08K5/41
CPC分类号： C09B47/22 , C08K5/43 , C09B47/18 , C09B47/20 , C09B47/26 , C09B69/00
摘要： A colorant for natural or synthetic resinous or polymeric materials, having the formula A--[SO.sub.2 --N(R.sub.2)--Y].sub.1-4 ; wherein: R.sub.2 is selected for example from hydrogen, methyl, cyclohexyl, phenyl or Y; A is a nonionic metallophthalocyanine chromophore which can be substituted for example with halogen, alkyl. alkoxy, alkylthio, or aryloxy; Y is a poly(oxyalkylene) moiety containing at least three monomeric units or mixtures thereof of the formula (--RO--) wherein each R is straight or branched alkylene of 1-4 carbons or mixtures thereof, up to about 20 mole percent of said monomeric units may be connected by one or more linking groups such as alkyleneoxy, --NH--, or --NHCONH--, and wherein Y can be terminated by hydrogen, or by at branch substituents, containing 1--3 groups or moieties selected from alkyl, cycloalkyl, acyl, or aryl; wherein any of the above recited hydrocarbon groups, moieties or substitutents may themselves be substituted with up to four substitutents selected, for example, from alkyl, halogen, mercapto, alkoxycarbonyl, hydroxy, alkoxy, or the like; and wherein each aliphatic hydrocarbon portion or moiety of the groups, moieties or substituents recited above contains from 1-20 carbons.
摘要翻译：具有式A- [SO 2 -N（R 2）-Y] 1-4的天然或合成树脂或聚合物材料的着色剂; 其中：R2选自例如氢，甲基，环己基，苯基或Y; A是非离子金属酞菁发色团，其可以被卤素，烷基取代。烷氧基，烷硫基或芳氧基; Y是包含式（-RO-）的至少三个单体单元或其混合物的聚（氧化烯）部分，其中每个R是1-4个碳的直链或支链亚烷基或其混合物，最多约20摩尔％单体单元可以通过一个或多个连接基团例如亚烷基氧基，-NH-或-NHCONH-连接，并且其中Y可以被氢封端，或者通过分支取代基连接，所述分支取代基包含1-3个选自烷基，环烷基，酰基或芳基; 其中任何上述烃基，部分或取代基本身可以被至多四个选自例如烷基，卤素，巯基，烷氧基羰基，羟基，烷氧基等的取代基取代; 并且其中上述基团，部分或取代基的每个脂族烃部分或部分含有1-20个碳。

6. 发明授权

US5240464A Organic materials having sulfonamido linked poly(oxyalkylene) moieties and their preparation 失效
标题翻译：具有亚磺酰氨基连接的聚（氧化烯）部分的有机材料及其制备
公开(公告)号：US5240464A
公开(公告)日：1993-08-31
申请号：US896508
申请日：1992-06-02
申请人： Edward W. Kluger , Max A. Weaver , Jeffery R. Harris , David J. Moody
发明人： Edward W. Kluger , Max A. Weaver , Jeffery R. Harris , David J. Moody
IPC分类号： C07C311/29 , C07C311/37 , C07C311/40 , C07C311/46 , C07C311/48 , C07D209/14 , C07D209/40 , C07D209/48 , C07D213/85 , C07D213/90 , C07D215/38 , C07D221/18 , C07D233/70 , C07D233/88 , C07D233/90 , C07D277/50 , C07D277/64 , C07D277/82 , C07D285/12 , C07D285/135 , C07D307/34 , C07D317/28 , C07D333/34 , C07D333/36 , C07D333/38 , C07D333/60 , C08G65/329 , C08G65/334 , C09B69/00
CPC分类号： C07D209/48 , C07C311/29 , C07C311/37 , C07C311/40 , C07C311/46 , C07C311/48 , C07D209/14 , C07D209/40 , C07D213/85 , C07D213/90 , C07D215/38 , C07D221/18 , C07D233/70 , C07D233/88 , C07D233/90 , C07D277/50 , C07D277/64 , C07D277/82 , C07D285/135 , C07D307/34 , C07D317/28 , C07D333/34 , C07D333/36 , C07D333/38 , C07D333/60 , C08G65/329 , C08G65/3348 , C09B69/00
摘要： The process for chemically modifying metal-free, organic material for improving one or more properties thereof such as water dispersibility, compatibility with other organics, or increased chemical reactivity, wherein the process includes providing material with from 1-6 sulfonylhalide groups or sulfonate ester groups or mixtures thereof, and contacting the material under sulfonamido forming conditions with one or more reactants containing one or more poly(oxyalkylene) moieties, each of the reactants having from 1 to 4 functional amine groups, and each of the poly(oxyalkylene) moieties being comprised of from about 4 to about 200 epoxide reactant residues at least about 50 mole percent of which residues contain 2-4 carbons.
摘要翻译：化学改性无机有机材料以改进其一种或多种性质如水分散性，与其它有机物的相容性或增加的化学反应性的方法，其中该方法包括提供具有1-6个磺酰卤基团或磺酸酯基团的材料或其混合物，并且在亚磺酰氨基形成条件下使材料与一种或多种含有一个或多个聚（氧化烯）部分的反应物接触，每个反应物具有1至4个官能胺基，并且每个聚（氧化烯）部分为由约4至约200个环氧化物反应物残余物组成，其残留物的至少约50摩尔％含有2-4个碳。

7. 发明授权

US5082938A Organic materials containing poly(oxyalkylene) moieties having enhanced functionality and their preparation 失效
标题翻译：含有具有增强的功能性及其制备的聚（氧化烯）部分的有机材料
公开(公告)号：US5082938A
公开(公告)日：1992-01-21
申请号：US486992
申请日：1990-03-01
申请人： Edward W. Kluger , David J. Moody
发明人： Edward W. Kluger , David J. Moody
IPC分类号： C08G65/26 , C09B69/00
CPC分类号： C09B69/00 , C08G65/2627
摘要： Enhanced branched chain hydroxyl compounds are provided of formulaY--(Z).sub.1-6wherein Y is the residue of a nucleophile devoid of conjugated divalent linking moieties, and each Z is a poly(oxyalkylene) moiety having a molecular weight of from about 200-10,000 and containing at least one glycidol residue, wherein at least one of the primary oxy sites of said glycidol residue is linked preferably directly to a first epoxide residue of three or more carbons, and wherein said first epoxide residue is linked through a secondary oxy site preferably directly to a second epoxide reside having a primary terminal hydroxyl.
摘要翻译：增强的支链羟基化合物由式Y-（Z）1-6提供，其中Y是没有共轭二价连接部分的亲核体的残基，每个Z是分子量为约200的聚（氧化烯）部分 -10,000并且含有至少一个缩水甘油残基，其中所述缩水甘油残基的至少一个主要氧位置优选直接连接到三个或更多个碳的第一环氧化物残基，并且其中所述第一环氧化物残基通过仲氧基优选直接位于具有伯基端羟基的第二环氧化物。

8. 发明授权

US08703945B2 Process and intermediate compounds useful in the preparation of statins, particularly rosuvastatin 失效
标题翻译：用于制备他汀类药物，特别是瑞舒伐他汀的方法和中间体化合物
公开(公告)号：US08703945B2
公开(公告)日：2014-04-22
申请号：US10594380
申请日：2005-03-23
申请人： David J. Moody , Jonathan W. Wiffen
发明人： David J. Moody , Jonathan W. Wiffen
IPC分类号： C07D239/42 , C07D403/12
CPC分类号： C07D405/06 , C07D309/10 , C07D309/30 , Y02P20/55
摘要： There is provided a process for the preparation of a compound of formula (7) wherein R1 represents an alkyl group; R2 represents an aryl group; R3 represents hydrogen, a protecting group or an alkyl group; and R4 represents hydrogen, a protecting group or a SO2R5 group where R5 is an alkyl group, which comprises a) hydroxylating a compound of formula (1) wherein Y represents a halo group; P1 represents hydrogen or a protecting group, and W represents ═O or —OP2, in which P2 represents hydrogen or a protecting group, to give a compound of formula (2), b) oxidixing the compound of formula (2) to give a compound of formula (3), c) coupling the compound of formula (3) with a compound of formula (4), wherein R3 represents a protecting group or an alkyl group; R4 represents a protecting group or a SO2R5 group where R5 is an alkyl group; and R6 represents (PR7R8)+X− or P(═O)R7R8 in which X is an anion and R7 and R8 each independently is an alkyl, aryl.
摘要翻译：提供了制备式（7）化合物的方法，其中R 1表示烷基; R2表示芳基; R3表示氢，保护基或烷基; R 4表示氢，保护基或SO 2 R 5基团，其中R 5为烷基，其包括a）羟基化式（1）的化合物，其中Y表示卤素基团; P1表示氢或保护基，W表示= O或-OP2，其中P2表示氢或保护基，得到式（2）化合物，b）氧化式（2）化合物，得到式（3）化合物，c）将式（3）化合物与式（4）化合物偶联，其中R 3表示保护基或烷基; R4代表保护基团或其中R5为烷基的SO2R5基团; 并且R 6表示其中X为阴离子且R 7和R 8各自独立地为烷基，芳基的（PR 7 R 8）+ X-或P（= O）R 7 R 8。

9. 发明授权

US5591833A Colorants and intermediates therefor having branched poly(oxyalkylene)moieties, and their manufacture 失效
标题翻译：具有支链聚（氧化烯）部分的着色剂和中间体及其制备
公开(公告)号：US5591833A
公开(公告)日：1997-01-07
申请号：US104276
申请日：1993-08-10
申请人： John B. Hines , David J. Moody , Edward W. Kluger
发明人： John B. Hines , David J. Moody , Edward W. Kluger
IPC分类号： C09B69/00 , C09B69/10 , D06P5/13
CPC分类号： C09B69/00
摘要： Colorants and compositions useful as a fugitive or permanent colorant for a variety of substrates, or as intermediates for their manufacture, and having one or more improved properties of enhanced aqueous washability, compatibility with and non-extractibility from thermoplastic resins, or reactivity with resins having reactive functionality, said composition having the formula C(Z).sub.1-8 wherein:C is the residue of a reactant having from 1-8 nucleophilic site residues to which the Z moieties are attached; said Z moieties containing at least about 60 weight percent of poly(oxyalkylene) which is comprised of(a) at least one glycidol residue segment of 2-6 glycidol residues attached to a nucleophilic site of C, wherein said poly(oxyalkylene) contains a total of from 2-20 glycidol residues,(b) and wherein said poly(oxyalkylene) further contains the residues of one or more other epoxide reactants of ethylene oxide (EO), propylene oxide (PO), or butylene oxide (BO), or mixtures thereof, wherein said poly(oxyalkylene) contains a total of from about 10 to about 600 of said EO, PO or BO residues, or mixtures thereof, at least about 75 mole percent of which are EO residues,(c) and with the provisions that the ratio of the total of --0--PO-- and --O--BO-- linkages of all glycidol residues to the total of all functional oxy linkages of said glycidol residues is less than one, and the molar ratio of EO residues to glycidol residues is from 4 to 75.
摘要翻译：可用作各种底物的挥发性或永久性着色剂的着色剂和组合物，或作为其制造的中间体，并且具有一种或多种改进的水性洗涤性，与热塑性树脂的相容性和不可萃取性的改进性能，或与具有所述组合物具有式C（Z）1-8，其中：C是具有与Z部分连接的1-8个亲核位点残基的反应物的残基; 所述Z部分包含至少约60重量％的聚（氧化烯），其由（a）至少一个连接到C的亲核位点的2-6个缩水甘油残基的缩水甘油残基部分组成，其中所述聚（氧化烯）含有总共2-20个缩水甘油残基，（b），其中所述聚（氧化烯）还含有环氧乙烷（EO），环氧丙烷（PO）或环氧丁烷（BO））的一种或多种其它环氧化物反应物的残基，或其混合物，其中所述聚（氧化烯）含有总共约10至约600的所述EO，PO或BO残基或其混合物，其至少约75摩尔％为EO残基，（c）和所有缩水甘油残基的-O-PO-和-O-BO-键的总和与所述缩水甘油残基的所有功能氧键的总和的比例小于1，EO残基与缩水甘油残基为4-75。

10. 发明授权

US5290921A Intermediates and colorants having primary hydroxyl enriched poly (oxyalkylene) moieties and their preparation 失效
标题翻译：具有伯羟基富集聚（氧化烯）部分的中间体和着色剂及其制备
公开(公告)号：US5290921A
公开(公告)日：1994-03-01
申请号：US461852
申请日：1990-01-08
申请人： David J. Moody , Edward W. Kluger , John W. Rekers
发明人： David J. Moody , Edward W. Kluger , John W. Rekers
IPC分类号： C08G65/26 , C09B69/00 , C09B29/033 , C09B29/09 , D06P3/24
CPC分类号： C09B69/00 , C08G65/2627 , Y10S534/01
摘要： The present invention provides primary hydroxyl enhanced colorants having markedly improved reactivities in e.g., polyurethane foams for imparting permanent coloring thereto, the colorants having the formulaC--(Z).sub.1-4are provided wherein C is an azo, methine, or azamethine chromogen and Z is a poly(oxyalkylene) moiety comprised of (1) at least two (A) units independently selected from those of the formulae--CH.sub.2 CH(O--T)CH.sub.2 O-- or --CH.sub.2 CH(O--T)CH.sub.2 O--Tand (2) from none to about 200 (B) units of the formula (--RO--) wherein R is straight or branched chain hydrocarbon of 2-4 carbons, T is a moiety of the formula--CH.sub.2 CH(R.sub.1)--O--(RO).sub.0-40 --CH.sub.2 CH.sub.2 OHwherein R.sub.1 is selected from unsubstituted or substituted alkyl, aryl, alkenyloxyalkyl, alkoxyalkyl or aryloxyalkyl, and wherein the A units comprise at least 0.5 percent of the total A+B units.
摘要翻译：本发明提供具有明显改善的反应性的主要羟基增强着色剂，例如用于赋予永久性着色的聚氨酯泡沫，提供了具有式C-（Z）1-4的着色剂，其中C是偶氮，次甲基或氮杂酮色原体， Z是由（1）独立地选自式-CH 2 CH（OT）CH 2 O-或-CH 2 CH（OT）CH 2 O-T的单元中的至少两个（A）单元组成的聚（氧化烯）部分，（2）约200（B）单位的式（-RO-）其中R是2-4个碳的直链或支链烃，T是式-CH 2 CH（R 1）-O-（RO）0-40- 其中R 1选自未取代或取代的烷基，芳基，烯氧基烷基，烷氧基烷基或芳氧基烷基，其中A单元占总A + B单元的至少0.5％。

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