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1. 发明授权

US4045454A Production of 1-nitroanthraquinone and 1-aminoanthraquinone 失效
标题翻译：生产1-硝基蒽醌和1-氨基蒽醌
公开(公告)号：US4045454A
公开(公告)日：1977-08-30
申请号：US625475
申请日：1975-10-24
申请人： Eiji Yamada , Akira Fukasawa , Shinzaburo Masaki
发明人： Eiji Yamada , Akira Fukasawa , Shinzaburo Masaki
IPC分类号： C07C225/34 , C07C79/10 , C07C79/36 , C09B1/00
CPC分类号： C07C225/34
摘要： A process for producing 1-nitroanthraquinone with high purity which comprises treating crude 1-nitroanthraquinone containing as the main impurities dinitroanthraquinones and .beta.-nitroanthraquinone with an alkali sulfite in an aqueous medium under heating and which is characterized in that the crystals of the crude 1-nitroanthraquinone are pulverized by the aid of a pulverizer, a fine pulverizer or an ultra-fine pulverizer prior to and/or during the treatment with the aqueous alkali sulfite; and a process for producing 1-aminoanthraquinone which comprises subjecting the reaction mixture obtained by the said treatment with the alkali sulfite solution mentioned above, if necessary after further fine pulverization, to a reaction with a reducing agent, or ammonia or an aliphatic or aromatic amine.
摘要翻译：一种高纯度的1-硝基蒽醌的制备方法，其特征在于，在加热下，在水性介质中用碱金属亚硫酸盐处理含有二硝基蒽醌和β-硝基蒽醌的粗1-硝基蒽醌，其特征在于粗1- 在用碱金属亚硫酸盐处理之前和/或处理期间，借助于粉碎机，细粉碎机或超细粉碎机将硝基蒽醌粉碎; 以及一种1-氨基蒽醌的制备方法，该方法包括在进一步精细粉碎后，将上述处理得到的反应混合物用上述碱金属亚硫酸盐溶液与还原剂或氨或脂族或芳族胺反应。

2. 发明授权

US4695407A Method for purifying 1-aminoanthraquinone 失效
标题翻译： 1-氨基蒽醌的纯化方法
公开(公告)号：US4695407A
公开(公告)日：1987-09-22
申请号：US466568
申请日：1983-02-15
申请人： Norio Kotera , Masatoshi Uegaki , Masakatsu Yoshimura , Shinzaburo Masaki , Tatsuo Kaneoya , Takashi Miyaoka , Yuzo Maegawa , Akira Fukasawa
发明人： Norio Kotera , Masatoshi Uegaki , Masakatsu Yoshimura , Shinzaburo Masaki , Tatsuo Kaneoya , Takashi Miyaoka , Yuzo Maegawa , Akira Fukasawa
IPC分类号： C09B1/22 , C07C221/00 , C07C225/34 , C09B1/16 , C07C97/24
CPC分类号： C07C221/00 , C07C225/34
摘要： A method for purifying 1-aminoanthraquinone which comprises previously subjecting a crude 1-aminoanthraquinone to a removal treatment of inorganic impurities so that their content is reduced to not more than 4 wt. % as converted to ash basis or to a removal treatment of iodine-consuming reductive inorganic impurities so that their content is reduced to not more than 2 wt. % as converted to consumed iodine basis, and then rectifying the 1-aminoanthraquinone.
摘要翻译：一种纯化1-氨基蒽醌的方法，其包括先将粗制的1-氨基蒽醌处理无机杂质，使其含量降至不超过4重量％。％转化为灰分或去除处理碘消耗的还原性无机杂质，使其含量降低至不超过2重量％。％转化为消耗碘，然后精馏1-氨基蒽醌。

3. 发明授权

US4289706A Method for producing 1-nitroanthraquinone 失效
标题翻译： 1-硝基蒽醌的制备方法
公开(公告)号：US4289706A
公开(公告)日：1981-09-15
申请号：US61382
申请日：1979-07-27
申请人： Akira Fukasawa , Shinzaburo Masaki , Norio Serizawa
发明人： Akira Fukasawa , Shinzaburo Masaki , Norio Serizawa
IPC分类号： C07C205/47 , C07C20060101 , C07C50/18 , C07C67/00 , C07C201/00
CPC分类号： C07C205/47
摘要： Anthraquinone is nitrated using a mixed acid comprising sulfuric acid and nitric acid, the concentration of sulfuric acid being 70 to 76% by weight and the amount of nitric acid being 33 to 55% by weight based on the total weight of sulfuric acid and nitric acid, whereby 1-nitroanthraquinone is obtained in a high yield and a high purity.
摘要翻译：使用包含硫酸和硝酸的混合酸对蒽醌进行硝化，硫酸的浓度为70〜76重量％，硝酸的量为33〜55重量％，相对于硫酸和硝酸的总重量从而以高产率和高纯度获得1-硝基蒽醌。

4. 发明授权

US4845298A Process for preparation of unsaturated long-chain aliphatic secondary amine 失效
标题翻译：不饱和长链脂肪族仲胺的制备方法
公开(公告)号：US4845298A
公开(公告)日：1989-07-04
申请号：US7219
申请日：1987-01-27
申请人： Takeo Inagaki , Akira Fukasawa , Hiroshi Yamagishi
发明人： Takeo Inagaki , Akira Fukasawa , Hiroshi Yamagishi
IPC分类号： C07B61/00 , B01J31/00 , B01J31/02 , C07C67/00 , C07C209/00 , C07C209/48 , C07C211/21
CPC分类号： C07C209/48
摘要： A process for selectively preparing an unsaturated long-chain aliphatic secondary amine at a high yield comprising reducing an unsaturated aliphatic nitrile having 8 to 22 carbon atoms or a nitrile mixture containing said nitrile with hydrogen in the presence of a Ni hydrogenation catalyst and a carboxylic acid amide at a reaction temperature of 160.degree. C. to 200.degree. C.
摘要翻译：一种以高产率选择性制备不饱和长链脂肪族仲胺的方法，包括在Ni氢化催化剂和羧酸存在下还原具有8-22个碳原子的不饱和脂族腈或含有腈的腈混合物酰胺，反应温度为160〜200℃。

5. 发明授权

US4272396A Enzyme-containing detergent composition 失效
标题翻译：含酶洗涤剂组合物
公开(公告)号：US4272396A
公开(公告)日：1981-06-09
申请号：US96158
申请日：1979-11-20
申请人： Kazuaki Fukano , Ryuichi Nakagawa , Akira Fukasawa , Hiroshi Nishio
发明人： Kazuaki Fukano , Ryuichi Nakagawa , Akira Fukasawa , Hiroshi Nishio
IPC分类号： C11D1/14 , C11D3/37 , C11D3/386 , C11D7/42
CPC分类号： C11D3/0094 , C11D1/143 , C11D3/3707 , C11D3/386
摘要： Enzyme-containing detergent compositions containing, as essential ingredients, .alpha.-olefin sulfonates having 10 to 20 carbon atoms, polyethylene glycols having a weight-average molecular weight of 1,000 to 20,000 and enzymes are presented. These enzyme-containing detergent compositions do not cause the decrease in foaming property when objects being washed are previously soaked in an aqueous solution of the enzyme-containing detergent composition.
摘要翻译：含有作为必要成分的含有10〜20个碳原子的α-烯烃磺酸盐，重均分子量为1,000〜20,000的聚乙二醇和酶的含酶洗涤剂组合物。这些含酶洗涤剂组合物在预先浸泡在含酶洗涤剂组合物的水溶液中时不会引起发泡性的降低。

6. 发明授权

US4407756A Process for producing aminoanthraquinone 失效
标题翻译：生产氨基蒽醌的方法
公开(公告)号：US4407756A
公开(公告)日：1983-10-04
申请号：US39606
申请日：1979-05-16
申请人： Akira Fukasawa , Masakatsu Yoshimura , Tatsuo Kaneoya , Kenji Takahashi
发明人： Akira Fukasawa , Masakatsu Yoshimura , Tatsuo Kaneoya , Kenji Takahashi
IPC分类号： C07C225/34 , C09B1/22 , C07C97/24
CPC分类号： C09B1/22
摘要： A process for producing an aminoanthraquinone, which comprises feeding of a nitroanthraquinone and an alkali sulfide continuously into a reaction zone kept at a temperature of from 80.degree. to 140.degree. C., the alkali sulfide being used in an amount of 1.6 or more times the mole number of the nitro group, and withdrawing the reaction product continuously or intermittently from the reaction zone; and an aminoanthraquinone obtained by the above process which is one of the most important intermediates of anthraquinone dyes.
摘要翻译：一种制备氨基蒽醌的方法，其包括将硝基蒽醌和碱金属硫化物连续加入到保持温度为80-140℃的反应区中，碱金属硫化物的用量为1.6或更多倍硝基的摩尔数，连续或间歇地从反应区取出反应产物; 和通过上述方法获得的氨基蒽醌，其是蒽醌染料的最重要的中间体之一。

7. 发明授权

US4345987A Coated electrode and a method of its production 失效
标题翻译：涂层电极及其生产方法
公开(公告)号：US4345987A
公开(公告)日：1982-08-24
申请号：US227688
申请日：1981-01-23
申请人： Akira Fukasawa , Minoru Ueda
发明人： Akira Fukasawa , Minoru Ueda
IPC分类号： C25B11/04 , C25B11/16 , C25C7/02 , H01M4/02
CPC分类号： C25B11/16 , C25B11/0431
摘要： A coated electrode having excellent electric conductivity and resistance against corrosion is obtained by electrodepositing lead dioxide on the surface of an alloy which consists of lead and silver.Prior to electrodepositing lead dioxide, the alloy is anodically oxidized beforehand in a solution of sulfate such that the surface of the alloy is oxidized. This enables the lead dioxide to be electrodeposited even in an acidic electrolyte.
摘要翻译：通过在由铅和银组成的合金的表面上电沉积二氧化铅，可以获得具有优异导电性和耐腐蚀性的涂覆电极。在电沉积二氧化铅之前，合金在硫酸盐溶液中预先阳极氧化，使得合金的表面被氧化。这使得即使在酸性电解质中二氧化铅也能电沉积。

8. 发明授权

US4064035A Lead dioxide electrode 失效
标题翻译：二氧化铅电极
公开(公告)号：US4064035A
公开(公告)日：1977-12-20
申请号：US711498
申请日：1976-08-04
申请人： Akira Fukasawa
发明人： Akira Fukasawa
IPC分类号： C02F1/46 , C25B11/16 , C25C7/02
CPC分类号： C25B11/16
摘要： Disclosed is a novel lead dioxide electrode excellent in shock-resistance, chemical-resistance and electrical conductivity, which has as the electrode proper at least one set of double layer consisting of an .alpha.-lead dioxide layer and a .beta.-lead dioxide layer.
摘要翻译：公开了一种耐冲击性，耐化学性和导电性优异的新型二氧化铅电极，其具有由α二氧化碳层和β-二氧化碳层组成的至少一组双层电极。

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