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    • 9. 发明授权
    • Storage apparatus and position sensitivity setting method
    • 存储设备和位置灵敏度设置方法
    • US06556367B2
    • 2003-04-29
    • US09751096
    • 2000-12-28
    • Eisaku Takahashi
    • Eisaku Takahashi
    • G11B502
    • G11B5/59622
    • High-accuracy position signals are obtained by correcting nonlinear position sensitivities of two phase signals demodulated from two-phase servo information, into linear ones. A position sensitivity adjusting unit detects the signal level at the intersection of position signals N and Q having different phases by a predetermined track pitch which are demodulated from read signals of two-phase servo information buried and recorded in a disk medium and makes an adjustment of the gain of an AGC amplifier so that the intersection signal level coincides with a predetermined level. A sensitivity correcting unit corrects into linear position sensitivities the nonlinear position sensitivities approximated by sine functions or cosine functions relative to the actual track position X of the two position signals N and Q output from the AGC amplifier.
    • 通过将从两相伺服信息解调的两相信号的非线性位置灵敏度校正为线性位置信号来获得高精度位置信号。 位置灵敏度调整单元检测具有不同相位的位置信号N和Q的交点处的信号电平,该预定轨道间距是从埋入并记录在盘介质中的两相伺服信息的读取信号解调的,并进行调整 AGC放大器的增益使得交叉信号电平与预定电平一致。 灵敏度校正单元将相对于从AGC放大器输出的两个位置信号N和Q的实际轨道位置X相对于由正弦函数或余弦函数近似的非线性位置灵敏度校正为线性位置灵敏度。
    • 10. 发明授权
    • Process for optical resolution of 1,2-diol derivatives
    • 1,2-二醇衍生物的光学拆分方法
    • US5493063A
    • 1996-02-20
    • US345463
    • 1994-11-21
    • Eisaku TakahashiTakashi KimuraSatoru Kumazawa
    • Eisaku TakahashiTakashi KimuraSatoru Kumazawa
    • C12P7/62C12P41/00C07C27/00C07C27/02
    • C12P7/62C12P41/004
    • This invention provides a process for producing an optically active 1,2-diol derivative by optical resolution. The optically active 1,2-diol derivative of the formula (I) which is capable of utilizing as an intermediate of fungicidal optically-active azole derivatives can be produced by esterifying a 1,2-diol derivative of the formula (I) as a substrate with a carboxylic acid derivative of the formula (II) as a reagent in the presence of a lipase as a catalyst. ##STR1## wherein R.sup.1 is C1-C5 alkyl group, C3-C7 cycloalkyl group or C1-C5 haloalkyl group, R.sup.2 is C1-C3 alkyl group substituted by a phenyl group which may have one or two halogen atoms and/or C1-C4 alkyl groups, C2-C3 alkenyl group substituted by a phenyl group which may have one or two halogen atoms and/or C1-C4 alkyl groups, or C1-C3 alkyl group substituted by a phenoxy group which may have one or two halogen atoms and/or C1-C4 alkyl groups, R.sup.3 is C1-C10 alkyl group or aryl group, and R.sup.4 is hydrogen atom, C1-C5 alkyl group, C2-C4 alkenyl group or COR.sub.3.
    • 本发明提供了通过光学拆分制备光学活性1,2-二醇衍生物的方法。 能够用作杀真菌的光学活性唑衍生物的中间体的式(I)的光学活性1,2-二醇衍生物可以通过将式(I)的1,2-二醇衍生物酯化为 在作为催化剂的脂肪酶存在下,用式(II)的羧酸衍生物作为试剂的底物。 (I)R 3 COOR 4(II)其中R 1是C 1 -C 5烷基,C 3 -C 7环烷基或C 1 -C 5卤代烷基,R 2是被可以具有一个或两个卤素的苯基取代的C 1 -C 3烷基 原子和/或C 1 -C 4烷基,被可具有一个或两个卤素原子和/或C 1 -C 4烷基的苯基取代的C 2 -C 3烯基或被苯氧基取代的C 1 -C 3烷基, 具有一个或两个卤素原子和/或C 1 -C 4烷基,R 3是C 1 -C 10烷基或芳基,R 4是氢原子,C 1 -C 5烷基,C 2 -C 4烯基或COR 3。