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1. 发明授权

US4600662A Ferrous article layered with ion vapor deposited non-oxidized aluminum 失效
标题翻译：亚铁制品用离子气相沉积非氧化铝分层
公开(公告)号：US4600662A
公开(公告)日：1986-07-15
申请号：US712597
申请日：1985-03-18
申请人： Donald J. Broomfield , Paul C. Briggs , Eric G. Parker , David P. Wagner
发明人： Donald J. Broomfield , Paul C. Briggs , Eric G. Parker , David P. Wagner
IPC分类号： C23C14/12 , B05D3/06 , B05D3/10 , B05D3/12 , B05D7/14 , B05D7/24 , C23C14/32 , C23C14/58 , C23C28/00 , B21C23/32
CPC分类号： C23C28/00 , Y10T428/12556 , Y10T428/12569
摘要： Method and apparatus for the coating of a substrate wherein the following chronologically takes place under vacuum conditions: (i) non-oxidized plating material is deposited on the substrate via ion vapor deposition; and (ii) a coating material is chemically bonded with the non-oxidized plating material. The coating material may comprise a primer, which chemically bonds with the non-oxidized plating material, and a polymer, which impregnates the primer-prepared plating material. Said polymer may also chemically bond with the primer. Alternatively, the coating material may comprise an epoxy which forms an organo-metallic bond with the plating material. In another embodiment of the invention, the coating material may comprise boron trifluoride, which chemically bonds with the non-oxidized plating material, and a polymer, which impregnates the boron trifluoride-prepared plating material. Alternatively, the coating material may comprise calcium, silicon, and oxygen which chemically bonds with the plating material. The coating material may be bifunctional, in that it not only chemically bonds with the plating material but also bonds with a second coating material, yielding a chemically bonded uniform coating with desired results.
摘要翻译：用于涂覆基材的方法和装置，其中以下按时间顺序在真空条件下进行：（i）未氧化的镀覆材料通过离子气相沉积沉积在基材上; 和（ii）涂层材料与未氧化的镀覆材料化学键合。涂料可以包括与非氧化镀覆材料化学键合的底漆和浸渍底漆制备的电镀材料的聚合物。所述聚合物也可以与引物化学键合。或者，涂层材料可以包括与电镀材料形成有机金属键的环氧树脂。在本发明的另一个实施方案中，涂料可以包括与未氧化的镀覆材料化学键合的三氟化硼，以及浸渍三氟化硼制备的电镀材料的聚合物。或者，涂层材料可以包括与电镀材料化学结合的钙，硅和氧。涂层材料可以是双官能的，因为它不仅与电镀材料化学键合，而且与第二涂层材料结合，产生具有期望结果的化学键合的均匀涂层。

2. 发明授权

US4715316A Apparatus for plating and coating 失效
标题翻译：电镀和涂层装置
公开(公告)号：US4715316A
公开(公告)日：1987-12-29
申请号：US850517
申请日：1986-04-11
申请人： Donald J. Broomfield , Paul C. Briggs , Eric G. Parker , David P. Wagner
发明人： Donald J. Broomfield , Paul C. Briggs , Eric G. Parker , David P. Wagner
IPC分类号： C23C28/00 , C23C16/00
CPC分类号： C23C28/00
摘要： Method and apparatus for the coating of a substrate wherein the following chronologically takes place under vacuum conditions: (i) non-oxidized plating material is deposited on the substrate via ion vapor deposition; and (ii) a coating material is chemically bonded with the non-oxidized plating material. The coating material may comprise a primer, which chemically bonds with the non-oxidized plating material, and a polymer, which impregnates the primer-prepared plating material. Said polymer may also chemically bond with the primer. Alternatively, the coating material may comprise an epoxy which forms an organo-metallic bond with the plating material. In another embodiment of the invention, the coating material may comprise boron trifluoride, which chemically bonds with the non-oxidized plating material, and a polymer, which impregnates the boron trifluoride-prepared plating material. Alternatively, the coating material may comprise calcium, silicon, and oxygen which chemically bonds with the plating material. The coating material may be bifunctional, in that it not only chemically bonds with the plating material but also bonds with a second coating material, yielding a chemically bonded uniform coating with desired results.
摘要翻译：用于涂覆基材的方法和装置，其中以下按时间顺序在真空条件下进行：（i）未氧化的镀覆材料通过离子气相沉积沉积在基材上; 和（ii）涂层材料与未氧化的镀覆材料化学键合。涂料可以包括与非氧化镀覆材料化学键合的底漆和浸渍底漆制备的电镀材料的聚合物。所述聚合物也可以与引物化学键合。或者，涂层材料可以包括与电镀材料形成有机金属键的环氧树脂。在本发明的另一个实施方案中，涂料可以包括与未氧化的镀覆材料化学键合的三氟化硼，以及浸渍三氟化硼制备的电镀材料的聚合物。或者，涂层材料可以包括与电镀材料化学结合的钙，硅和氧。涂层材料可以是双官能的，因为它不仅与电镀材料化学键合，而且与第二涂层材料结合，产生具有期望结果的化学键合的均匀涂层。

3. 发明授权

US4788078A Method for plating and coating articles 失效
标题翻译：电镀和涂层方法
公开(公告)号：US4788078A
公开(公告)日：1988-11-29
申请号：US108957
申请日：1987-10-16
申请人： Donald J. Broomfield , Paul C. Briggs , Eric G. Parker , David P. Wagner
发明人： Donald J. Broomfield , Paul C. Briggs , Eric G. Parker , David P. Wagner
IPC分类号： C23C28/00 , B05D3/06
CPC分类号： C23C28/00
摘要： Method and apparatus for the coating of a substrate wherein the following chronologically takes place under vacuum conditions: (i) non-oxidized plating material is deposited on the substrate via ion vapor deposition; and (ii) a coating material is chemically bonded with the non-oxidized plating material. The coating material may comprise a primer, which chemically bonds with the non-oxidized plating material, and a polymer, which impregnates the primer-prepared plating material. Said polymer may also chemically bond with the primer. Alternatively, the coating material may comprise an epoxy which forms an organo-metallic bond with the plating material. In another embodiment of the invention, the coating material may comprise boron trifluoride, which chemcially bonds with the non-oxidized plating material, and a polymer, which impregnates the boron trifluoride-prepared plating material. Alternatively, the coating material may comprise calcium, silicon, and oxygen which chemically bonds with the plating material. The coating material may be bifunctional, in that it not only chemically bonds with the plating material but also bonds with a second coating material, yielding a chemically bonded uniform coating with desired results.
摘要翻译：用于涂覆基材的方法和装置，其中以下按时间顺序在真空条件下进行：（i）未氧化的镀覆材料通过离子气相沉积沉积在基材上; 和（ii）涂层材料与未氧化的镀覆材料化学键合。涂料可以包括与非氧化镀覆材料化学键合的底漆和浸渍底漆制备的电镀材料的聚合物。所述聚合物也可以与引物化学键合。或者，涂层材料可以包括与电镀材料形成有机金属键的环氧树脂。在本发明的另一个实施方案中，涂层材料可以包括与未氧化镀覆材料化学结合的三氟化硼和浸渍三氟化硼制备的电镀材料的聚合物。或者，涂层材料可以包括与电镀材料化学结合的钙，硅和氧。涂层材料可以是双官能的，因为它不仅与电镀材料化学键合，而且与第二涂层材料结合，产生具有期望结果的化学键合的均匀涂层。

4. 发明申请

US20080177004A1 ADHESIVE COMPOSITIONS FOR BONDING AND FILLING LARGE ASSEMBLIES 有权
标题翻译：用于粘合和填充大型组件的粘合剂组合物
公开(公告)号：US20080177004A1
公开(公告)日：2008-07-24
申请号：US12056342
申请日：2008-03-27
申请人： Samuel B. Osae , Paul C. Briggs
发明人： Samuel B. Osae , Paul C. Briggs
IPC分类号： C08L9/00
CPC分类号： C08F283/01 , C08F220/18 , C08F263/00 , C08F279/02 , C08F291/00 , C08L23/0869 , C08L23/286 , C08L33/08 , C08L45/00 , C08L51/00 , C08L55/02 , C08L101/00 , C08L2312/00 , C08L2666/02 , C08L2666/04 , C08L2666/24 , C09J4/06 , C09J133/08 , C09J167/06 , C08F255/00 , C08F287/00 , C08F265/04
摘要： Adhesive composition for bonding and filling large assemblies, including a mixture of about 5 percent to about 75 percent by weight of a thermoplastic polymer, about 0.5 percent to about 35 percent by weight of a polyester resin or vinyl ester resin, and about 20 percent to about 80 percent by weight of an alkyl acrylate or methacrylate monomer.
摘要翻译：用于粘合和填充大组件的粘合剂组合物，包括约5重量％至约75重量％的热塑性聚合物，约0.5重量％至约35重量％的聚酯树脂或乙烯基酯树脂的混合物，和约20重量％约80重量％的丙烯酸烷基酯或甲基丙烯酸烷基酯单体。

5. 发明授权

US5112691A Adhesive for low temperature applications 失效
标题翻译：用于低温应用的粘合剂
公开(公告)号：US5112691A
公开(公告)日：1992-05-12
申请号：US547970
申请日：1990-07-05
申请人： Paul C. Briggs , Donald E. Gosiewski
发明人： Paul C. Briggs , Donald E. Gosiewski
IPC分类号： C09J4/02 , C09J4/06
CPC分类号： C09J4/06 , Y10T428/31507 , Y10T428/31692 , Y10T428/31696 , Y10T428/31931 , Y10T428/31935
摘要： Adhesive compositions are made from methacrylate ester monomers, elastomeric polymers having a Tg below -25.degree. C. and which are soluble in the monomers, core-shell polymers which swell in the monomers but do not dissolve therein, and free radical producing catalysts. These adhesive compositions when used in bonded assemblies exhibit a combination of high adhesive bond impact strength and high bulk tensile elongation.
摘要翻译：粘合剂组合物由甲基丙烯酸酯单体，Tg低于-25℃，可溶于单体的弹性体聚合物，在单体中溶胀但不溶解的核 - 壳聚合物和自由基生成催化剂制成。当粘合组合物使用时，这些粘合剂组合物表现出高的粘合剂粘合冲击强度和高体积拉伸伸长率的组合。

6. 发明授权

US4959405A Acid modified adhesive composition 失效
标题翻译：酸改性粘合剂组合物
公开(公告)号：US4959405A
公开(公告)日：1990-09-25
申请号：US361749
申请日：1989-06-02
申请人： Paul C. Briggs , Donald E. Gosiewski
发明人： Paul C. Briggs , Donald E. Gosiewski
IPC分类号： C08F255/02 , C09J4/06
CPC分类号： C08F255/023 , C09J4/06
摘要： It has been discovered that by adding one or more strong organic carboxylic acids to conventional acrylate and/or methacrylate based adhesive compositions, the bonding characteristics thereof change dramatically.Thermoplastic materials whose bondability is most dramatically enhanced by the compositions of the present invention are nylon and blends of nylon and nylon-like materials with other polymers.Thermoset materials which exhibit dramatically enhanced bondability comprise homogeneous materials such as epoxies, and composite materials such as polyesters, urethanes, and/or epoxies, containing glass, minerals, and the like, which are polar or have hydrogen bonding capability.The present invention thus utilizes acrylate and/or methacrylate based adhesive compositions as a base material. To this base material is added an effective amount of one or more strong organic carboxylic acids, e.g., acids having a relatively high dissociation constant (K.sub.d or K.sub.ld). It has further been discovered that, the addition of water to these acids can increase their effectiveness, apparently through partial or enhanced solubility, which is believed to aid in the dissociation thereof.
摘要翻译：已经发现，通过向常规的丙烯酸酯和/或甲基丙烯酸酯基粘合剂组合物中加入一种或多种强有机羧酸，其粘合特性显着变化。通过本发明的组合物最能显着提高其粘合性的热塑性材料是尼龙和尼龙和尼龙类材料与其它聚合物的共混物。显示出显着增强的粘合性的热固性材料包括均匀的材料，例如环氧树脂，以及包含玻璃，矿物等的具有极性或具有氢键能力的复合材料如聚酯，聚氨酯和/或环氧树脂。因此，本发明利用基于丙烯酸酯和/或甲基丙烯酸酯的粘合剂组合物作为基材。向该基础材料中加入有效量的一种或多种强有机羧酸，例如具有较高解离常数的酸（Kdor Kld）。进一步发现，向这些酸中加入水可以提高它们的有效性，显然是通过部分或增强的溶解度，这被认为有助于其解离。

7. 发明授权

US4714730A Acid modified adhesive compositions 失效
标题翻译：酸改性粘合剂组合物
公开(公告)号：US4714730A
公开(公告)日：1987-12-22
申请号：US870710
申请日：1986-06-04
申请人： Paul C. Briggs , Donald E. Gosiewski
发明人： Paul C. Briggs , Donald E. Gosiewski
IPC分类号： B29C65/52 , B32B7/12 , C08F2/44 , C08F20/12 , C08F255/02 , C08L23/34 , C08L51/00 , C09J4/02 , C09J4/06 , C08K5/09
CPC分类号： C09J4/06 , C08F255/023 , B29C66/7392 , B29C66/7394
摘要： It has been discovered that by adding one or more strong organic carboxylic acids to conventional acrylate and/or methacrylate based adhesive compositions, the bonding characteristics thereof change dramatically.Thermoplastic materials whose bondability is most dramatically enhanced by the compositions of the present invention are nylon and blends of nylon and nylon-like materials with other polymers.Thermoset materials which exhibit dramatically enhanced bondability comprise homogeneous materials such as epoxies, and composite materials such as polyesters, urethanes, and/or epoxies, containing glass, minerals, and the like, which are polar or have hydrogen bonding capability.The present invention thus utilizes acrylate and/or methacrylate based adhesive compositions as a base material. To this base material is added an effective amount of one or more strong organic carboxylic acids, e.g., acids having a relatively high dissociation constant (K.sub.d or K.sub.1d). It has further been discovered that, the addition of water to these acids can increase their effectiveness, apparently through partial or enhanced solubility, which is believed to aid in the dissociation thereof.
摘要翻译：已经发现，通过向常规的丙烯酸酯和/或甲基丙烯酸酯基粘合剂组合物中加入一种或多种强有机羧酸，其粘合特性显着变化。通过本发明的组合物最能显着提高其粘合性的热塑性材料是尼龙和尼龙和尼龙类材料与其它聚合物的共混物。显示出显着增强的粘合性的热固性材料包括均匀的材料，例如环氧树脂，以及包含玻璃，矿物等的具有极性或具有氢键能力的复合材料如聚酯，聚氨酯和/或环氧树脂。因此，本发明利用基于丙烯酸酯和/或甲基丙烯酸酯的粘合剂组合物作为基材。向该基材中加入有效量的一种或多种强有机羧酸，例如具有较高解离常数（Kd或K1d）的酸。进一步发现，向这些酸中加入水可以提高它们的有效性，显然是通过部分或增强的溶解度，这被认为有助于其解离。

8. 发明授权

US07816453B2 Adhesive compositions for bonding and filling large assemblies 有权
标题翻译：用于粘合和填充大型组件的粘合剂组合物
公开(公告)号：US07816453B2
公开(公告)日：2010-10-19
申请号：US12056342
申请日：2008-03-27
申请人： Samuel B. Osae , Paul C. Briggs
发明人： Samuel B. Osae , Paul C. Briggs
IPC分类号： C08L23/00 , C08L23/04 , C08L27/04 , C08L33/00 , C08L33/02 , C08L33/14 , C08L41/00 , C08L45/00 , C08K5/00
CPC分类号： C08F283/01 , C08F220/18 , C08F263/00 , C08F279/02 , C08F291/00 , C08L23/0869 , C08L23/286 , C08L33/08 , C08L45/00 , C08L51/00 , C08L55/02 , C08L101/00 , C08L2312/00 , C08L2666/02 , C08L2666/04 , C08L2666/24 , C09J4/06 , C09J133/08 , C09J167/06 , C08F255/00 , C08F287/00 , C08F265/04
摘要： Adhesive composition for bonding and filling large assemblies, including a mixture of about 5 percent to about 75 percent by weight of a thermoplastic polymer, about 0.5 percent to about 35 percent by weight of a polyester resin or vinyl ester resin, and about 20 percent to about 80 percent by weight of an alkyl acrylate or methacrylate monomer.
摘要翻译：用于粘合和填充大组件的粘合剂组合物，包括约5重量％至约75重量％的热塑性聚合物，约0.5重量％至约35重量％的聚酯树脂或乙烯基酯树脂的混合物，和约20重量％约80重量％的丙烯酸烷基酯或甲基丙烯酸烷基酯单体。

9. 发明授权

US5206288A Adhesive for low temperature applications 失效
标题翻译：用于低温应用的粘合剂
公开(公告)号：US5206288A
公开(公告)日：1993-04-27
申请号：US547969
申请日：1990-07-05
申请人： Donald E. Gosiewski , Paul C. Briggs
发明人： Donald E. Gosiewski , Paul C. Briggs
IPC分类号： C09J4/02 , C09J4/06 , C09J111/00 , C09J151/00
CPC分类号： C09J4/06 , Y10S525/902
摘要： Adhesive compositions are made from methacrylate ester monomers, elastomeric polymers having a Tg below -25.degree. C. and which are soluble in the monomers, core-shell polymers which swell in the monomers but do not dissolve therein, and free radical producing catalysts. These adhesive compositions when used in bonded assemblies exhibit a combination of high adhesive bond impact strength and high bulk tensile elongation.
摘要翻译：粘合剂组合物由甲基丙烯酸酯单体，Tg低于-25℃，可溶于单体的弹性体聚合物，在单体中溶胀但不溶解的核 - 壳聚合物和自由基生成催化剂制成。当粘合组合物使用时，这些粘合剂组合物表现出高的粘合剂粘合冲击强度和高体积拉伸伸长率的组合。

10. 发明授权

US4773957A Bonding method employing novel methacrylate based adhesive compositions 失效
标题翻译：采用新型甲基丙烯酸酯粘合剂组合物的粘合方法
公开(公告)号：US4773957A
公开(公告)日：1988-09-27
申请号：US53586
申请日：1987-05-19
申请人： Paul C. Briggs
发明人： Paul C. Briggs
IPC分类号： C09J4/06 , B32B7/00
CPC分类号： C09J4/06
摘要： A novel methacrylate-based composition is disclosed. The composition is preferably used as an adhesive. The composition comprises an acrylate-based or methacrylate-based ester monomer, a catalyst, a chlorinated or chlorosulfonated polyethylene polymer resin and a graft co-polymer resin. The chlorinated polyethylene polymer resin used includes organic sulfonyl chloride. The composition preferably further includes an acrylate-based or methacrylate-based acid monomer, and a catalyst activator. A preferred chlorosulfonated polyethylene polymer resin contains about 43 weight percent chlorine, about 1.1 weight percent sulfur, and about 34 millimoles sulfonyl chloride moiety per 100 grams thereof. Preferred graft co-polymer resins are ABS, MBS, MABS, ASA, all-acrylic, SA EPDM and MAS. More-preferred graft co-polymer resins are MABS, ASA, all-acrylic and MBS. Most-preferred graft co-polymer resins are MABS and ASA. A preferred methacrylate-based acid monomer is methacrylic acid. Preferred methacrylate-based ester monomers are methyl methacrylate, ethyl methacrylate, butyl methacrylate, cyclohexyl methacrylate, 2-ethylhexyl methacrylate and tetrahydrofurfuryl methacrylate. More-preferred methacrylate-based ester monomers are methyl methacrylate and ethyl methacrylate. A most-preferred methacrylate-based ester monomer is methyl methacrylate. The composition possesses enhanced compression shear strength, lap shear strength, peel strength and impact strength adhesive physical properties.
摘要翻译：公开了一种新的基于甲基丙烯酸酯的组合物。组合物优选用作粘合剂。组合物包含基于丙烯酸酯或甲基丙烯酸酯的酯单体，催化剂，氯化或氯磺化的聚乙烯聚合物树脂和接枝共聚物树脂。使用的氯化聚乙烯聚合物树脂包括有机磺酰氯。组合物优选还包括基于丙烯酸酯或甲基丙烯酸酯的酸单体和催化剂活化剂。优选的氯磺化聚乙烯聚合物树脂含有约43重量％的氯，约1.1重量％的硫和约34毫摩尔磺酰氯部分/ 100克。优选的接枝共聚物树脂是ABS，MBS，MABS，ASA，全丙烯酸，SA EPDM和MAS。更优选的接枝共聚物树脂是MABS，ASA，全丙烯酸和MBS。最优选的接枝共聚物树脂是MABS和ASA。优选的基于甲基丙烯酸酯的酸单体是甲基丙烯酸。优选的基于甲基丙烯酸酯的酯单体是甲基丙烯酸甲酯，甲基丙烯酸乙酯，甲基丙烯酸丁酯，甲基丙烯酸环己酯，甲基丙烯酸2-乙基己酯和甲基丙烯酸四氢糠酯。更优选的基于甲基丙烯酸酯的酯单体是甲基丙烯酸甲酯和甲基丙烯酸乙酯。最优选的甲基丙烯酸酯单体是甲基丙烯酸甲酯。该组合物具有增强的压缩剪切强度，搭接剪切强度，剥离强度和冲击强度粘合剂物理性能。

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