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1. 发明授权

US4521404A Polymeric hair preparation 失效
标题翻译：聚合头发准备
公开(公告)号：US4521404A
公开(公告)日：1985-06-04
申请号：US440648
申请日：1982-11-10
申请人： Donald H. Lorenz , Edward J. Murphy , John M. Rutherford, Jr.
发明人： Donald H. Lorenz , Edward J. Murphy , John M. Rutherford, Jr.
IPC分类号： C08F26/00 , A61K8/00 , A61K8/20 , A61K8/22 , A61K8/37 , A61K8/40 , A61K8/42 , A61K8/81 , A61Q5/00 , A61Q5/02 , A61Q5/06 , A61Q5/12 , C08F26/10 , C08F226/06 , A61K7/09 , A45D7/00 , C08F226/10
CPC分类号： A61Q5/12 , A61K8/8182 , A61Q5/02 , A61Q5/06 , C08F226/06 , A61K2800/5426
摘要： The present invention relates to a polymeric hair conditioning composition of vinyl pyrrolidone monomer, an ammonium derivative monomer and a substantially major amount, based on said monomers, of vinyl caprolactam said polymeric composition optionally containing a minor amount of stearyl methacrylate. Suitable ammonium derivative monomers include dimethylamino propyl methacrylamide, dimethyl diallyl ammonium chloride and a dialkylamino alkyl methacrylate, such as for example dimethylamino ethyl methacrylate.
摘要翻译：本发明涉及基于所述单体的乙烯基吡咯烷酮单体，铵衍生物单体和基本上主要量的乙烯基己内酰胺的聚合物毛发调理组合物，所述聚合物组合物任选地含有少量的甲基丙烯酸硬脂基酯。合适的铵衍生物单体包括二甲基氨基丙基甲基丙烯酰胺，二甲基二烯丙基氯化铵和二烷基氨基烷基甲基丙烯酸酯，例如甲基丙烯酸二甲基氨基乙酯。

2. 发明申请

US20080241535A1 D1364 BT SECONDARY COATINGS ON OPTICAL FIBER 审中-公开
标题翻译： D1364 BT光纤二次涂层
公开(公告)号：US20080241535A1
公开(公告)日：2008-10-02
申请号：US11955838
申请日：2007-12-13
申请人： Wendell Wayne CATTRON , Steven R. Schmid , Edward J. Murphy , John M. Zimmerman , Anthony Joseph Tortorello
发明人： Wendell Wayne CATTRON , Steven R. Schmid , Edward J. Murphy , John M. Zimmerman , Anthony Joseph Tortorello
IPC分类号： B32B17/02 , C08L75/04 , B32B17/10 , C03C25/34
CPC分类号： G02B1/12 , C03C25/1065 , C08G18/672 , C08G18/724 , C09D163/00 , C09D175/14 , C09D175/16 , Y10T428/2938 , Y10T428/2964 , C08G18/48
摘要： The invention relates to a Radiation Curable Secondary Coating composition for use on an Optical Fiber. The Radiation Curable Secondary Coating composition is a urethane-free Alpha Oligomer prepared by reaction of the following: (a) an acrylate compound selected from an alcohol-containing acrylate or alcohol-containing methacrylate compound, (b) an anhydride compound, (c) an epoxy-containing compound, (d) optionally an extender compound, and (e) optionally a catalyst. The invention also relates to a coated wire and to a coated optical fiber.
摘要翻译：本发明涉及一种用于光纤的辐射固化二次涂料组合物。辐射固化二次涂料组合物是通过以下反应制备的不含氨基甲酸酯的α-低聚物：（a）选自含醇丙烯酸酯或含醇甲基丙烯酸酯化合物的丙烯酸酯化合物，（b）酸酐化合物，（c）含环氧基的化合物，（d）任选的增量化合物，和（e）任选的催化剂。本发明还涉及涂覆线和涂覆光纤。

3. 发明申请

US20080226912A1 D1365 BJ RADIATION CURABLE PRIMARY COATING FOR OPTICAL FIBER 审中-公开
标题翻译： D1365 BJ辐射可固化主要用于光纤的涂层
公开(公告)号：US20080226912A1
公开(公告)日：2008-09-18
申请号：US11955547
申请日：2007-12-13
申请人： Tyson Dean NORLIN , Steven R. Schmid , Edward J. Murphy , John M. Zimmerman , Anthony Joseph Tortorello
发明人： Tyson Dean NORLIN , Steven R. Schmid , Edward J. Murphy , John M. Zimmerman , Anthony Joseph Tortorello
IPC分类号： B32B17/02 , C08L75/00 , B32B17/10 , C03C25/34
CPC分类号： C09D175/08 , C03C25/1065 , C03C25/326 , C08G18/672 , C09D5/002 , C09D175/16 , G02B6/02395 , Y10T428/2964 , C08G18/48
摘要： Radiation curable coatings for use as a Primary Coating for optical fibers, optical fibers coated with said coatings and methods for the preparation of coated optical fibers. The present invention provides a radiation curable Primary Coating composition comprising: an oligomer; first diluent monomer; a second diluent monomer; a third diluent monomer; a first light stabilizer; a first photoinitiator; a second photoinitiator; an antioxidant; a second light stabilizer; and an adhesion promoter; wherein said oligomer is the reaction product of hydroxyl-containing acrylate; an isocyanate; a polyether polyol; a polymerization inhibitor; a catalyst; and a diluent; wherein said oligomer has a number average molecular weight of from at least about 4000 g/mol to less than or equal to about 15,000 g/mol; and wherein said catalyst is selected from the group consisting of copper naphthenate; cobalt naphthenate; zinc naphthenate; triethylamine; triethylenediamine; 2-methyltriethyleneamine; dibutyl tin dilaurate; metal carboxylates, including, but not limited to: organobismuth catalysts such as bismuth neodecanoate; zinc neodecanoate; zirconium neodecanoate; zinc 2-ethylhexanoate; sulfonic acids, including but not limited to dodecylbenzene sulfonic acid, methane sulfonic acid; amino or organo-base catalysts, including, but not limited to, 1,2-dimethylimidazole and diazabicyclooctane; triphenyl phosphine; alkoxides of zirconium and titanium, including, but not limited to Zirconium butoxide and Titanium butoxide; and Ionic liquid phosphonium salts; and tetradecyl(trihexyl) phosphonium chloride; and wherein a cured film of said radiation curable Primary Coating composition has a peak tan □ Tg of from about −25° C. to about −55° C.; and a modulus of from about 0.85 MPa to about 1.10 MPa.
摘要翻译：用作光纤的主要涂层的辐射固化涂层，涂覆有所述涂层的光纤以及用于制备涂覆的光纤的方法。本发明提供了一种可辐射固化的初级涂料组合物，其包含：低聚物; 第一稀释剂单体; 第二稀释剂单体; 第三稀释剂单体; 第一光稳定剂; 第一种光引发剂; 第二光引发剂; 抗氧化剂第二种光稳定剂; 和粘合促进剂; 其中所述低聚物是含羟基的丙烯酸酯的反应产物; 异氰酸酯; 聚醚多元醇; 阻聚剂; 催化剂和稀释剂; 其中所述低聚物的数均分子量为至少约4000g / mol至小于或等于约15,000g / mol; 并且其中所述催化剂选自环烷酸铜; 环烷酸钴; 环烷酸锌; 三乙胺三亚乙基二胺 2-甲基三亚乙基胺; 二月桂酸二丁基锡; 金属羧酸盐，包括但不限于：有机铋催化剂如新戊酸铋; 新癸酸锌; 新癸酸锆; 2-乙基己酸锌; 磺酸，包括但不限于十二烷基苯磺酸，甲磺酸; 氨基或有机碱催化剂，包括但不限于1,2-二甲基咪唑和二氮杂双环辛烷; 三苯基膦锆和钛的醇盐包括但不限于丁氧基锆和丁醇钛; 和离子液体鏻盐; 和十四烷基（三己基）鏻氯化物; 并且其中所述可辐射固化的初级涂层组合物的固化膜具有约-25℃至约-55℃的峰值tanδTg。和约0.85MPa至约1.10MPa的模量。

4. 发明授权

US06107361A Solvent-free, radiation-curable, optical glass fiber coating composition and solvent-free method for making a solvent-free, radiation-curable, optical glass fiber coating composition 失效
标题翻译：无溶剂，可辐射固化，光学玻璃纤维涂料组合物和无溶剂方法制备无溶剂，可辐射固化的光学玻璃纤维涂料组合物
公开(公告)号：US06107361A
公开(公告)日：2000-08-22
申请号：US168290
申请日：1998-10-08
申请人： Anthony J. Tortorello , Edward J. Murphy
发明人： Anthony J. Tortorello , Edward J. Murphy
IPC分类号： C03C25/24 , C03C25/10 , C08F2/06 , C08F2/50 , C08F8/30 , C08F290/12 , C08G18/62 , C08G18/81 , C09D4/06 , G03F7/027 , G03F7/038 , C08G18/10 , C08G18/12
CPC分类号： G03F7/0388 , C03C25/1055 , C03C25/106 , C03C25/1065 , C08G18/6229 , C08G18/8158 , G03F7/027 , Y10T428/2938
摘要： The invention relates to a solvent-free radiation curable, optical glass fiber coating composition containing:a) a urethane oligomer having a functional group capable of polymerization in the presence of actinic radiation, with an average functionality of at least about 1.2, having a vinyl addition polymer as backbone.b) a urethane compound having a functional group capable of polymerization in the presence of actinic radiation, with an average functionality of at least about 1, containing an organic moiety having about 5 or more carbon atoms as backbone.c) a reactive diluent.Furthermore, the invention relates to a solvent-free method for producing a solvent-free, radiation curable urethane oligomer composition.
摘要翻译：本发明涉及无溶剂的可辐射固化的光学玻璃纤维涂料组合物，其含有：a）具有能在光化辐射存在下能够聚合的官能团的氨基甲酸酯低聚物，平均官能度至少为约1.2，具有乙烯基加成聚合物作为骨架。 b）具有能够在光化辐射存在下能够聚合的官能团的氨基甲酸酯化合物，其平均官能度为至少约1，其含有具有约5个或更多个碳原子的有机部分作为主链。 c）反应性稀释剂。此外，本发明涉及一种无溶剂的无辐射固化型氨基甲酸酯低聚物组合物的制造方法。

5. 发明授权

US4532021A Adherent ultraviolet cured coatings 失效
标题翻译：附着紫外线固化涂层
公开(公告)号：US4532021A
公开(公告)日：1985-07-30
申请号：US606527
申请日：1984-05-07
申请人： Edward J. Murphy , Ronald J. Lewarchik , Jeffrey W. Thompson
发明人： Edward J. Murphy , Ronald J. Lewarchik , Jeffrey W. Thompson
IPC分类号： C09D4/06 , C08J3/28 , C08L31/08
CPC分类号： C09D4/06
摘要： Ultraviolet-curable liquid coating compositions are disclosed in which improved adhesion to metal and plastic surfaces is obtained. This improvement is obtained by using, in admixture: (1) from 10% to about 60% of total resin solids of an organic solvent-soluble solution copolymer of monoethylenically unsaturated monomers including from 2.5% to 10% of tertiary amine monomer which is an aminoalkyl ester or amide of an alpha, beta-monoethylenic monocarboxylic acid in which the alkyl group contains 2-4 carbon atoms; and (2) from 40% to 90% of total resin solids of radiation-curable ethylenically unsaturated liquid. The coating composition includes photoinitiators and/or photosensitizers rendering the composition sensitive to ultraviolet light, and the components are present in solution in at least about 10% of inert volatile organic solvent.
摘要翻译：公开了可获得改善的对金属和塑料表面的粘附性的紫外线固化液体涂料组合物。这种改进通过以下方式获得：（1）总树脂固体的10％至约60％的单烯属不饱和单体的有机溶剂可溶性溶液共聚物，包括2.5％至10％的叔胺单体，其为其中烷基含有2-4个碳原子的α，β-单烯基单羧酸的氨基烷基酯或酰胺; 和（2）可辐射固化的烯属不饱和液体的总树脂固体的40％至90％。涂料组合物包括光引发剂和/或光敏剂，使组合物对紫外光敏感，并且组分在溶液中存在于至少约10％的惰性挥发性有机溶剂中。

6. 发明授权

US4310653A Production of monomeric etherified bisphenol-formaldehyde condensates 失效
标题翻译：单体醚化双酚 - 甲醛缩合物的生产
公开(公告)号：US4310653A
公开(公告)日：1982-01-12
申请号：US195110
申请日：1980-10-08
申请人： John J. Krajewski , Edward J. Murphy
发明人： John J. Krajewski , Edward J. Murphy
IPC分类号： C08G8/36 , C09D161/14 , C08G2/34 , C08G8/20
CPC分类号： C09D161/14 , C08G8/36 , Y10S524/901
摘要： A method of producing essentially monomeric etherified formaldehyde condensates with a bisphenol having a plurality of formaldehyde-reactive sites is disclosed in which the bisphenol is reacted with at least about 2 moles of formaldehyde per mole of bisphenol in solution in etherifying alcohol in the presence of an insoluble strong acid cation exchange resin. The reaction is carried out at a reaction temperature of from about 30.degree. C. to about 100.degree. C. to simultaneously provide the desired methylolation and etherification without introducing soluble ionic contaminants.
摘要翻译：公开了一种用具有多个甲醛反应性位点的双酚生产基本上单体醚化的甲醛缩合物的方法，其中在醚化醇存在下，双酚与溶剂中每摩尔双酚的至少约2摩尔甲醛反应不溶性强酸阳离子交换树脂。反应在约30℃至约100℃的反应温度下进行，以同时提供所需的羟甲基化和醚化，而不引入可溶性离子污染物。

7. 发明申请

US20080226909A1 D1381 SUPERCOATINGS FOR OPTICAL FIBER 有权
标题翻译： D1381光纤超滤器
公开(公告)号：US20080226909A1
公开(公告)日：2008-09-18
申请号：US11955541
申请日：2007-12-13
申请人： Steven R. Schmid , Petrus Jacobus Hubertus Niels , Paulus Antonius Maria Steeman , Xiaosong Wu , Wendell Wayne Cattron , Tyson Dean Norlin , Edward J. Murphy , John M. Zimmerman , Anthony Joseph Tortorello
发明人： Steven R. Schmid , Petrus Jacobus Hubertus Niels , Paulus Antonius Maria Steeman , Xiaosong Wu , Wendell Wayne Cattron , Tyson Dean Norlin , Edward J. Murphy , John M. Zimmerman , Anthony Joseph Tortorello
IPC分类号： B32B1/08 , B05D3/06
CPC分类号： G02B1/14 , C03C25/1065 , C08G18/672 , C08G18/724 , C09D5/002 , C09D175/16 , G02B1/10 , G02B6/02395 , Y10T428/24942 , Y10T428/2933 , Y10T428/2942 , Y10T428/2947 , C08G18/48
摘要： The invention provides an optical fiber coated with a Supercoating, wherein the Supercoating comprises at least two layers, wherein the first layer is a Primary Coating that is in contact with the outer surface of the optical fiber and the second layer is a Secondary Coating in contact with the outer surface of the Primary Coating, wherein the cured Primary Coating on the optical fiber has the following properties after initial cure and after one month aging at 85° C. and 85% relative humidity: A) a % RAU of from about 84% to about 99%;B) an in-situ modulus of between about 0.15 MPa and about 0.60 MPa; and C) a Tube Tg, of from about −25° C. to about −55° C.; wherein the cured Secondary Coating on the optical fiber has the following properties after initial cure and after one month aging at 85° C. and 85% relative humidity: A) a % RAU of from about 80% to about 98%; B) an in-situ modulus of between about 0.60 GPa and about 1.90 GPa; and C) a Tube Tg, of from about 50° C. to about 80° C.
摘要翻译：本发明提供涂覆有超涂层的光纤，其中超涂层包括至少两层，其中第一层是与光纤的外表面接触的主涂层，第二层是接触的第二涂层其中主要涂层的外表面，其中光纤上的固化的一次涂层在初始固化后和在85℃和85％相对湿度下老化一个月后具有以下性质：A）约84％的％RAU，至约99％; B）约0.15MPa至约0.60MPa的原位模量; 和C）管Tg，约-25℃至约-55℃; 其中光纤上的固化的二次涂层在初始固化之后和在85℃和85％相对湿度下老化一个月后具有以下性能：A）约80％至约98％的％RAU; B）原位模量在约0.60GPa和约1.90GPa之间; 和C）管Tg，为约50℃至约80℃

8. 发明授权

US06197422B1 Ribbon assemblies and radiation-curable ink compositions for use in forming the ribbon assemblies 失效
标题翻译：色带组件和可用于形成色带组件的可辐射固化油墨组合物
公开(公告)号：US06197422B1
公开(公告)日：2001-03-06
申请号：US09158134
申请日：1998-09-22
申请人： Edward J. Murphy , Edward P. Zahora , Johannes C. van den Burg
发明人： Edward J. Murphy , Edward P. Zahora , Johannes C. van den Burg
IPC分类号： D02G300
CPC分类号： C03C25/106 , C03C25/1065 , C08F290/064 , C08F290/067 , G02B6/4482 , Y10T428/2933 , Y10T428/2938 , Y10T428/2964
摘要： Provided is a ribbon assembly having the functional capability of providing break-out of ink coated or colored outer primary coated optical glass fibers from the ribbon assembly. The ink coating or colored outer primary coating is formulated from a benzophenone compound and at least about 1 wt. % of a homolytic photoinitiator to provide a level of adhesion between the ink coating or colored outer primary coating and matrix material which is less than the level of adhesion between the ink coating or colored outer primary coating and an adjacent underlying coating. Also provided are ink coating and colored outer primary coating compositions adapted to form ink coatings and colored outer primary coatings suitable for use on optical glass fibers contained in a ribbon assembly.
摘要翻译：提供了一种带状组件，其具有从带状组件提供油墨涂覆或着色的外部初级涂覆光学玻璃纤维的功能性能。油墨涂料或着色的外部初级涂料由二苯甲酮化合物配制，并且至少约1wt。％的均相光引发剂，以提供油墨涂层或着色的外部初级涂层和基质材料之间的粘附水平，其小于油墨涂层或着色外初级涂层和相邻下层涂层之间的粘合程度。还提供了适用于形成油墨涂层和适用于包含在色带组件中的光学玻璃纤维上的着色的外部主要涂层的着色的外部初级涂料组合物的油墨涂料和着色的外部初级涂料组合物。

9. 发明授权

US6085010A Optical glass fiber ribbon assemblies and radiation-curable compositions for use in forming ribbon assemblies 失效
标题翻译：用于形成带组件的光学玻璃纤维带组件和可辐射固化组合物
公开(公告)号：US6085010A
公开(公告)日：2000-07-04
申请号：US129234
申请日：1998-08-05
申请人： Edward P. Zahora , Edward J. Murphy , David M. Szum , John T. Vandeberg , Gerry K. Noren , Eva Montgomery
发明人： Edward P. Zahora , Edward J. Murphy , David M. Szum , John T. Vandeberg , Gerry K. Noren , Eva Montgomery
IPC分类号： C08G18/67 , G02B6/44
CPC分类号： C08G18/672 , G02B6/4482 , Y10T428/2933 , Y10T428/2947
摘要： Provided is a ribbon assembly having the functional capability of providing mid-span access without the use of additives, monomers or oligomers containing fluorine or silicone. The ribbon assembly is formulated from an oligomer which reduces the surface energy of the ink coating and/or the matrix material.
摘要翻译：提供了具有提供中跨通道的功能能力的带组件，而不使用添加剂，含氟或硅酮的单体或低聚物。色带组件由低聚物配制，其降低了油墨涂层和/或基质材料的表面能。

10. 发明授权

US5847021A Solvent-free, radiation-curable, optical glass fiber coating composition and solvent-free method for making a solvent-free, radiation-curable, optical glass fiber coating composition 失效
公开(公告)号：US5847021A
公开(公告)日：1998-12-08
申请号：US740725
申请日：1996-11-01
申请人： Anthony J. Tortorello , Edward J. Murphy
发明人： Anthony J. Tortorello , Edward J. Murphy
IPC分类号： C03C25/24 , C03C25/10 , C08F2/06 , C08F2/50 , C08F8/30 , C08F290/12 , C08G18/62 , C08G18/81 , C09D4/06 , G03F7/027 , G03F7/038 , C08L75/06 , C08L75/08 , C08L75/16
CPC分类号： G03F7/0388 , C03C25/1055 , C03C25/106 , C03C25/1065 , C08G18/6229 , C08G18/8158 , G03F7/027 , Y10T428/2938
摘要： The invention relates to a solvent-free radiation curable, optical glass fiber coating composition containing: a) a urethane oligomer having a functional group capable of polymerization in the presence of actinic radiation, with an average functionality of at least about 1.2, having a vinyl addition polymer as backbone. b) a urethane compound having a functional group capable of polymerization in the presence of actinic radiation, with an average functionality of at least about 1, containing an organic moiety having about 5 or more carbon atoms as backbone. c) a reactive diluent. Furthermore, the invention relates to a solvent-free method for producing a solvent-free, radiation curable urethane oligomer composition.

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