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1. 发明申请

US20080226909A1 D1381 SUPERCOATINGS FOR OPTICAL FIBER 有权
标题翻译： D1381光纤超滤器
公开(公告)号：US20080226909A1
公开(公告)日：2008-09-18
申请号：US11955541
申请日：2007-12-13
申请人： Steven R. Schmid , Petrus Jacobus Hubertus Niels , Paulus Antonius Maria Steeman , Xiaosong Wu , Wendell Wayne Cattron , Tyson Dean Norlin , Edward J. Murphy , John M. Zimmerman , Anthony Joseph Tortorello
发明人： Steven R. Schmid , Petrus Jacobus Hubertus Niels , Paulus Antonius Maria Steeman , Xiaosong Wu , Wendell Wayne Cattron , Tyson Dean Norlin , Edward J. Murphy , John M. Zimmerman , Anthony Joseph Tortorello
IPC分类号： B32B1/08 , B05D3/06
CPC分类号： G02B1/14 , C03C25/1065 , C08G18/672 , C08G18/724 , C09D5/002 , C09D175/16 , G02B1/10 , G02B6/02395 , Y10T428/24942 , Y10T428/2933 , Y10T428/2942 , Y10T428/2947 , C08G18/48
摘要： The invention provides an optical fiber coated with a Supercoating, wherein the Supercoating comprises at least two layers, wherein the first layer is a Primary Coating that is in contact with the outer surface of the optical fiber and the second layer is a Secondary Coating in contact with the outer surface of the Primary Coating, wherein the cured Primary Coating on the optical fiber has the following properties after initial cure and after one month aging at 85° C. and 85% relative humidity: A) a % RAU of from about 84% to about 99%;B) an in-situ modulus of between about 0.15 MPa and about 0.60 MPa; and C) a Tube Tg, of from about −25° C. to about −55° C.; wherein the cured Secondary Coating on the optical fiber has the following properties after initial cure and after one month aging at 85° C. and 85% relative humidity: A) a % RAU of from about 80% to about 98%; B) an in-situ modulus of between about 0.60 GPa and about 1.90 GPa; and C) a Tube Tg, of from about 50° C. to about 80° C.
摘要翻译：本发明提供涂覆有超涂层的光纤，其中超涂层包括至少两层，其中第一层是与光纤的外表面接触的主涂层，第二层是接触的第二涂层其中主要涂层的外表面，其中光纤上的固化的一次涂层在初始固化后和在85℃和85％相对湿度下老化一个月后具有以下性质：A）约84％的％RAU，至约99％; B）约0.15MPa至约0.60MPa的原位模量; 和C）管Tg，约-25℃至约-55℃; 其中光纤上的固化的二次涂层在初始固化之后和在85℃和85％相对湿度下老化一个月后具有以下性能：A）约80％至约98％的％RAU; B）原位模量在约0.60GPa和约1.90GPa之间; 和C）管Tg，为约50℃至约80℃

2. 发明授权

US08426020B2 D1381 supercoatings for optical fiber 有权
标题翻译： D1381超级涂层光纤
公开(公告)号：US08426020B2
公开(公告)日：2013-04-23
申请号：US11955541
申请日：2007-12-13
申请人： Steven R. Schmid , Petrus Jacobus Hubertus Niels , Paulus Antonius Maria Steeman , Xiaosong Wu , Wendell Wayne Cattron , Tyson Dean Norlin , Edward J. Murphy , John M. Zimmerman , Anthony Joseph Tortorello
发明人： Steven R. Schmid , Petrus Jacobus Hubertus Niels , Paulus Antonius Maria Steeman , Xiaosong Wu , Wendell Wayne Cattron , Tyson Dean Norlin , Edward J. Murphy , John M. Zimmerman , Anthony Joseph Tortorello
IPC分类号： C08F2/50 , B05D5/06 , D02G3/00 , G02B6/00
CPC分类号： G02B1/14 , C03C25/1065 , C08G18/672 , C08G18/724 , C09D5/002 , C09D175/16 , G02B1/10 , G02B6/02395 , Y10T428/24942 , Y10T428/2933 , Y10T428/2942 , Y10T428/2947 , C08G18/48
摘要： The invention provides an optical fiber coated with a Supercoating, wherein the Supercoating comprises at least two layers, wherein the first layer is a Primary Coating that is in contact with the outer surface of the optical fiber and the second layer is a Secondary Coating in contact with the outer surface of the Primary Coating, wherein the cured Primary Coating on the optical fiber has the following properties after initial cure and after one month aging at 85° C. and 85% relative humidity: A) a % RAU of from about 84% to about 99%;B) an in-situ modulus of between about 0.15 MPa and about 0.60 MPa; andC) a Tube Tg, of from about −25° C. to about −55° C.; wherein the cured Secondary Coating on the optical fiber has the following properties after initial cure and after one month aging at 85° C. and 85% relative humidity: A) a % RAU of from about 80% to about 98%; B) an in-situ modulus of between about 0.60 GPa and about 1.90 GPa; and C) a Tube Tg, of from about 50° C. to about 80° C.
摘要翻译：本发明提供涂覆有超涂层的光纤，其中超涂层包括至少两层，其中第一层是与光纤的外表面接触的主涂层，第二层是接触的第二涂层其中主要涂层的外表面，其中光纤上的固化的一次涂层在初始固化后和在85℃和85％相对湿度下老化一个月后具有以下性质：A）约84％的％RAU，至约99％; B）约0.15MPa至约0.60MPa的原位模量; 和C）管Tg，约-25℃至约-55℃; 其中光纤上的固化的二次涂层在初始固化之后和在85℃和85％相对湿度下老化一个月后具有以下性能：A）约80％至约98％的％RAU; B）原位模量在约0.60GPa和约1.90GPa之间; 和C）管Tg，为约50℃至约80℃

3. 发明申请

US20080226914A1 D1368 CR RADIATION CURABLE PRIMARY COATING FOR OPTICAL FIBER 审中-公开
标题翻译： D1368 CR辐射可固化主要用于光纤的涂层
公开(公告)号：US20080226914A1
公开(公告)日：2008-09-18
申请号：US11955614
申请日：2007-12-13
申请人： Tyson Dean Norlin , Steven R. Schmid , Edward J. Murphy , John M. Zimmerman , Anthony Joseph Tortorello
发明人： Tyson Dean Norlin , Steven R. Schmid , Edward J. Murphy , John M. Zimmerman , Anthony Joseph Tortorello
IPC分类号： B32B17/02 , C08L75/04 , B32B17/10 , C03C25/34
CPC分类号： G02B6/036 , C03B37/01262 , C03C25/106 , C08G18/672 , C08G18/724 , C09D5/002 , C09D175/16 , G02B6/02395 , Y10T428/2964 , C08G18/48
摘要： Radiation curable coatings for use as a Primary Coating for optical fibers, optical fibers coated with said coatings and processes for coating optical fibers. The radiation curable Primary Coating composition of the instant claimed invention includes an oligomer, a diluent monomer; a photoinitiator; an antioxidant; and an adhesion promoter; wherein said oligomer is the reaction product of: a hydroxyethyl acrylate; an aromatic isocyanate; an aliphatic isocyanate; a polyol; a catalyst; and an inhibitor, wherein said oligomer has a number average molecular weight of from at least about 4000 g/mol to less than or equal to about 15,000 g/μmol; and wherein said catalyst is selected from the group consisting of dibutyl tin dilaurate; metal carboxylates, including, but not limited to: organobismuth catalysts such as bismuth neodecanoate; zinc neodecanoate; zirconium neodecanoate; zinc 2-ethylhexanoate; sulfonic acids, including but not limited to dodecylbenzene sulfonic acid, methane sulfonic acid; amino or organo-base catalysts, including, but not limited to: 1,2-dimethylimidazole and diazabicyclooctane; triphenyl phosphine; alkoxides of zirconium and titanium, including, but not limited to Zirconium butoxide and Titanium butoxide; and Ionic liquid phosphonium salts; and tetradecyl(trihexyl)phosphonium chloride; and wherein a cured film of said radiation curable Primary Coating composition has a peak tan delta Tg of from about −25° C. to about −45° C. and a modulus of from about 0.50 MPa to about 1.2 MPa.
摘要翻译：用作光纤的主要涂层的可辐射固化涂层，涂覆有所述涂层的光纤和用于涂覆光纤的工艺。本发明的可辐射固化的初级涂料组合物包括低聚物，稀释剂单体; 光引发剂; 抗氧化剂和粘合促进剂; 其中所述低聚物是以下物质的反应产物：丙烯酸羟乙酯; 芳香族异氰酸酯; 脂族异氰酸酯; 多元醇催化剂和抑制剂，其中所述低聚物的数均分子量为至少约4000g / mol至小于或等于约15,000g / mumol; 并且其中所述催化剂选自二月桂酸二丁基锡; 金属羧酸盐，包括但不限于：有机铋催化剂如新戊酸铋; 新癸酸锌; 新癸酸锆; 2-乙基己酸锌; 磺酸，包括但不限于十二烷基苯磺酸，甲磺酸; 氨基或有机碱催化剂，包括但不限于：1,2-二甲基咪唑和二氮杂双环辛烷; 三苯基膦锆和钛的醇盐包括但不限于丁氧基锆和丁醇钛; 和离子液体鏻盐; 和十四烷基（三己基）鏻氯化物; 并且其中所述可辐射固化的初级涂料组合物的固化膜的峰值tanδTg为约-25℃至约-45℃，模量为约0.50MPa至约1.2MPa。

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