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1. 发明授权

US06287529B1 Method for selective catalytic oxidation of carbon monoxide 失效
标题翻译：一氧化碳选择性催化氧化的方法
公开(公告)号：US06287529B1
公开(公告)日：2001-09-11
申请号：US09192576
申请日：1998-11-17
申请人： Dietmar Heil , Barbara Strobel , Norbert Wiesheu , Detlef zur Megede , Uwe Benz
发明人： Dietmar Heil , Barbara Strobel , Norbert Wiesheu , Detlef zur Megede , Uwe Benz
IPC分类号： C01B3120
CPC分类号： B01J12/007 , B01D53/864 , B01J8/0285 , B01J19/249 , B01J2219/2453 , B01J2219/2461 , B01J2219/2462 , B01J2219/2474 , B01J2219/2477 , B01J2219/2479 , B01J2219/2496 , B01J2219/2498 , C01B3/583 , C01B2203/044 , C01B2203/047 , H01M8/04029 , H01M8/0662
摘要： In a method and apparatus for selective catalytic oxidation of carbon monoxide, the gas mixture and an additionally added oxidizing gas are conducted through a reactor containing the catalyst. Oxidizing gas is added at several points along the mixed gas flow path with a controlled or regulated through flow volume. The mixed gas stream is cooled passively by static mixing structures located in the inlet area of the CO-oxidation reactor. By controlling exothermal CO oxidation along the reactor path, a very variable process guidance is provided, that can be adjusted to individual situations.
摘要翻译：在用于一氧化碳的选择性催化氧化的方法和装置中，气体混合物和附加添加的氧化气体通过含有催化剂的反应器进行。氧化气体在具有受控或调节的通过流量的混合气体流动路径的几个点处加入。通过位于CO氧化反应器入口区域的静态混合结构被动地冷却混合气流。通过控制沿着反应器路径的放热CO氧化，提供了非常可变的过程指导，可以根据个别情况进行调整。

2. 发明授权

US5874051A Method and apparatus for selective catalytic oxidation of carbon monoxide 失效
标题翻译：一氧化碳选择性催化氧化的方法和装置
公开(公告)号：US5874051A
公开(公告)日：1999-02-23
申请号：US753809
申请日：1996-12-02
申请人： Dietmar Heil , Barbara Strobel , Norbert Wiesheu , Detlef zur Megede , Uwe Benz
发明人： Dietmar Heil , Barbara Strobel , Norbert Wiesheu , Detlef zur Megede , Uwe Benz
IPC分类号： B01D53/86 , B01J8/02 , B01J12/00 , B01J19/24 , C01B3/58 , H01M8/04029 , H01M8/0662 , B01D53/34
CPC分类号： B01J12/007 , B01D53/864 , B01J19/249 , B01J8/0285 , C01B3/583 , H01M8/0662 , B01J2219/2453 , B01J2219/2461 , B01J2219/2462 , B01J2219/2474 , B01J2219/2477 , B01J2219/2479 , B01J2219/2496 , B01J2219/2498 , C01B2203/044 , C01B2203/047 , H01M8/04029
摘要： In a method and apparatus for selective catalytic oxidation of carbon monoxide, the gas mixture and an additionally added oxidizing gas are conducted through a reactor containing the catalyst. Oxidizing gas is added at several points along the mixed gas flow path with a controlled or regulated through flow volume. The mixed gas stream is cooled passively by static mixing structures located in the inlet area of the CO-oxidation reactor. By controlling exothermal CO oxidation along the reactor path, a very variable process guidance is provided, that can be adjusted to individual situations.
摘要翻译：在用于一氧化碳的选择性催化氧化的方法和装置中，气体混合物和附加添加的氧化气体通过含有催化剂的反应器进行。氧化气体在具有受控或调节的通过流量的混合气体流动路径的几个点处加入。通过位于CO氧化反应器入口区域的静态混合结构被动地冷却混合气流。通过控制沿着反应器路径的放热CO氧化，提供了非常可变的过程指导，可以根据个别情况进行调整。

3. 发明授权

US6086839A System and process for the water vapor reforming of a hydrocarbon 失效
标题翻译：烃的水汽重整的系统和方法
公开(公告)号：US6086839A
公开(公告)日：2000-07-11
申请号：US206380
申请日：1998-12-07
申请人： Rainer Autenrieth , Stefan Boneberg , Dietmar Heil , Martin Schuessler , Barbara Strobel , Steffen Wieland , Detlef zur Megede
发明人： Rainer Autenrieth , Stefan Boneberg , Dietmar Heil , Martin Schuessler , Barbara Strobel , Steffen Wieland , Detlef zur Megede
IPC分类号： B01B1/00 , C01B3/38 , C01B3/48 , C01B3/50 , C01B3/58 , H01M8/0612 , B01J8/04 , B01J10/00
CPC分类号： H01M8/0631 , B01B1/005 , C01B3/382 , C01B3/48 , C01B3/583 , H01M8/0612 , C01B2203/0233 , C01B2203/0283 , C01B2203/044 , C01B2203/047 , C01B2203/066 , C01B2203/0811 , C01B2203/0822 , C01B2203/0827 , C01B2203/0838 , C01B2203/0844 , C01B2203/0866 , C01B2203/1223 , C01B2203/1288 , C01B2203/143 , C01B2203/1604 , C01B2203/1685 , C01B2203/169 , C01B2203/82 , Y02P20/128
摘要： A system for the water vapor reforming of a hydrocarbon includes an evaporator, a prereforming unit, a main reformer, a CO removal unit and at least one catalytic burner unit. A first burner unit is in a thermal contact with the evaporator and a second burner unit is in a thermal contact with the main reformer, and the prereforming unit is in a thermal contact with the CO removal unit by way of one heat conducting separating medium. In addition, the outlet of the CO removal unit is connected with the inlet of the at least one burner unit. During a cold start, a heating-up operation is carried out during which first the two burner units are activated with an external feeding of hydrogen or hydrocarbon, and the reforming operation is started with a hydrocarbon fraction that is lower than in the normal operation. The resulting reformate gas, instead of the externally fed hydrogen or hydrocarbon, is introduced as fuel into the burner units.
摘要翻译：用于烃的水蒸气重整的系统包括蒸发器，预成型单元，主重整器，CO去除单元和至少一个催化燃烧器单元。第一燃烧器单元与蒸发器热接触，并且第二燃烧器单元与主重整器热接触，并且预成形单元通过一个导热分离介质与CO去除单元热接触。此外，CO去除单元的出口与至少一个燃烧器单元的入口连接。在冷启动期间，进行加热操作，其中首先通过外部进料氢气或烃来激活两个燃烧器单元，并且重整操作以低于正常操作的烃馏分开始。所得到的重整气体代替外部供给的氢气或烃，作为燃料引入燃烧器单元。

4. 发明授权

US06447736B1 System for the water vapor reforming of a hydrocarbon 失效
标题翻译：烃类水汽重整系统
公开(公告)号：US06447736B1
公开(公告)日：2002-09-10
申请号：US09206379
申请日：1998-12-07
申请人： Rainer Autenrieth , Stefan Boneberg , Andreas Christen , Dietmar Heil , Barbara Strobel , Steffen Wieland , Detlef zur Megede
发明人： Rainer Autenrieth , Stefan Boneberg , Andreas Christen , Dietmar Heil , Barbara Strobel , Steffen Wieland , Detlef zur Megede
IPC分类号： B01J800
CPC分类号： H01M8/0631 , B01B1/005 , B01J19/249 , B01J2219/0002 , B01J2219/2453 , B01J2219/2462 , B01J2219/2492 , C01B3/323 , C01B3/382 , C01B3/48 , C01B3/583 , C01B2203/0233 , C01B2203/0283 , C01B2203/044 , C01B2203/047 , C01B2203/066 , C01B2203/0811 , C01B2203/0838 , C01B2203/0844 , C01B2203/0866 , C01B2203/1223 , C01B2203/1288 , C01B2203/143 , C01B2203/1604 , C01B2203/82
摘要： A system for the water vapor reforming of a hydrocarbon includes a modular reactor unit of the plate stack and/or tube bundle type that, in an integrated manner, contains an evaporator, a prereforming unit, a main reformer, a CO removal unit and a catalytic burner unit. The evaporator and the main reformer are in a thermal contact with the catalytic burner unit and, the prereforming unit is in a thermal contact with the CO removal unit.
摘要翻译：用于烃的水蒸气重整的系统包括板堆叠和/或管束型的模块化反应器单元，其以整体方式包含蒸发器，预成型单元，主重整器，CO去除单元和催化燃烧器单元。蒸发器和主重整器与催化燃烧器单元热接触，并且预成型单元与CO去除单元热接触。

5. 发明授权

US5922291A Reforming reactor system and particle filter usable therefor 失效
标题翻译：重整反应器系统和可用的颗粒过滤器
公开(公告)号：US5922291A
公开(公告)日：1999-07-13
申请号：US873772
申请日：1997-06-12
申请人： Josef Hanfling , Dietmar Heil , Rainer Autenrieth , Norbert Wiesheu
发明人： Josef Hanfling , Dietmar Heil , Rainer Autenrieth , Norbert Wiesheu
IPC分类号： B01J8/00 , B01J8/02 , C01B3/32 , H01M8/0612
CPC分类号： H01M8/0631 , B01J8/006 , B01J8/0085 , B01J8/02 , C01B3/323 , B01J2208/00495 , B01J2219/182
摘要： A reforming reactor system for water vapor reforming of methanol in fuel-cell operated motor vehicles has a reactor unit with a catalyst-filled reaction space and a particle filter which is arranged in a reformate gas pipe downstream of the reactor unit. The catalyst material is carried in the reaction space by a sieve below which a metallic nonwoven for catching sieved-out fragments and dust particles of the catalyst fill is situated. The particle filter contains a spun steel wool netting and/or several filter steps serially connected behind one another. The particle filter may be arranged to be exchangeable without interrupting the operation of the system. Specifically, a particle filter which has a filter body which can be changed in a gas-tight manner transversely to the gas flow and/or a cyclone filter can be used which has a closing device for the purpose of an emptying of a particle collecting pot which does not interrupt the operation.
摘要翻译：用于在燃料电池操作的机动车辆中进行甲醇水汽重整的重整反应器系统具有反应器单元，其具有填充有催化剂的反应空间和颗粒过滤器，其被布置在反应器单元下游的重整气体管道中。催化剂材料通过一个筛子在反应空间中载置，在该筛下方，放置用于捕获筛分碎片的金属非织造物和催化剂填充物的粉尘颗粒。颗粒过滤器包含纺丝钢丝网和/或彼此串联连接的几个过滤器步骤。颗粒过滤器可以被布置为可以交换而不中断系统的操作。具体而言，可以使用具有能够以气密方式与气流横向变化的过滤体的粒子过滤器和/或旋风过滤器，其具有用于排空颗粒收集罐的关闭装置这不会中断操作。

6. 发明授权

US06264856B1 Three-step reforming reactor especially for mobile fuel cell 失效
标题翻译：特别是用于移动燃料电池的三步重整反应堆
公开(公告)号：US06264856B1
公开(公告)日：2001-07-24
申请号：US09475275
申请日：1999-12-30
申请人： Rainer Autenrieth , Josef Haenfling , Dietmar Heil , Heinz Steinke , Norbert Wiesheu
发明人： Rainer Autenrieth , Josef Haenfling , Dietmar Heil , Heinz Steinke , Norbert Wiesheu
IPC分类号： C01B302
CPC分类号： H01M8/0631 , B01J8/0285 , B01J8/067 , B01J2208/00132 , C01B3/323 , C01B3/38
摘要： A reforming reactor, particularly for the water vapor reforming of methanol, with three serially arranged reactor steps, each of which is charged with a catalyst pellet fill. According to the invention, the center reactor step is maintained at a temperature which is suitable for the reforming reaction, while the two other reactor steps remain unheated. The present invention may be used as a reforming reactor for the water vapor reforming of methanol for the purpose of producing hydrogen in a fuel-cell operated motor vehicle.
摘要翻译：一种重整反应器，特别是用于甲醇的水蒸气重整，具有三个连续排列的反应器步骤，每个反应器装有催化剂颗粒填料。根据本发明，中心反应器步骤保持在适于重整反应的温度，而另外两个反应器步骤保持不加热。本发明可以用作用于在燃料电池操作的机动车辆中产生氢气的甲醇的水蒸气重整的重整反应器。

7. 发明授权

US5672629A Two-stage reforming of methanol 失效
标题翻译：甲醇二阶段重整
公开(公告)号：US5672629A
公开(公告)日：1997-09-30
申请号：US488660
申请日：1995-06-08
申请人： Dietmar Heil , Uwe Benz
发明人： Dietmar Heil , Uwe Benz
IPC分类号： B01J8/02 , B01J8/04 , B01J8/06 , B01J19/24 , C01B3/32 , H01M8/06 , C07C27/00
CPC分类号： H01M8/0631 , B01J19/249 , B01J8/0285 , B01J8/04 , B01J8/0438 , B01J8/0496 , B01J8/067 , C01B3/323 , B01J2208/00212 , B01J2208/00309 , B01J2208/00398 , B01J2208/022 , B01J2219/182 , B01J2219/2453 , B01J2219/2454 , B01J2219/2461 , B01J2219/2462 , B01J2219/2465 , B01J2219/2467 , B01J2219/2474 , B01J2219/2479 , B01J2219/2481 , B01J2219/2482 , B01J2219/2497 , B01J2219/2498
摘要： This invention relates to a process and an apparatus for the catalytic water vapor reforming of methanol. The reforming process is carried out in two stages. The methanol is incompletely reacted in the first stage in a heat-transfer-optimized process with a high specific catalyst load. In a reaction-optimized second stage, while the specific catalyst load is lower, a further reaction is carried out which completes the methanol reaction. In addition, a tube bundle reactor is disclosed in which the first, heat-transfer-optimized stage takes place in reaction tubes which, for constructing heat transfer medium ducts, are each surrounded by a concentric outer tube, while the second, reaction-optimized stage is carried out after the return of the reform gas in the housing. The reaction tubes as well as the area between the outer tubes are filled with catalyst material.
摘要翻译：本发明涉及甲醇催化水蒸气重整的方法和装置。重整过程分两个阶段进行。在具有高比催化剂负载的热转移优化方法中，甲醇在第一阶段不完全反应。在反应优化的第二阶段中，当特定催化剂负载较低时，进行进一步的反应，其完成甲醇反应。另外，公开了一种管束反应器，其中第一个传热优化阶段发生在反应管中，反应管用于构造传热介质管道，每个管道被同心的外管包围，而第二个反应优化的在房屋中改造气体返回后进行阶段。反应管以及外管之间的区域填充有催化剂材料。

8. 发明授权

US5753194A Two-stage reforming of methanol 失效
标题翻译：甲醇二阶段重整
公开(公告)号：US5753194A
公开(公告)日：1998-05-19
申请号：US708967
申请日：1996-09-06
申请人： Dietmar Heil , Uwe Benz
发明人： Dietmar Heil , Uwe Benz
IPC分类号： B01J8/02 , B01J8/04 , B01J8/06 , B01J19/24 , C01B3/32 , H01M8/06
CPC分类号： H01M8/0631 , B01J19/249 , B01J8/0285 , B01J8/04 , B01J8/0438 , B01J8/0496 , B01J8/067 , C01B3/323 , B01J2208/00212 , B01J2208/00309 , B01J2208/00398 , B01J2208/022 , B01J2219/182 , B01J2219/2453 , B01J2219/2454 , B01J2219/2461 , B01J2219/2462 , B01J2219/2465 , B01J2219/2467 , B01J2219/2474 , B01J2219/2479 , B01J2219/2481 , B01J2219/2482 , B01J2219/2497 , B01J2219/2498
摘要： This invention relates to a process and an apparatus for the catalytic water vapor reforming of methanol. The reforming process is carried out in two stages. The methanol is incompletely reacted in the first stage in a heat-transfer-optimized process with a high specific catalyst load. In a reaction-optimized second stage, while the specific catalyst load is lower, a further reaction is carried out which completes the methanol reaction. In addition, a tube bundle reactor is disclosed in which the first, heat-transfer-optimized stage takes place in reaction tubes which, for constructing heat transfer medium ducts, are each surrounded by a concentric outer tube, while the second, reaction-optimized stage is carried out after the return of the reform gas in the housing. The reaction tubes as well as the area between the outer tubes are filled with catalyst material.
摘要翻译：本发明涉及甲醇催化水蒸气重整的方法和装置。重整过程分两个阶段进行。在具有高比催化剂负载的热转移优化方法中，甲醇在第一阶段不完全反应。在反应优化的第二阶段中，当特定催化剂负载较低时，进行进一步的反应，其完成甲醇反应。另外，公开了一种管束反应器，其中第一个传热优化阶段发生在反应管中，反应管用于构造传热介质管道，每个管道被同心的外管包围，而第二个反应优化的在房屋中改造气体返回后进行阶段。反应管以及外管之间的区域填充有催化剂材料。

9. 发明授权

US06187066B1 Central heating device for a gas-generating system 失效
标题翻译：用于气体发生系统的中央加热装置
公开(公告)号：US06187066B1
公开(公告)日：2001-02-13
申请号：US08937357
申请日：1997-09-24
申请人： Uwe Benz , Stefan Boneberg , Dietmar Heil
发明人： Uwe Benz , Stefan Boneberg , Dietmar Heil
IPC分类号： B01J804
CPC分类号： H01M8/0631 , B01J12/007 , B01J2208/00008 , B01J2208/00716 , C01B3/323 , C01B3/38 , C01B2203/0233 , C01B2203/066 , C01B2203/0811 , C01B2203/0833 , C01B2203/085 , C01B2203/1223 , C01B2203/1604 , C01B2203/1695 , F28D9/00
摘要： In a device for providing heating energy to a gas-generating system by means of essentially complete catalytic combustion of a fuel on a suitable catalyst material, heat energy is transferred directly or by means of a heat-conducting medium from the catalytic burner to the gas-generating system. To improve the starting behavior and the exhaust emissions, the device comprises three components that are at least temporarily traversed by fuel, with a cold-start component having an electrical heating device. The central component is preferably designed as a filter press with an integrated heat exchanger. A third, unheated, stage is also provided for residual gas combustion.
摘要翻译：在通过燃料在合适的催化剂材料上基本上完全催化燃烧来向气体发生系统提供加热能量的装置中，热能直接地或通过导热介质从催化燃烧器转移到气体生成系统。为了改善起动行为和废气排放，该装置包括至少由燃料临时穿过的三个部件，具有电加热装置的冷启动部件。中心部件优选地设计为具有集成热交换器的压滤机。第三个未加热的阶段也用于残余气体燃烧。

10. 发明授权

US5935277A Reforming reactor, particularly for the water vapor reforming of methanol 失效
标题翻译：重整反应器，特别适用于甲醇的水汽重整
公开(公告)号：US5935277A
公开(公告)日：1999-08-10
申请号：US876390
申请日：1997-06-16
申请人： Rainer Autenrieth , Dietmar Heil , Wolfgang Weger , Uwe Benz
发明人： Rainer Autenrieth , Dietmar Heil , Wolfgang Weger , Uwe Benz
IPC分类号： B01J8/00 , B01J8/06 , C01B3/32 , C01B3/38 , H01M8/0612
CPC分类号： H01M8/0631 , B01J8/002 , B01J8/008 , B01J8/06 , C01B3/323 , C01B3/38 , B01J2208/00132 , B01J2208/0069 , B01J2208/00884 , C01B2203/0233 , C01B2203/066 , C01B2203/0833 , C01B2203/1011 , C01B2203/1076 , C01B2203/1082 , C01B2203/1223
摘要： In a reforming reactor suitable particularly for the water vapor reforming of methanol in mobile applications such as vehicles, a reaction space is filled with a catalyst pellet fill and has a movable reaction space wall which exerts a position-fixing pressure onto the catalyst pellet fill. According to the invention, a filling device is provided through which catalyst material can be filled from the outside into the reaction space through a passage opening formed in one of the reaction space walls.
摘要翻译：在适用于诸如车辆的移动应用中特别适用于甲醇的水汽重整的重整反应器中，反应空间填充有催化剂颗粒填充物，并且具有向催化剂颗粒填充物施加位置固定压力的可移动的反应空间壁。根据本发明，提供一种填充装置，催化剂材料可以通过该填充装置通过形成在反应空间壁之一中的通道开口从外部填充到反应空间中。

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