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1. 发明授权

US06242549B1 Composition based on a dicyclopentenyloxyalkyl ester of (meth) acrylic acid and its applications in the building sector 失效
标题翻译：基于（甲基）丙烯酸的二环戊烯氧基烷基酯的组合物及其在建筑领域的应用
公开(公告)号：US06242549B1
公开(公告)日：2001-06-05
申请号：US08632081
申请日：1996-04-15
申请人： Didier Vanhoye , Martine Cerf , Yves Barbier , Mieczyslaw Wnuk
发明人： Didier Vanhoye , Martine Cerf , Yves Barbier , Mieczyslaw Wnuk
IPC分类号： C08L3304
CPC分类号： C04B41/009 , C04B26/04 , C04B41/483 , C04B41/4857 , C04B41/63 , C04B2111/00491 , C04B2111/60 , C08F220/30 , C04B41/52 , C04B28/02
摘要： This composition, which is useful as a binder in the preparation of synthetic resin concretes or mortars, bonding primers or finishing coats, comprises (A) a system of monomers comprising: (a1) 50-90 parts of a dicyclopentenyloxyalkyl eater: where R=H or CH3; n=1 or 2; and R1=C2-C6 alkylene; (a2) 0-25 parts of at least one heavy (meth)acrylate giving a homopolymer with a Tg higher than that of a homopolymer of (a1); (a3) 0-25 parts of at least one heavy (meth)acrylate giving a homopolymer with a Tg lower than that of a homopolymer of (a1); (a4) 0-25 parts of at least one monomer containing at least two (meth)acrylic unsaturations; and (B) 5-30 parts of at least one poly(allyl glycidyl ether); and (C) an initiating system chosen from (C1) to (C4): (C1) 0.1-3 parts of at least one organic peroxide derived from a C3-C18 hydrocarbon compound and 0.1-2 parts of at least one aromatic amine; (C2) 0.1-3 parts of at least one organic hydroperoxide derived from a C3-C18, hydrocarbon compound and 0.0005-2 parts of at least one polyvalent metal salt; (C3): (C1) +0.0005-2 partsof at least one polyvalent metal salt; and (C4): (C1)+(C2), all the amounts being given by weight per 100 parts by weight of (A)+(B).
摘要翻译：该组合物可用作制备合成树脂混凝土或砂浆，粘结底漆或整理涂料中的粘合剂，包括（A）单体体系，其包含：（a1）50-90份二环戊烯基氧基烷基酯：其中R = H或CH3; n = 1或2; 和R1 = C2-C6亚烷基; （a2）0-25份至少一种重量（甲基）丙烯酸酯，得到Tg高于（a1）的均聚物的均聚物; （a3）0-25份至少一种重（甲基）丙烯酸酯，得到的Tg低于（a1）的均聚物的Tg的均聚物; （a4）0-25份至少一种含有至少两个（甲基）丙烯酸不饱和度的单体; 和（B）5-30份至少一种聚（烯丙基缩水甘油醚）; 和（C）选自（C1）至（C4）的引发体系：（C1）0.1-3份至少一种衍生自C3-C18烃化合物的有机过氧化物和0.1-2份至少一种芳族胺; （C2）0.1-3份至少一种衍生自C3-C18烃化合物的有机氢过氧化物和0.0005-2份至少一种多价金属盐; （C3）：（C1）+ 0.0005-2至少一种多价金属盐; 和（C4）：（C1）+（C2），所有的量均为每100重量份的（A）+（B）的重量。

2. 发明授权

US5798406A Fluorinated acrylic and methacrylic latices and mixtures thereof, processes for manufacturing them and their applications in the field of hydrophobic coatings 失效
标题翻译：氟化丙烯酸和甲基丙烯酸胶乳及其混合物，其制造方法及其在疏水性涂料领域的应用
公开(公告)号：US5798406A
公开(公告)日：1998-08-25
申请号：US544693
申请日：1995-10-18
申请人： Bruno Feret , Laure Sarrazin , Didier Vanhoye
发明人： Bruno Feret , Laure Sarrazin , Didier Vanhoye
IPC分类号： C08L33/16 , C08F2/22 , C08F2/24 , C08F2/44 , C08F20/22 , C08F20/24 , C08F265/04 , C08F285/00 , C08L13/02 , C08L33/04 , C08L51/00 , C09D133/04 , C09D133/16 , D06M15/277 , C08J3/02
CPC分类号： D06M15/277 , C08F20/22 , C08F265/04 , C08F285/00
摘要： This fluorinated (meth)acrylic latex consists of a dispersion of particles or of a mixture of dispersions of particles, these dispersions being obtained by emulsion polymerization in an aqueous medium, in at least one stage, wherein one more perfluorinated monomer(s) of formula (I) has/have been used as sole fluorinated comonomer(s) for the formation of the particles, and which is/are distributed statistically in particles formed in one stage or distributed statistically in the shell of structured particles of the core-shell or core-intermediate layer(s)-shell type resulting from a polymerization in two stages and in more than two stages, respectively, the said latex consisting of a dispersion of the said structured particles or of a mixture of at least one dispersion of the said fluorinated structured particles and/or at least one dispersion of the said fluorinated statistical particles and at least one dispersion of unfluorinated statistical particles, the monomer or monomers of formula (I) representing less than 80% by weight of the shell of the fluorinated structured particles, the proportion of monomers of formula (I) relative to the collective monomers used to form all of the particles of the said latex being between 1.8 and 20% by weight. ##STR1## R.sup.1 .dbd.CH.sub.3 or H; R.sup.2 =perfluorinated C.sub.1 -C.sub.10 alkyl; and 0
摘要翻译：该氟化（甲基）丙烯酸胶乳由颗粒分散体或颗粒分散体的混合物组成，这些分散体通过在至少一个阶段中在水性介质中的乳液聚合获得，其中一个或更多个全氟化单体（I）已经/已经被用作用于形成颗粒的唯一的氟化共聚单体，并且其在统计学上分布在一个阶段中形成的颗粒中或在统计学上分布在核壳的结构化颗粒的壳中或分布在分别由两个阶段和两个以上阶段的聚合产生的核 - 中间层 - 壳型，所述胶乳由所述结构化颗粒的分散体或所述结构化颗粒的至少一种分散体的混合物组成氟化结构化颗粒和/或所述氟化统计颗粒和至少一种未氟化统计颗粒分散体的至少一种分散体，形式的单体或单体 ula（I）占氟化结构化颗粒的壳的小于80重量％，式（I）单体相对于用于形成所有胶乳的所有颗粒的共聚单体的比例在1.8和20之间重量％。（I）R1 = CH3或H; R2 =全氟化C1-C10烷基; 和0

3. 发明授权

US06673884B2 Method for making monomers with two quarternary amino group and (co)polymers obtained from said monomers 失效
标题翻译：制备具有两个季氨基的单体和由所述单体获得的（共）聚合物的方法
公开(公告)号：US06673884B2
公开(公告)日：2004-01-06
申请号：US09959622
申请日：2002-08-28
申请人： Alain Riondel , Denis Tembou N'Zudie , Marc Esch , Vladimir Chaplinski , Didier Vanhoye
发明人： Alain Riondel , Denis Tembou N'Zudie , Marc Esch , Vladimir Chaplinski , Didier Vanhoye
IPC分类号： C08F12600
CPC分类号： C07C213/08 , C07C219/08
摘要： To prepare compound (I), a quaternising agent R3—X⊖ is introduced into a solution, in an organic solvent or a mixture of organic solvents, of a compound of formula (III), at a temperature of 35 to 80° C., and the reaction is then allowed to continue at said temperature until compound (III) has disappeared completely or substantially completely, after which water is added and then an aqueous solution of compound (I) is separated and the water removed as necessary. R1=H or —CH3; R2=one of —CH3, —C2H5, —C3H7 and —C4H9; the two R3 are the same or different and each represents one of —CH3, —C2H5, —C3H7, —C4H9 and —CH2C6H5; and the two X⊖ are the same or different and each represents Cl⊖ or Br⊖.
摘要翻译：为了制备化合物（I），在35℃的温度下将季铵化物R 3 -X'引入式（III）化合物的有机溶剂或有机溶剂的混合物的溶液中至80℃，然后使所述反应在所述温度下继续，直到化合物（III）完全或基本上完全消失，然后加入水，然后分离出化合物（I）的水溶液，并除去水 R 1 = H或-CH 3; R 2 = -CH 3，-C 2 H 5，-C 3 H 7和-C 4 H 9之一; 两个R 3相同或不同，各自表示-CH 3，-C 2 H 5，-C 3 H 7，-C 4 H 9和-CH 2 C 6 H 5中的一个; 两个X <⊖>相同或不同，分别表示Cl <⊖>或Br <⊖>。

4. 发明授权

US5908908A Pressure-sensitive adhesive polymers 失效
标题翻译：压敏粘合剂聚合物
公开(公告)号：US5908908A
公开(公告)日：1999-06-01
申请号：US903151
申请日：1997-07-30
申请人： Didier Vanhoye , Denis Melot , Jean Lebez , Cyril Wiegert
发明人： Didier Vanhoye , Denis Melot , Jean Lebez , Cyril Wiegert
IPC分类号： C09J133/08 , C08F2/26 , C08F218/04 , C08F220/06 , C08F220/10 , C08F220/12 , C08F220/18 , C09J133/06 , C09J133/10 , C09K3/00 , C09K3/10 , F16J15/00 , C08F20/10
CPC分类号： C08F220/12 , C09J133/064
摘要： This pressure-sensitive adhesive polymer is obtained by emulsion polymerization of the mixture of the following monomers, for a total of 100% by weight: (A) 40 to 95% by weight of at least one (meth)acrylic or vinyl monomer capable of resulting in a homopolymer which has a glass transition temperature lower than or equal to -40.degree. C.; (B) 2 to 50% by weight of at least one (meth)acrylic or vinyl monomer capable of resulting in a homopolymer which has a glass transition temperature higher than or equal to 0.degree. C.; (C) 0.5 to 6% by weight of at least one carboxylic (meth)acrylic monomer; (D) 0 to 5% by weight of at least one (meth)acrylic monomer ethoxylated with 1 to 20 moles of ethylene oxide; (E) 0.05 to 1% by weight of at least one (meth)acrylic or vinyl monomer containing a ureido group; and (F) 0 to 2% by weight of at least one acrylic or vinyl monomer carrying a sulphonate functional group, the said polymer having a glass transition temperature lower than or equal to -25.degree. C.
摘要翻译：该压敏粘合剂聚合物通过以下单体的混合物的乳液聚合获得，总共100重量％：（A）40至95重量％的至少一种能够具有下列单体的（甲基）丙烯酸或乙烯基单体导致玻璃化转变温度低于或等于-40℃的均聚物; （B）2〜50重量％的能够得到玻璃化转变温度高于或等于0℃的均聚物的至少一种（甲基）丙烯酸或乙烯基单体; （C）0.5〜6重量％的至少一种羧酸（甲基）丙烯酸单体; （D）0至5重量％的至少一种用1至20摩尔环氧乙烷乙氧基化的（甲基）丙烯酸单体; （E）0.05至1重量％的至少一种含有脲基的（甲基）丙烯酸或乙烯基单体; 和（F）0至2重量％的至少一种带有磺酸酯官能团的丙烯酸或乙烯基单体，所述聚合物具有低于或等于-25℃的玻璃化转变温度。

5. 发明授权

US5256748A Precursors of polymers containing isocyanurate units 失效
标题翻译：含有异氰脲酸酯单元的聚合物的前体
公开(公告)号：US5256748A
公开(公告)日：1993-10-26
申请号：US722495
申请日：1991-07-02
申请人： Didier Vanhoye , Paul Grosius
发明人： Didier Vanhoye , Paul Grosius
IPC分类号： C07D251/32 , C07D251/34 , C08F16/00 , C08F20/34 , C08F220/34 , C08F290/00 , C08F299/06 , C08G18/32 , C08G18/38 , C08G18/64 , C08G18/67 , C08G18/78 , C08G73/06 , C08F26/08
CPC分类号： C08G18/3853 , C07D251/34 , C08G18/672 , C08G18/7893
摘要： Oligomers of the formula ##STR1## wherein: (1) at least one A=--CH.sub.2 CHR.sup.1 COODOH (a) (R.sup.1 =H, CH.sub.3 and D=C.sub.1 -C.sub.4 alkylene), the other A's=H or C.sub.1 -C.sub.4 alkyl, it being possible for at least a part of the residues (a) to be converted into A.sup.1 =--CH.sub.2 CHR.sup.1 COODOCONHD.sup.1 NCO (D.sup.1 =divalent organic residue), it being possible for at least a part of the residues A.sup.1 to be converted into A.sup.2 =--CH.sub.2 CHR.sup.1 COODOCONHD.sup.1 NHCOOR.sup.2 (R.sup.2 =monovalent radical obtained by removal of OH from a monoalcohol containing a vinylidene group);(2) at least one A=D.sup.2 OCONHD'.sup.1 NHCOOR'.sup.2 (b) where D.sup.2 =C.sub.1 -C.sub.4 alkylene or --D.sup.3 --(--O--D.sup.3 --).sub.n --, with D.sup.3 =C.sub.1 -C.sub.4 alkylene and n=1-12; D'.sup.1 analogous to D.sup.1 ; R'.sup.2 analogous to R.sup.2 ; the other residue(s) A denoting --D.sup.2 OCONHD'.sup.1 NCO.These oligomers are intended especially to be copolymerized under ultraviolet radiation in a reactive diluent and in the presence of an initiator so as to form (co)polymers which have good hardness and good thermal resistance and which can be employed in the field of coatings, inks, and photopolymerizable adhesives.
摘要翻译：其中：（1）至少一个A = -CH 2 CHR 1 COODOH（a）（R 1 = H，CH 3和D = C 1 -C 4亚烷基），另一个A'= H或C 1 -C 4烷基，残留物（a）的至少一部分可能被转化为A1 = -CH2CHR1COODOCONHD1NCO（D1 =二价有机残基），至少部分残基A1可能转化为A2 = -CH2CHR1COODOCONHD1NHCOOR2（R2 =通过从含有亚乙烯基的一元醇除去OH而获得的单价基团）; （2）至少一个A = D2OCONHD'1NHCOOR'2（b）其中D2 = C1-C4亚烷基或-D3 - （ - O-D3-）n-，其中D3 = C1-C4亚烷基，n = 1-12 ; D'1类似于D1; R'2类似于R2; 其他残留物A表示-D2OCONHD'1NCO。这些低聚物特别是在反应性稀释剂中和在引发剂的存在下在紫外线辐射下共聚以形成具有良好硬度和良好耐热性并且可用于涂料，油墨领域的（共）聚合物，和光聚合粘合剂。

6. 发明授权

US5210199A Process for the preparation of alkylimidazolidone (meth) acrylate 失效
标题翻译：制备丙烯酰胺（甲基）丙烯酸酯的方法
公开(公告)号：US5210199A
公开(公告)日：1993-05-11
申请号：US626107
申请日：1990-12-14
申请人： Paul Grosius , Didier Vanhoye
发明人： Paul Grosius , Didier Vanhoye
IPC分类号： B01J31/12 , C07B61/00 , C07D233/32 , C07D239/10 , C07D243/04 , C07D245/02 , C07D247/02
CPC分类号： C07D239/10 , C07D233/32 , C07D243/04 , C07D245/02 , C07D247/02
摘要： At least one (meth)acrylate is reacted with a heterocyclic alcohol (III) in the presence of at least one catalyst chosen from dialkyltin oxides and dialkyltin dialkoxides. Alkylimidazolidone acrylates and methacrylates are known for the part they play in the constitution of polymers which can be used as coatings and adhesives and for the treatment of paper and textiles, and for their use as agents for the treatment of leather and in the production of emulsion paints. ##STR1## R.sub.1 =H, CH.sub.3 ; A, B=straight or branched chain alkylene group containing from 2 to 5 carbon atoms.
摘要翻译：在至少一种选自二烷基锡氧化物和二烷基锡二烷氧基化物的催化剂的存在下，至少一种（甲基）丙烯酸酯与杂环醇（III）反应。烷基咪唑烷酮丙烯酸酯和甲基丙烯酸酯在其可以用作涂料和粘合剂以及用于处理纸和纺织品的聚合物的构成中起作用的部分是已知的，并且作为用于处理皮革和在乳液生产中的用途油漆（III）（III）R1 = H，CH3; A，B =含有2至5个碳原子的直链或支链亚烷基。

7. 发明授权

US06174950B1 Concentrated aqueous dispersions of water-soluble polymers 失效
标题翻译：水溶性聚合物的浓缩水分散体
公开(公告)号：US06174950B1
公开(公告)日：2001-01-16
申请号：US09013093
申请日：1998-01-26
申请人： Denis Tembou Nzudie , Didier Vanhoye
发明人： Denis Tembou Nzudie , Didier Vanhoye
IPC分类号： B01D1705
CPC分类号： C02F1/56 , C08F2/10 , Y10S526/932
摘要： Concentrated and low viscosity aqueous dispersions, e.g., opaque emulsions, well suited as flocculants for water treatment, comprise the water-soluble polymerizate of at least one water-soluble hydrophilic monomer A, optionally, at least one amphiphilic comonomer B and/or, also optionally, at least one hydrophobic comonomer C, in the presence of at least one polymeric dispersant incompatible therewith, for example an imidized and salified styrene/maleic anhydride copolymer or poly(diallyldimethylammonium chloride).
摘要翻译：浓缩和低粘度水分散体，例如不适合作为水处理的絮凝剂的不透明乳液，包含至少一种水溶性亲水单体A，任选地至少一种两亲共聚单体B和/或任选地，至少一种疏水性共聚单体C在至少一种与其不相容的聚合分散剂存在下，例如酰亚胺化和成盐的苯乙烯/马来酸酐共聚物或聚（二烯丙基二甲基氯化铵）。

8. 发明授权

US5728749A Photocrosslinkable compositions based on crafted reactive telomer of trifluoroethyl methacrylate and processes for their preparation 失效
标题翻译：基于制备的甲基丙烯酸三氟乙酯的反应性调聚物的光可交联组合物及其制备方法
公开(公告)号：US5728749A
公开(公告)日：1998-03-17
申请号：US564980
申请日：1995-11-30
申请人： Didier Vanhoye , Elsa Ballot , Robert Legros , Olivier Loubet , Bernard Boutevin , Bruno Ameduri
发明人： Didier Vanhoye , Elsa Ballot , Robert Legros , Olivier Loubet , Bernard Boutevin , Bruno Ameduri
IPC分类号： C08K5/00 , C08F2/38 , C08F2/48 , C08F2/50 , C08F220/18 , C08F290/00 , C08F290/04 , C08F299/00 , C08K5/37 , C08L33/04 , C08L33/14 , C08L33/16 , C09D4/06 , C09D5/00 , C09D133/04 , C09D133/16 , C08G75/04
CPC分类号： C08F290/046 , C09D4/06
摘要： This photopolymerizable composition includes an grafted reactive telomer containing trifluoroethyl methacrylate units, a reactive diluent and a photopolymerization initiator. It gives hydrophobic transparent coatings.
摘要翻译：该可光聚合组合物包括含有三氟乙基甲基丙烯酸酯单元，反应性稀释剂和光聚合引发剂的接枝反应性调聚物。它提供疏水性透明涂层。

9. 发明授权

US5169980A Process for the manufacture of benzyl methacrylate and its derivatives which are halogenated or alkylated on the aromatic nucleus 失效
标题翻译：制备甲基丙烯酸苄酯及其衍生物的方法，该衍生物在芳族核上被卤化或碱化
公开(公告)号：US5169980A
公开(公告)日：1992-12-08
申请号：US694287
申请日：1991-05-03
申请人： Didier Vanhoye , Paul Grosius , Patrice Hurtel
发明人： Didier Vanhoye , Paul Grosius , Patrice Hurtel
IPC分类号： B01J31/02 , C07B61/00 , C07C67/10 , C07C67/11 , C07C69/54
CPC分类号： C07C67/11 , C07C69/54
摘要： This process for the manufacture of benzyl methacrylate and of its halogenated or alkylated derviatives by the reaction of benzyl chloride or of one of its halogenated or alkylated derivatives with an alkali metal methacrylate is characterized in that the reaction is carried out in the presence of not more than 3 mol %, based on the benzyl chloride or a derivative, of a tertiary amine. The alkali metal is chosen especially from lithium, potassium and sodium. The tertiary amine is preferably a tertiary diamine of general formula: ##STR1## in which n is an integer ranging from 1 to 10 and R.sub.1, R.sub.2, R.sub.3 and R.sub.4, which are identical or different, are alkyl, cycloalkyl or aryl radicals containing from 1 to 12 carbon atoms, functionalized if appropriate and, if appropriate, such that they form a heterocyclic ring with the nitrogen atom(s) carrying them.
摘要翻译：通过苄基氯或其卤化或烷基化衍生物与碱金属甲基丙烯酸酯的反应制备甲基丙烯酸苄基酯及其卤代或烷基化脱乙烯的方法的特征在于反应在不多于基于苄基氯或衍生物的叔胺为3摩尔％以上。碱金属特别选自锂，钾和钠。叔胺优选为通式如下的叔胺：其中n为1至10的整数，且R 1，R 2，R 3和R 4为相同或不同的烷基，环烷基或芳基含有1至12个碳原子的基团，如果合适的话可以官能化，如果合适的话，它们与携带它们的氮原子形成杂环。

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