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    • 2. 发明授权
    • Capillary column sealing technique
    • 毛细管柱密封技术
    • US06709027B2
    • 2004-03-23
    • US09791332
    • 2001-02-23
    • David Rittenhouse
    • David Rittenhouse
    • F16L2106
    • G01N30/6034G01N30/10
    • A method and apparatus for creating a fluid tight seal between a capillary column and a connector. The method and apparatus are easy to employ and do not require the use of screws, ferrules, or additional tools. The method can be used for any capillary tubing as well as for megabore and microbore columns and tubing. In the method, a length of auxiliary tubing is placed over the outside of tubing requiring a fluid tight seal, such as a capillary column. After the capillary column is inserted into the connector, the length of auxiliary tubing is press-fit into the connector creating a secondary fluid tight seal. The auxiliary tubing provides additional mechanical stability during mechanical vibration and dramatically increases the tensile force required to compromise the fluid seal. This method can be used for many types of chromatography including gas chromatography and liquid chromatography. A connector assembly and fluid tight seal assembly are also disclosed.
    • 一种用于在毛细管柱和连接器之间产生流体密封的方法和装置。 该方法和设备易于使用,并且不需要使用螺钉,套圈或附加工具。 该方法可用于任何毛细管,以及大孔和微孔柱和管道。 在该方法中,将一段辅助管道置于需要流体密封的管道外侧,例如毛细管柱。 将毛细管柱插入连接器后,辅助管道的长度压配合到连接器中,形成二次流体密封。 辅助管道在机械振动期间提供额外的机械稳定性,并显着增加了损害流体密封所需的拉力。 该方法可用于多种色谱法,包括气相色谱和液相色谱法。 还公开了连接器组件和流体密封组件。