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    • 4. 发明授权
    • Method for determining oil and water saturation of core samples at
overburden pressure
    • 岩石样品在上覆压力下的油水饱和度测定方法
    • US5299453A
    • 1994-04-05
    • US10250
    • 1993-01-28
    • Eve S. SpruntNizar F. Djabbarah
    • Eve S. SpruntNizar F. Djabbarah
    • G01N15/08E21B49/00
    • G01N15/0893
    • A method and apparatus is provided to determine the amount of oil and water or brine in a representative core sample of reservoir rock at an overburden stress which approximates reservoir stress conditions. The core sample is initially saturated with reservoir hydrocarbon (crude oil) and aqueous fluids (water or brine). The core sample is surrounded with an elastic jacket, or sleeve, and placed in a confining pressure vessel that simulates reservoir overburden stress on the core sample. The hydrocarbon (oil) fluids and aqueous fluids (water or brine) are than extracted from the core sample with a solvent capable of dissolving both aqueous and hydrocarbon fluids. The solvent and aqueous fluids are separated from the hydrocarbon fluids by evaporation. Thereafter the aqueous fluids are separated from the solvent by extraction. The amounts of oil and aqueous fluids from the sample may be separately determined. The volume of the hydrocarbon fluids and aqueous fluids is determined from their weight and density or from direct volume measurement. For a rock sample fully saturated with a combination of oil and aqueous fluids, the total pore volume is the sum of the volumes of the two fluids and the fluid saturation is then the ratio of the fluid volume to the pore volume.
    • 提供了一种方法和装置,用于确定近似于储层应力条件的上覆层应力的储层岩石的代表性核心样品中的油和水或盐水的量。 核心样品最初饱和储层烃(原油)和含水流体(水或盐水)。 核心样品用弹性护套或套管包围,并放置在模拟压力容器中,该压力容器模拟核心样品上的储层覆盖层应力。 烃(油)流体和含水流体(水或盐水)不是用能够溶解水和烃流体的溶剂从芯样品中提取的。 通过蒸发将溶剂和含水流体与烃流体分离。 此后,通过萃取将含水流体与溶剂分离。 来自样品的油和水溶液的量可以单独测定。 烃流体和含水流体的体积由其重量和密度或直接体积测量确定。 对于完全饱和油和含水流体的岩石样品,总孔体积是两种流体体积的总和,而流体饱和度则是流体体积与孔体积之比。
    • 6. 发明授权
    • Method for desaturating a porous rock for electrical resistivity
measurements
    • 多孔岩石去饱和电阻率测量方法
    • US5209104A
    • 1993-05-11
    • US824268
    • 1992-01-23
    • Samuel H. CollinsEve S. Sprunt
    • Samuel H. CollinsEve S. Sprunt
    • G01N33/24
    • G01N33/241
    • A porous rock is saturated with a first fluid and electrical resistivity is measured along its length. A second fluid, immiscible with the first fluid, is injected into the porous rock at a first flow rate. This injection continues until displacement of the first fluid from the porous rock ceases and the pressure drop along the porous rock becomes constant, indicating a first residual fluid saturation equilibrium. The foregoing is repeated for a plurality of increasing second fluid injection flow rates to effect electrical resistivity measurements at decreasing residual fluid saturation equilibriums. The method may then be repeated substituting the second fluid for the first and vice versa to perform an imbibition experiment.
    • 多孔岩石被第一流体饱和,并沿其长度测量电阻率。 与第一流体不混溶的第二流体以第一流速注入多孔岩石中。 该喷射继续进行,直到来自多孔岩石的第一流体的位移停止,并且沿着多孔岩石的压降变得恒定,表明第一残余液体饱和平衡。 对于多个增加的第二流体喷射流速重复上述以在降低的残余流体饱和平衡时实现电阻率测量。 然后可以重复该方法将第二流体替换为第一流体,反之亦然,以执行吸入实验。
    • 7. 发明授权
    • Method for determining lithological characteristics of a porous material
    • 确定多孔材料的岩性特征的方法
    • US4688238A
    • 1987-08-18
    • US868487
    • 1986-05-30
    • Eve S. SpruntNeil V. HumphreysErnest L. MueggeJames R. Dixon, Jr.
    • Eve S. SpruntNeil V. HumphreysErnest L. MueggeJames R. Dixon, Jr.
    • G01N15/08G01N23/04G01N23/00
    • G01N23/046G01N15/08G01N2223/419
    • A substantially cylindrical sample of a porous material is surrounded by an elastic jacket and placed in a confining pressure cell. Pressure is supplied to the cell to press the jacket into contact with the surface of the sample. The pressure is varied over a plurality of pressure points and is scanned at a plurality of locations with X-rays at each such pressure point. A computed tomographic image is produced for each X-ray scan. Conformance of the jacket to the sample is determined from these computed tomographic images and a range of confining pressure is determined over which parameters of the sample may be measured without being affected by improper conformance of the jacket to the surface of the sample. The sample structure is monitored with these tomographic images for fractures produced due to the increase of pressure. The fracture starting point is determined to be interior or surface related.
    • 多孔材料的基本上圆柱形的样品由弹性护套包围并放置在围压压力池中。 将压力供应到电池以将夹套压紧到样品的表面。 压力在多个压力点上变化,并且在每个这样的压力点处的X射线的多个位置处被扫描。 为每个X射线扫描产生计算机断层图像。 从这些计算机断层图像确定护套与样品的一致性,并且确定可以测量样品的哪些参数而不受套件与样品表面的不适当一致性的影响的范围的限制压力范围。 用这些断层图像监测样品结构,用于由于压力的增加而产生的裂缝。 断裂起点被确定为内部或表面相关。
    • 8. 发明授权
    • Method for measuring wettability of porous rock
    • 测量多孔岩石润湿性的方法
    • US5069065A
    • 1991-12-03
    • US641965
    • 1991-01-16
    • Eve S. SpruntSamuel H. Collins
    • Eve S. SpruntSamuel H. Collins
    • G01N13/00G01N33/24
    • G01N33/241G01N13/00
    • A core sample of a porous rock having a wettability representative of a subterranean formation is saturated with a first medium. This first medium is then displaced with an immiscible second medium. Capillary pressure versus wetting phase saturation is measured during the displacement of the first medium with the second medium within the core sample. Mercury is injected into an evacuated core sample of the porous rock, mercury vapor acting as a wetting phase on the porous rock. Capillary pressure versus wetting phase saturation is measured during mercury injection on the evacuated core sample. The ratio of the two capillary pressure versus wetting phase saturation measurements is determined and taken to be an indicator of the wettability of different size pore throats in the porous rock.
    • 具有代表地层的润湿性的多孔岩石的核心样品被第一介质饱和。 然后将该第一介质用不混溶的第二介质置换。 在第一介质与核心样品中的第二介质置换期间测量毛细管压力与润湿相饱和度。 将汞注入多孔岩石的真空芯样品中,在多孔岩石上作为润湿阶段的汞蒸气。 在抽空的芯样品上注入汞期间,测量毛细管压力与润湿相饱和度。 确定两个毛细管压力与湿相饱和度测量值的比值,并将其视为多孔岩石中不同大小孔喉的润湿性的指标。