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1. 发明授权

US4324714A Vinylidene chloride polymer microgel powder lacquer coating composition and substrates coated therewith 失效
标题翻译：偏二氯乙烯聚合物微凝胶粉末涂料组合物和涂覆的基材
公开(公告)号：US4324714A
公开(公告)日：1982-04-13
申请号：US145169
申请日：1980-04-30
申请人： Dale S. Gibbs , James F. Sinacola , Dan E. Ranck
发明人： Dale S. Gibbs , James F. Sinacola , Dan E. Ranck
IPC分类号： C09D127/08 , C09D3/74 , C08K5/15
CPC分类号： C09D127/08
摘要： A lacquer coating composition containing a crosslinked vinylidene chloride polymer microgel powder which is recovered from a latex obtained by emulsion polymerizing about 85 to 92 parts by weight of vinylidene chloride, about 8 to 15 parts by weight of a copolymerizable ethylenically unsaturated comonomer, and a minor amount of a copolymerizable crosslinking polyfuntional comonomer. Coatings prepared from such lacquers have excellent barrier and heat-sealing properties.
摘要翻译：一种漆涂料组合物，其含有交联的偏二氯乙烯聚合物微凝胶粉末，其由通过乳液聚合得到的胶乳回收，所述胶乳通过乳液聚合约85至92重量份的偏二氯乙烯，约8至15重量份的可共聚的烯键式不饱和共聚单体和次要可共聚的交联多官能共聚单体的量。由这种漆制备的涂料具有优异的阻隔性和热封性。

2. 发明授权

US4225407A Cathodic electrodeposition of polymers onto a conductive surface 失效
标题翻译：将聚合物阴极电沉积到导电表面上
公开(公告)号：US4225407A
公开(公告)日：1980-09-30
申请号：US26720
申请日：1979-04-04
申请人： Earl H. Wagener , Ritchie A. Wessling , Dale S. Gibbs
发明人： Earl H. Wagener , Ritchie A. Wessling , Dale S. Gibbs
IPC分类号： C09D5/44 , C25D13/22 , C25D13/06 , C25D13/10
CPC分类号： C25D13/22 , C09D5/44
摘要： A method for electrodeposition of an organic material on an electroconductive surface comprising placing the electroconductive surface to be coated in contact with an aqueous dispersion containing a water-insoluble, essentially electrically nonconductive, film-forming, organic polymer as cation-active particles wherein the cation-activity is provided at least predominantly by reducible nitrogen-containing cations and passing an electric current from an electrode through the latex to the electroconductive surface in such a direction that the electroconductive surface is negatively charged, i.e., becomes a cathode in an electrophoretic cell. By use of alternating current, both electrodes become coated with an adherent coating of polymer.
摘要翻译：一种用于在导电表面上电沉积有机材料的方法，包括将要涂覆的导电表面放置在与包含不溶于水的基本上不导电的成膜有机聚合物的水性分散体接触，所述有机材料作为阳离子活性颗粒，其中所述阳离子至少主要是通过可还原的含氮阳离子提供活性，并使电流从电极通过胶乳到导电表面，使得导电表面带负电，即在电泳池中成为阴极。通过使用交流电，两个电极都涂覆有聚合物的粘附涂层。

3. 发明授权

US4575529A Dispersible vinylidene chloride polymer powders as additives for polymers 失效
标题翻译：可分散偏氯乙烯聚合物粉末作为聚合物的添加剂
公开(公告)号：US4575529A
公开(公告)日：1986-03-11
申请号：US312566
申请日：1981-10-19
申请人： Dale S. Gibbs , Jack H. Benson , Reet T. Fernandez
发明人： Dale S. Gibbs , Jack H. Benson , Reet T. Fernandez
IPC分类号： C08F214/08 , C08J3/11 , C08J9/00 , C08G18/06
CPC分类号： C08J9/0061 , C08F214/08 , C08J3/11 , C08J2327/08 , C08J2375/04 , C08J2427/00
摘要： A vinylidene chloride polymer powder, having a second order transition temperature of at least about 50.degree. C., is recovered from a latex and dispersed with moderate shear in a non-solvent for vinylidene chloride polymers, such as a polyol used in the preparation of polyurethane materials. A dispersion of the powder and a polyol is eminently suitable for use in the preparation of polyurethane foams to impart enhanced flame retardancy and load-bearing properties thereto.
摘要翻译：具有至少约50℃的二级转变温度的偏二氯乙烯聚合物粉末从胶乳中回收并在中等剪切下分散在用于偏二氯乙烯聚合物的非溶剂中，例如用于制备聚氨酯材料。粉末和多元醇的分散体非常适用于制备聚氨酯泡沫以赋予其更好的阻燃性和承载性能。

4. 发明授权

US4225406A Cationic deposition of polymers onto a conductive surface 失效
标题翻译：将聚合物阳离子沉积到导电表面上
公开(公告)号：US4225406A
公开(公告)日：1980-09-30
申请号：US587472
申请日：1975-06-16
申请人： Earl H. Wagener , Ritchie A. Wessling , Dale S. Gibbs
发明人： Earl H. Wagener , Ritchie A. Wessling , Dale S. Gibbs
IPC分类号： C09D5/44 , C25D13/06
CPC分类号： C09D5/4488
摘要： A method for electrodeposition of an organic material on an electroconductive surface comprising placing the electroconductive surface to be coated in contact with an aqueous dispersion containing a water-insoluble, essentially electrically non-conductive, film-forming, organic polymer as cation-active particles wherein the cation-activity is provided at least predominantly by sulfonium cations and passing an electric current from an electrode through the latex to the electroconductive surface in such a direction that the electroconductive surface is negatively charged, i.e., becomes a cathode in an electrophoretic cell. By use of alternating current both electrodes become coated with the polymer.
摘要翻译：一种用于在导电表面上电沉积有机材料的方法，包括将待涂覆的导电表面放置在与包含不溶于水的基本上不导电的成膜有机聚合物的水性分散体接触，所述有机材料作为阳离子活性颗粒，其中阳离子活性至少主要由锍阳离子提供，并将电流从电极通过胶乳传递到导电表面，使得导电表面带负电，即在电泳池中成为阴极。通过使用交流电，两个电极都被聚合物涂覆。

5. 发明授权

US3994792A Electrodeposition of sulfoxonium stabilized colloids 失效
标题翻译：氧化铌稳定胶体的电沉积
公开(公告)号：US3994792A
公开(公告)日：1976-11-30
申请号：US554382
申请日：1975-03-03
申请人： Earl H. Wagener , Dale S. Gibbs , Ritchie A. Wessling
发明人： Earl H. Wagener , Dale S. Gibbs , Ritchie A. Wessling
IPC分类号： C09D5/44 , C25D13/06
CPC分类号： C09D5/4407 , C09D5/4403
摘要： A method for electrodeposition of an organic material on an electroconductive surface comprising placing the electroconductive surface to be coated in contact with an aqueous dispersion containing a water-insoluble, essentially electrically non-conductive, film-forming, organic polymer as cation-active particles wherein a substantial portion of the cation-activity is provided by sulfoxonium cations and passing an electric current from an electrode through the latex to the electroconductive surface in such a direction that the electroconductive surface is negatively charged, i.e., becomes a cathode in an electrophoretic cell. By use of alternating current both electrodes become coated with an adherent coating of polymer.
摘要翻译：一种用于在导电表面上电沉积有机材料的方法，包括将待涂覆的导电表面放置在与包含不溶于水的基本上不导电的成膜有机聚合物的水性分散体接触，所述有机材料作为阳离子活性颗粒，其中阳离子活性的很大一部分由氧化锍阳离子提供，并将电流从电极通过胶乳传递到导电表面，使得导电表面带负电，即在电泳池中成为阴极。通过使用交流电，两个电极都涂覆有聚合物的粘附涂层。

6. 发明授权

US4451632A High vinylidene chloride content interpolymer coating resins and method of preparation 失效
标题翻译：高偏二氯乙烯含量互聚物涂料树脂及其制备方法
公开(公告)号：US4451632A
公开(公告)日：1984-05-29
申请号：US395442
申请日：1982-07-06
申请人： Dale S. Gibbs , Warren L. Treptow
发明人： Dale S. Gibbs , Warren L. Treptow
IPC分类号： C08F214/08 , C08F14/08
CPC分类号： C08F214/08
摘要： A process for preparing, in aqueous emulsion, controlled interpolymer compositions. The interpolymer compositions have polymerized therein from about 86 to 92 mole percent, vinylidene chloride, from about 14 to 8 mole percent of a comonomer mixture of methyl methacrylate and a comonomer selected from the group consisting of acrylonitrile, methacrylic acid and methacrylonitrile in a ratio of the comonomer to methyl methacrylate of from about 0.5:1 to 2:1, and from about 0.5 to 1.0 weight percent itaconic acid, based on weight of vinylidene chloride plus comonomer mixture. The interpolymers are prepared in a three step process. The third step, or Step III, wherein monomer feeding is step-wise reduced for a portion of the step and a polymerization initiator is added at generally the same constant rate as the rate of addition in Steps I and II, generally reduces the amount of unreacted mixed monomers remaining after monomer addition is completed. As such, the detrimental results produced when a large amount of polymer composition variation in the direction of high vinylidene chloride fractions are markedly reduced.
摘要翻译：在水乳液中制备控制互聚物组合物的方法。互聚物组合物在其中聚合约86至92摩尔％偏二氯乙烯，约14至8摩尔％的甲基丙烯酸甲酯和选自丙烯腈，甲基丙烯酸和甲基丙烯腈的共聚单体混合物的比例为基于偏二氯乙烯加共聚单体混合物的重量，共聚单体为甲基丙烯酸甲酯的约0.5:1至2:1，以及约0.5至1.0重量％的衣康酸。互聚物以三步法制备。第三步骤或步骤III，其中步骤中单体进料逐步还原，并且聚合引发剂以与步骤I和II中的加入速率基本相同的恒定速率加入，通常减少单体添加后剩余的未反应的混合单体完成。因此，当高偏二氯乙烯部分的方向上的大量聚合物组合物变化显着降低时产生的有害结果。

7. 发明授权

US4296013A Vinylidene chloride polymer microgels 失效
标题翻译：偏二氯乙烯聚合物微凝胶
公开(公告)号：US4296013A
公开(公告)日：1981-10-20
申请号：US103020
申请日：1979-12-13
申请人： Dale S. Gibbs
发明人： Dale S. Gibbs
IPC分类号： C08F214/08 , C09D127/08 , C08L27/08
CPC分类号： C09D127/08 , C08F214/08
摘要： Discrete, crosslinked vinylidene chloride polymer microgels, having a latex particle size of less than 1 micron and a gel content of about 1 to 99 percent, such microgels being obtained by emulsion polymerizing (a) about 50 to about 95 parts by weight of vinylidene chloride, (b) about 5 to about 50 parts by weight of a copolymerizable ethylenically unsaturated comonomer, and (c) about 0.1 to about 10 parts by weight of a copolymerizable crosslinking polyfunctional comonomer. Such microgels have been found to have wide applicability as additives for synthetic foams and fibers, and for the preparation of improved coatings, films, and redispersible latexes.
摘要翻译：离散的交联偏二氯乙烯聚合物微凝胶，其胶乳粒度小于1微米，凝胶含量为约1至99％，这种微凝胶通过乳液聚合（a）约50至约95重量份的偏二氯乙烯，（b）约5至约50重量份的可共聚烯属不饱和共聚单体，和（c）约0.1至约10重量份可共聚的交联多官能共聚单体。已经发现这种微凝胶作为合成泡沫和纤维的添加剂具有广泛的适用性，并且用于制备改进的涂料，膜和可再分散的胶乳。

8. 发明授权

US4273901A Dispersible vinylidene chloride polymer microgel powders as additives for polymers 失效
标题翻译：可分散偏氯乙烯聚合物微凝胶粉末作为聚合物的添加剂
公开(公告)号：US4273901A
公开(公告)日：1981-06-16
申请号：US91281
申请日：1979-11-05
申请人： Dale S. Gibbs , Jack H. Benson , Reet T. Fernandez
发明人： Dale S. Gibbs , Jack H. Benson , Reet T. Fernandez
IPC分类号： C08F214/08 , C08J3/11 , C08J9/00 , C08L75/00 , C08K5/05 , C08G18/06 , C08K5/13
CPC分类号： C08J9/0061 , C08F214/08 , C08J3/11 , C08L75/00 , C08J2327/08 , C08J2375/04 , C08J2427/00
摘要： A crosslinked vinylidene chloride polymer microgel powder is recovered from a latex and dispersed with moderate shear in a nonsolvent for vinylidene chloride polymers, such as a polyol used in the preparation of polyurethane materials. A dispersion of the powder and a polyol is eminently suited for use in the preparation of polyurethane foams to impart enhanced flame-retardancy and load-bearing properties thereto.
摘要翻译：从胶乳中回收交联的偏二氯乙烯聚合物微粒凝胶粉末，并用中等剪切分散在偏二氯乙烯聚合物的非溶剂中，例如用于制备聚氨酯材料的多元醇。粉末和多元醇的分散体非常适合用于制备聚氨酯泡沫以赋予其更好的阻燃性和承载性能。

9. 发明授权

US4017442A Structured-particle latexes 失效
标题翻译：结构粒子胶乳
公开(公告)号：US4017442A
公开(公告)日：1977-04-12
申请号：US569724
申请日：1975-04-21
申请人： Dale S. Gibbs , Earl H. Wagener , Ritchie A. Wessling
发明人： Dale S. Gibbs , Earl H. Wagener , Ritchie A. Wessling
IPC分类号： C08C1/06 , C08F291/00 , C08L33/08
CPC分类号： C08C1/06 , C08F291/00
摘要： Structured-particle latexes are prepared from nonionic or slightly cationic latexes, either preformed or polymerized in situ, by emulsion polymerizing monomeric materials which include an ethylenically unsaturated, activated-halogen monomer such as vinylbenzyl chloride in the absence of a sufficient amount of a surfactant to initiate new particles whereby the activated-halogen monomer is copolymerized on the surface of the existing particles which are dispersed in aqueous media. To the resulting structured particle latex may then be added conventional cationic surfactants to provide greater stability. The cationic latexes are suitable for coatings.
摘要翻译：通过在不存在足够量的表面活性剂的情况下通过乳液聚合包括烯属不饱和的活性卤素单体如乙烯基苄基氯的单体材料，由非离子或微阳离子胶乳制备结构粒子胶乳，引发新的颗粒，由此活性卤素单体在分散在水性介质中的现有颗粒的表面上共聚。然后可以向得到的结构化颗粒胶乳中加入常规阳离子表面活性剂以提供更大的稳定性。阳离子胶乳适用于涂料。

10. 发明授权

US4255306A Vinylidene chloride polymer microgels 失效
公开(公告)号：US4255306A
公开(公告)日：1981-03-10
申请号：US942515
申请日：1978-09-15
申请人： Dale S. Gibbs
发明人： Dale S. Gibbs
IPC分类号： C08F214/00 , C08F2/00 , C08F2/22 , C08F14/00 , C08F214/08 , C09D127/08 , C08F14/08 , C08F114/08
CPC分类号： C08F214/08 , C09D127/08
摘要： Discrete, crosslinked vinylidene chloride polymer microgels, having a latex particle size of less than 1 micron and a gel content of about 1 to 99 percent, such microgels being obtained by emulsion polymerizing (a) about 50 to about 95 parts by weight of vinylidene chloride, (b) about 5 to about 50 parts by weight of a copolymerizable ethylenically unsaturated comonomer, and (c) about 0.1 to about 10 parts by weight of a copolymerizable crosslinking polyfunctional comonomer. Such microgels have been found to have wide applicability as additives for synthetic foams and fibers, and for the preparation of improved coatings, films, and redispersible latexes.

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