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1. 发明授权

US06302994B1 Process for producing labeled article 失效
标题翻译：制作标签制品的方法
公开(公告)号：US06302994B1
公开(公告)日：2001-10-16
申请号：US09242098
申请日：1999-02-08
申请人： Daisuke Kamiya , Kiyokazu Mizutani , Yoichi Kirito , Akemi Koketsu , Makoto Niwa , Kotaro Yoneda , Hiroshi Iesako , Hitoshi Kato
发明人： Daisuke Kamiya , Kiyokazu Mizutani , Yoichi Kirito , Akemi Koketsu , Makoto Niwa , Kotaro Yoneda , Hiroshi Iesako , Hitoshi Kato
IPC分类号： B65C1106
CPC分类号： G09F3/10
摘要： A process for producing an article with a label, which comprises attaching, to an article, a heat-sensitive and pressure-sensitive adhesive label having an adhesive layer composed of a pressure-sensitive adhesive composition, which is an aqueous emulsion type composition comprising: (A) a water-soluble resin obtained by neutralizing a resin having an acid value of 1 meq/g or more, with a base, and (B) a polymer having an acid value of 0.6 meq/g or less and a glass transition temperature of −20° C. or lower, obtained by emulsion polymerization of a radical-polymerizable monomer, and which, when made into an aqueous film and dried at a temperature lower than 60° C., becomes a film (1) of two-phase structure wherein particles composed of the component (B) are dispersed in a continuous phase composed of the component (A) and, when the film (1) is heated to a temperature of 60° C. or higher, is converted into a pressure-sensitive adhesive film (2) wherein the forms of the component (A) and the component (B) in the above two-phase structure are reversed and particles of the component (A) are dispersed in a continuous phase of the component (B).
摘要翻译：一种用于生产具有标签的制品的方法，其包括将具有由压敏粘合剂组合物构成的粘合剂层的热敏和压敏粘合剂标签附着到制品上，所述粘合剂层是水性乳液型组合物，其包含：（A）通过用碱将酸值为1meq / g以上的树脂中和得到的水溶性树脂，（B）酸值为0.6meq / g以下的聚合物和玻璃化转变温度温度为-20℃以下，通过自由基聚合性单体的乳液聚合而得到，并且当制成水性膜并在低于60℃的温度下干燥时，成为两层的膜（1）相组合，其中由组分（B）组成的颗粒分散在由组分（A）组成的连续相中，并且当膜（1）被加热至60℃或更高的温度时，转化为压敏粘合剂膜（2），其中组分（A）的形式和上述两相结构中的组分（B）相反，并且组分（A）的颗粒分散在组分（B）的连续相中。

2. 发明授权

US4849529A Method for production of spiro-orthocarbonate 失效
标题翻译：螺 - 原碳酸酯的生产方法
公开(公告)号：US4849529A
公开(公告)日：1989-07-18
申请号：US4401
申请日：1987-01-20
申请人： Kiyokazu Mizutani , Hitoshi Kato , Kuniko Ogasawara , Takeshi Endo
发明人： Kiyokazu Mizutani , Hitoshi Kato , Kuniko Ogasawara , Takeshi Endo
IPC分类号： C07D493/10
CPC分类号： C07D493/10
摘要： A method for producing spiro-orthocarbonate compounds is disclosed. The method comprises reacting a cyclic carbonate compound of the following formula with an epoxy compound containing an epoxy group: ##STR1## wherein R is an alkylene group or a substituted alkylene group. The disclosed method makes it easy to commercially produce spiro-orthocarbonate compounds in a one stage reaction. The starting materials can be easily handled without any hygienic difficulties and the method can be carried out without entailing any operational difficulties.
摘要翻译：公开了一种生产螺 - 原碳酸酯化合物的方法。该方法包括使下式的环状碳酸酯化合物与含有环氧基的环氧化合物反应：其中R是亚烷基或取代的亚烷基。所公开的方法使得在一步反应中容易商业生产螺原碳酸酯化合物。起始原料易于处理，无任何卫生困难，可以在不引起任何操作困难的情况下进行。

3. 发明授权

US4870193A Process for producing spiro-orthocarbonate 失效
标题翻译：生产螺 - 原碳酸酯的方法
公开(公告)号：US4870193A
公开(公告)日：1989-09-26
申请号：US771915
申请日：1985-09-03
申请人： Hiromu Taguchi , Kiyokazu Mizutani , Hiroyuki Kato , Takeshi Endo
发明人： Hiromu Taguchi , Kiyokazu Mizutani , Hiroyuki Kato , Takeshi Endo
IPC分类号： C07D493/08 , C07D319/00 , C07D493/10 , C08G65/16
CPC分类号： C07D493/10
摘要： A process for producing spiro-orthocarbonate having glycol unit (2) is described, which comprises reacting a spiro-orthocarbonate having glycol unit (1) which is different from glycol unit (2), with a glycol having glycol unit (2) to release a glycol having glycol unit (1).
摘要翻译：描述了一种生产具有二醇单元（2）的螺 - 原碳酸酯的方法，其包括使具有与二醇单元（2）不同的二醇单元（1）的螺 - 原碳酸酯与具有二醇单元（2）的二元醇反应以使其释放具有二醇单元（1）的二醇。

4. 发明授权

US4368314A Curable composition comprising spiro-orthoester compound 失效
标题翻译：包含螺 - 原酸酯化合物的可固化组合物
公开(公告)号：US4368314A
公开(公告)日：1983-01-11
申请号：US295739
申请日：1981-08-24
申请人： Takeshi Endo , Kiyokazu Mizutani , Takahisa Ogasawara
发明人： Takeshi Endo , Kiyokazu Mizutani , Takahisa Ogasawara
IPC分类号： C07D493/10 , C08G59/14 , C08G59/42 , C08G59/62 , C08G59/68 , C08G63/40 , C08G63/66 , C08G59/26 , C08G63/42
CPC分类号： C07D493/10 , C08G59/1438 , C08G59/4284 , C08G59/625 , C08G59/68 , C08G63/40 , C08G63/66
摘要： A curable composition comprising:(A) at least one spiro-orthoester compound having at least one spiro-orthoester group represented by the formula: [I] ##STR1## wherein n is an integer of 3-5, (B) at least one curing agent selected from the group consisting of organic polybasic acids and their anhydrides,(C) optionally, an epoxy compound having at least one epoxy group, and(D) optionally a cationic polymerization catalyst when the composition comprises ingredient (C).Said composition is small in shrinkage on curing, and provides a cured product of high dimensional accuracy when used as a molding material.
摘要翻译：一种可固化组合物，其包含：（A）至少一种具有至少一个由下式表示的螺原酸酯基团的螺 - 原酸酯化合物：其中n是3-5的整数，（B）至少一种选自有机多元酸及其酸酐的固化剂，（C）任选的具有至少一个环氧基的环氧化合物，和（D）任选的阳离子聚合催化剂，当组合物包含成分（C）。所述组合物在固化时的收缩率小，并且当用作模塑材料时提供高尺寸精度的固化产品。

5. 发明授权

US4370387A Pre-coated steel sheets and process for production thereof 失效
标题翻译：预涂钢板及其制造方法
公开(公告)号：US4370387A
公开(公告)日：1983-01-25
申请号：US245307
申请日：1981-03-19
申请人： Nagaharu Ueno , Joji Oka , Hidejiro Asano , Takahisa Ogasawara , Kiyokazu Mizutani , Yoshiitsu Tominaga
发明人： Nagaharu Ueno , Joji Oka , Hidejiro Asano , Takahisa Ogasawara , Kiyokazu Mizutani , Yoshiitsu Tominaga
IPC分类号： B05D7/14 , B05D3/06 , C08F299/04 , C08G63/47 , C09D5/00 , C09D167/06 , B32B9/06
CPC分类号： C08F299/0492 , C08G63/47 , C09D167/06 , Y10T428/31681
摘要： A precoated steel sheet and a process for production thereof is provided which comprises coating a resin composition comprising mainly an acryloxyloxy- or methacryloyloxy-terminated polyester on the surface of a steel sheet, said acryloyloxy- or methacryloyloxy-terminated polyester being prepared by reacting a hydroxy-terminated polyester comprising (a) a dicarboxylic acid unit containing about 10 to about 80 mol % of a terephthalic acid unit and (b) dihydric alcohol unit containing about 30 mol % or more of a dihydric alcohol unit containing 3 or more carbon atoms, and having a number average molecular weight of about 400 to about 5,000, with acrylic acid or methacrylic acid, and curing the thus-coated resin composition by irradiating the sheet with an electron beam.
摘要翻译：提供预涂钢板及其制造方法，其包括在钢板表面上涂覆主要包含丙烯酰氧基氧基或甲基丙烯酰氧基封端的聚酯的树脂组合物，所述丙烯酰氧基或甲基丙烯酰氧基封端的聚酯通过使羟基（a）含有约10〜约80摩尔％的对苯二甲酸单元的二羧酸单元和（b）含有约30摩尔％以上含有3个以上碳原子的二元醇单元的二元醇单元，并且用丙烯酸或甲基丙烯酸将数均分子量为约400至约5,000，并通过用电子束照射该片来固化如此涂覆的树脂组合物。

6. 发明授权

US4330643A Process for production of acryloyloxy- or methacryloyloxy-terminated polyesters 失效
标题翻译：丙烯酰氧基或甲基丙烯酰氧基封端的聚酯的制备方法
公开(公告)号：US4330643A
公开(公告)日：1982-05-18
申请号：US237054
申请日：1981-02-23
申请人： Takahisa Ogasawara , Kiyokazu Mizutani
发明人： Takahisa Ogasawara , Kiyokazu Mizutani
IPC分类号： C08F299/00 , C08F290/00 , C08G63/00 , C08G63/12 , C08G63/47 , C08G63/91 , C09D4/02 , C08G63/18
CPC分类号： C08G63/918 , C08G63/47
摘要： A process for production of an acryloyloxy- or methacryloyloxy-terminated polyester is described, which comprises reacting a specific hydroxy-terminated polyester with acrylic acid or methacrylic acid, wherein the hydroxy-terminated polyester comprises (a) a dicarboxylic acid unit comprising about 10 to about 80 mol % of a terephthalic acid unit and about 90 to about 20 mol % of another dicarboxylic acid unit and (b) a dihydric alcohol unit containing about 30 mol % or more of a dihydric alcohol unit containing 3 or more carbon atoms and having a number average molecular weight of about 400 to about 5,000.
摘要翻译：描述了制备丙烯酰氧基或甲基丙烯酰氧基封端的聚酯的方法，其包括将特定的羟基封端的聚酯与丙烯酸或甲基丙烯酸反应，其中羟基封端的聚酯包含（a）二羧酸单元，其包含约10〜约80摩尔％的对苯二甲酸单元和约90至约20摩尔％的另外的二羧酸单元和（b）含有约30摩尔％以上的含有3个或更多个碳原子的二元醇单元的二元醇单元，并且具有数均分子量为约400至约5,000。

7. 发明授权

US4425473A Polymerizable bicyclic orthoester compounds 失效
标题翻译：可聚合双环原酸酯化合物
公开(公告)号：US4425473A
公开(公告)日：1984-01-10
申请号：US230537
申请日：1981-02-02
申请人： Kiyokazu Mizutani , Takahisa Ogasawara
发明人： Kiyokazu Mizutani , Takahisa Ogasawara
IPC分类号： C07D493/08 , C08G71/04 , C07D319/14
CPC分类号： C07D493/08 , C08G71/04
摘要： Certain new derivatives of 2,6,7-trioxabicyclo[2,2,2]octane are found to undergo cationic ring-opening polymerization with positive expansion in volume or with no substantial change in volume, in contrast with known polymerizable compounds such as epoxides which present considerable shrinkage in volume on polymerization. These new bicyclic orthoester compounds can be prepared in a facile way known per se.
摘要翻译：发现2,6,7-三氧杂双环[2,2,2]辛烷的某些新衍生物与已知的可聚合化合物如环氧化物相比，体积正膨胀或体积没有显着变化，进行阳离子开环聚合其在聚合时呈现相当大的体积收缩。这些新的双环原酸酯化合物可以以本身已知的简便方式制备。

8. 发明授权

US4338240A Curable material and process for production thereof 失效
标题翻译：可固化材料及其生产方法
公开(公告)号：US4338240A
公开(公告)日：1982-07-06
申请号：US276488
申请日：1981-06-23
申请人： Kiyokazu Mizutani , Takahisa Ogasawara
发明人： Kiyokazu Mizutani , Takahisa Ogasawara
IPC分类号： C08G18/00 , C08G18/28 , C08G18/30 , C08G18/32 , C08G18/65 , C08G18/83 , C08G65/00 , C08G65/04 , C08G65/16
CPC分类号： C08G18/2815 , C08G18/83
摘要： A curable urethane material which shows no change in volume on polymerization and curing is prepared from polyisocyanate compound, polyhydroxy compound and a new compound 1-alkyl-4-hydroxymethyl-2,6,7-trioxabicyclo[2,2,2]octane.
摘要翻译：由聚异氰酸酯化合物，多羟基化合物和新化合物1-烷基-4-羟甲基-2,6,7-三氧杂双环[2,2,2]辛烷制备聚合和固化时体积无变化的可固化聚氨酯材料。

9. 发明授权

US4332731A 2-Methylene-1,4,6-trioxaspiro[4,6]undecane, process for the preparation thereof and process for the preparation of polymers 失效
标题翻译： 2-亚甲基-1,4,6-三氧杂螺[4,6]十一烷，其制备方法和制备聚合物的方法
公开(公告)号：US4332731A
公开(公告)日：1982-06-01
申请号：US188267
申请日：1980-09-17
申请人： Takeshi Endo , Takahisa Ogasawara , Kiyokazu Mizutani
发明人： Takeshi Endo , Takahisa Ogasawara , Kiyokazu Mizutani
IPC分类号： C07D493/10 , C08G63/06 , C08G65/02 , C07D317/02
CPC分类号： C07D493/10 , C08G63/06
摘要： Novel 2-methylene-1,4,6-trioxaspiro[4,6]undecane has both cationic polymerizability and radical ring-opening polymerizability, and it can be produced by reacting a 2-halomethyl-1,4,6-trioxaspiro[4,6]undecane with an alkali to effect dehydrohalogenation.
摘要翻译：新型2-亚甲基-1,4,6-三氧杂螺[4,6]十一烷具有阳离子聚合性和自由基开环聚合性，可以通过2-卤代甲基-1,4,6-三氧杂螺[4 ，6]十一烷与碱进行脱卤化氢反应。

10. 发明授权

US3935173A Curable compositions 失效
标题翻译：可固化组合物
公开(公告)号：US3935173A
公开(公告)日：1976-01-27
申请号：US452266
申请日：1974-03-18
申请人： Takahisa Ogasawara , Yorimasa Kobayashi , Kiyokazu Mizutani , Teruo Nakagawa , Noboru Hisanaga , Hidemaro Tatemichi
发明人： Takahisa Ogasawara , Yorimasa Kobayashi , Kiyokazu Mizutani , Teruo Nakagawa , Noboru Hisanaga , Hidemaro Tatemichi
IPC分类号： C08F2/00 , C08F2/48 , C08F2/54 , C08F20/20 , C08F290/00 , C08F299/00 , C09D167/07 , C08F220/20 , C08F222/12 , C08G63/52
CPC分类号： C08F20/20
摘要： A low viscous and solvent-free curable composition comprising a polyester type oligo(meth)acrylate having a plurality of (meth)acryloyl groups, and a polyol poly(meth)acrylate.
摘要翻译：一种低粘度和无溶剂的可固化组合物，其包含具有多个（甲基）丙烯酰基的聚酯型低聚（甲基）丙烯酸酯和多元醇聚（甲基）丙烯酸酯。

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