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1. 发明授权

US3903235A Method for separating nickel from cobalt 失效
标题翻译：从钴中分离镍的方法
公开(公告)号：US3903235A
公开(公告)日：1975-09-02
申请号：US24769272
申请日：1972-04-26
申请人： DEEPSEA VENTURES INC
发明人： CARDWELL PAUL H , KANE WILLIAM S , OLANDER JAMES A
IPC分类号： C01G51/00 , C01G53/00 , C22B1/08 , C22B3/28 , C22B3/30 , C22B3/32 , C22B3/36 , C22B3/38 , C22B47/00 , C01G3/00 , C01G45/00 , C22B3/00 , C22B15/00 , C22B23/00
CPC分类号： C22B3/0037 , C01G51/003 , C01G53/003 , C22B1/08 , C22B3/001 , C22B3/0017 , C22B3/0027 , C22B3/0063 , C22B23/04 , C22B47/0081 , Y02P10/234 , Y10S423/04
摘要： A process is provided for separating nickel and cobalt; the process comprises extracting the nickel and cobalt together with a liquid ion exchange agent. Stripping the nickel from the extractant with an acidic aqueous solution and then stripping the cobalt with an aqueous solution at least 6N in hydrogen ion and in chloride ion concentration.
摘要翻译：提供了分离镍和钴的方法; 该方法包括将镍和钴与液体离子交换剂一起提取。用酸性水溶液从萃取剂中剥离镍，然后用氢离子和氯离子浓度的至少6N的水溶液汽提钴。

2. 发明授权

US3903236A Method for obtaining metal values by the halidation of a basic manganiferous ore with ferric chloride pre-treatment 失效
标题翻译：通过用氯化铁预处理使碱性锰矿矿石卤化来获得金属值的方法
公开(公告)号：US3903236A
公开(公告)日：1975-09-02
申请号：US30994972
申请日：1972-11-27
申请人： DEEPSEA VENTURES INC
发明人： MCCUTCHEON HUGH L , KANE WILLIAM S , CARDWELL PAUL H
IPC分类号： C01G3/04 , C01G45/02 , C22B1/08 , C22B3/28 , C22B3/30 , C22B3/32 , C22B3/36 , C22B3/38 , C01G45/06 , C01G49/06 , C01G51/08 , C01G53/08
CPC分类号： C22B3/0037 , C22B1/08 , C22B3/001 , C22B3/0016 , C22B3/0017 , C22B3/0027 , C22B3/0068 , C22B3/0077 , C22B23/04 , Y02P10/216 , Y02P10/234 , Y10S423/04
摘要： This invention provides an improvement in the process of obtaining metal values from manganiferous iron-containing ore by halidating the ores and separating the metal values from the ore as the halides. This improvement comprises segregating the iron halide from the mixed halides and recycling the iron halide to react with the ore prior to halidating. This process is especially applicable to ocean floor nodule ores and utilizes preferably hydrogen halides or halogens as the halidating agents, in aqueous solutions.
摘要翻译：本发明提供了通过将矿石卤化并从金属中分离金属值作为卤化物从含锰铁矿石获得金属值的方法的改进。这种改进包括将卤化铁从混合卤化物中分离出来，并在卤化物之前再循环卤化铁与矿石反应。该方法特别适用于海底结核矿石，并在水溶液中优选使用卤化氢或卤素作为卤化剂。

3. 发明授权

US3894139A Nickel-cobalt separation from aqueous solutions 失效
标题翻译：从水溶液中分离镍钴
公开(公告)号：US3894139A
公开(公告)日：1975-07-08
申请号：US33673773
申请日：1973-02-28
申请人： DEEPSEA VENTURES INC
发明人： CARDWELL PAUL H , KANE WILLIAM S , OLANDER JAMES A
IPC分类号： C22B3/28 , C22B3/30 , C22B3/32 , C22B3/36 , C22B3/38 , C22B47/00 , C01G3/00 , C01G45/00 , C01G51/00 , C01G53/00 , C22B3/00 , C22B15/00 , C22B23/00
CPC分类号： C22B3/0017 , C22B3/001 , C22B3/0027 , C22B3/0037 , C22B3/0063 , C22B47/0081 , Y02P10/234 , Y10S423/04
摘要： This invention provides a process for obtaining separate solutions of a soluble nickel salt and a soluble cobalt salt from a pregnant aqueous solution comprising a mixture of a cobalt salt and a nickel salt. The nickel and cobalt are extracted together from the pregnant solution by a liquid ion exchange extraction medium and then selectively stripped from the extract. The pregnant aqueous solution can be derived from the leaching of various ores, such as ocean floor nodule ore, or from, e.g., spent electroplating solutions or spent acid pickling liquors, containing nickel and cobalt.
摘要翻译：本发明提供从包含钴盐和镍盐的混合物的怀孕水溶液中获得可溶性镍盐和可溶性钴盐的分离溶液的方法。镍和钴通过液体离子交换提取介质从怀孕溶液中一起提取，然后从提取物中选择性剥离。怀孕的水溶液可以衍生自各种矿石的浸出，例如海底结节矿石，或来自例如含有镍和钴的废电镀溶液或废酸洗液。

4. 发明授权

US3923615A Winning of metal values from ore utilizing recycled acid leaching agent 失效
标题翻译：从利用再生酸浸剂的矿石中获取金属价值
公开(公告)号：US3923615A
公开(公告)日：1975-12-02
申请号：US37921373
申请日：1973-07-16
申请人： DEEPSEA VENTURES INC
发明人： KANE WILLIAM S , CARDWELL PAUL H
IPC分类号： C22B47/00 , C25C1/10
CPC分类号： C25C1/10 , C22B47/0063 , Y02P10/236 , Y10S423/04
摘要： This invention provides a process for selectively removing desirable metal values from an ocean floor nodule ore wherein the ore is initially leached with an aqueous solution of a mineral acid to preferentially form water-soluble salts of nickel and copper, which are dissolved in the leach solution, followed by releaching the solid leached ore under reducing conditions using a reducing reagent capable of reducing tetravalent manganese to divalent manganese and of forming water-soluble salts of cobalt and divalent manganese which are in turn dissolved into the leach solution resulting preferably in a single aqueous pregnant leach solution comprising the dissolved salts of copper, cobalt, nickel and divalent manganese. Preferably, the above four named metal values are individually separated into individual aqueous solutions which preferably are in turn reduced to the elemental metals by electrolysis procedures. The advantage of this process lies in the fact that it can utilize waste products from this and other industrial procedures. The reducing reagents, which can be used, include ferrous salts obtained from pickling procedures, and the mineral acid leach solution can be recycled as spent electrolyte from the electrolysis procedures especially that for the formation of elemental manganese.
摘要翻译：本发明提供了一种从海底结节矿选择性去除所需金属值的方法，其中矿石最初用无机酸的水溶液浸出，以优先形成溶解在浸出溶液中的镍和铜的水溶性盐，然后在还原条件下使用能够将四价锰还原为二价锰的还原剂和形成钴和二价锰的水溶性盐的溶液再次溶解在浸出溶液中，从而优选地将单一水溶液包含铜，钴，镍和二价锰的溶解盐的怀孕浸出溶液。优选地，将上述四种命名的金属值分别分离为单独的水溶液，其优选通过电解方法还原成元素金属。

5. 发明授权

US3901775A Method of ocean floor nodule treatment and electrolytic recovery of metals 失效
标题翻译：海洋地面处理方法和金属电解回收方法
公开(公告)号：US3901775A
公开(公告)日：1975-08-26
申请号：US31587872
申请日：1972-12-18
申请人： DEEPSEA VENTURES INC
发明人： KANE WILLIAM S , CARDWELL PAUL H
IPC分类号： C22B3/00 , C22B47/00 , C22D1/24 , C22D1/14 , C22D1/16
CPC分类号： C22B47/00 , C22B3/00 , C22B47/0063 , C22B47/0081 , Y02P10/234 , Y10S423/04
摘要： Method of recovering metal values from ocean floor nodules of the type containing iron, manganese, copper, cobalt, and nickel, comprising grinding the nodules into particles and mixing with a chloride-forming medium so as to obtain metal chlorides as reaction products, including vaporizing the metal chlorides into fractions, converting the iron chloride in the fractions containing iron chloride to iron oxide, directly subjecting the manganese chloride fraction to fused salt electrolysis, leaching an iron oxide-copper chloride fraction, removing iron oxide and electrolyzing so as to obtain copper value, leaching the mixture of nickel, cobalt, and manganese chlorides, and separating the nickel chloride and cobalt chloride by liquid ion exchange and electrolyzing separately, then crystallizing any remaining manganese chloride and electrolyzing.

6. 发明授权

US3894927A Recovery of metal values from ocean floor nodule ores by halidation in molten salt bath 失效
标题翻译：在熔盐浴中通过卤化从海底结核矿石中回收金属值
公开(公告)号：US3894927A
公开(公告)日：1975-07-15
申请号：US30973872
申请日：1972-11-27
申请人： DEEPSEA VENTURES INC
发明人： KANE WILLIAM S , MCCUTCHEN HUGH L , CARDWELL PAUL H
IPC分类号： C01G3/00 , C01G3/05 , C01G45/06 , C01G51/08 , C01G53/08 , C01G53/09 , C22B3/00 , C22B3/28 , C22B3/30 , C22B3/32 , C22B3/36 , C22B15/00 , C22B47/00 , C22D3/00
CPC分类号： C01G3/003 , C01G3/05 , C01G45/06 , C01G51/08 , C01G53/08 , C01G53/09 , C22B3/00 , C22B3/001 , C22B3/0017 , C22B3/0027 , C22B3/0037 , C22B15/0021 , C22B15/003 , C22B15/0082 , C22B47/00 , C22B47/0027 , C22B47/0045 , C22B47/0081 , Y02P10/234 , Y02P10/236 , Y10S423/04 , Y10S423/12
摘要： This invention provides a process for removing metal values from ocean floor nodule ores comprising contacting the nodule ore with a molten bath of an alkali metal halide and/or an alkaline earth metal halide to form the halides of the manganese, copper, cobalt and nickel present in the ore, and separating the thus formed halides from the reaction mixture, as by vaporization. The mixture of halides can then be separated into the individual halides, e.g. by dissolving in water and separating by extraction. Preferably the ore is first dehydrated and the ore can be contacted with a reducing agent to reduce the manganese present to the divalent state.
摘要翻译：本发明提供一种从海底结节矿石中去除金属值的方法，包括使结核矿石与碱金属卤化物和/或碱土金属卤化物的熔池接触以形成存在的锰，铜，钴和镍的卤化物在矿石中，并通过蒸发从反应混合物中分离由此形成的卤化物。然后将卤化物的混合物分离成单独的卤化物，例如，通过溶解在水中并通过萃取分离。

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