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1. 发明申请

US20100121078A1 PROCESS FOR PREPARING ALKANEDIOL AND DIALKYL CARBONATE 审中-公开
标题翻译：制备阿尔卡尼和碳酸二乙酯的方法
公开(公告)号：US20100121078A1
公开(公告)日：2010-05-13
申请号：US12435173
申请日：2009-05-04
申请人： Cyrille Paul Allais , Minne Boelens , Evert Van Der Heide
发明人： Cyrille Paul Allais , Minne Boelens , Evert Van Der Heide
IPC分类号： C07D317/10
CPC分类号： C07C68/065 , C07C69/96
摘要： The invention relates to a process for the preparation of an alkanediol and a dialkyl carbonate comprising: (a) reacting an alkylene carbonate and an alkanol at a temperature of from 10 to 200° C., at a pressure of from 5×104 to 5×106 N/m2 and in the absence of a transesterification catalyst, to obtain a mixture comprising hydroxyalkyl alkyl carbonate, alkanol and alkylene carbonate; (b) contacting the mixture comprising hydroxyalkyl alkyl carbonate, alkanol and alkylene carbonate with a transesterification catalyst at a temperature of from 10 to 200° C. and at a pressure of from 5×104 to 5×106 N/m2, to obtain a mixture comprising the alkanediol and the dialkyl carbonate; and (c) recovering the alkanediol and the dialkyl carbonate from the mixture comprising the alkanediol and the dialkyl carbonate.
摘要翻译：本发明涉及一种制备链烷二醇和碳酸二烷基酯的方法，包括：（a）在10至200℃的温度下，在5×10 4至5的压力下使碳酸亚烷基酯和链烷醇反应 ×106N / m 2，并且在不存在酯交换催化剂的情况下，得到包含碳酸烷基酯，链烷醇和碳酸亚烷基酯的混合物; （b）使含碳酸烷基酯，链烷醇和碳酸亚烷基酯的混合物与酯交换催化剂在10〜200℃，压力为5×10 4〜5×10 6 N / m 2下接触，得到包含链烷二醇和碳酸二烷基酯的混合物; 和（c）从包含链烷二醇和碳酸二烷基酯的混合物中回收链烷二醇和碳酸二烷基酯。

2. 发明授权

US08735607B2 Process for the production of alkylene carbonate 有权
标题翻译：碳酸亚烷基酯的制备方法
公开(公告)号：US08735607B2
公开(公告)日：2014-05-27
申请号：US12993136
申请日：2009-05-19
申请人： Cyrille Paul Allais , Evert Van Der Heide , Gerardus Martinus Maria Van Kessel
发明人： Cyrille Paul Allais , Evert Van Der Heide , Gerardus Martinus Maria Van Kessel
IPC分类号： C07D317/36 , C07D317/38
CPC分类号： C07D317/36 , C07D317/38
摘要： The invention relates to a process for the production of an alkylene carbonate by the reaction of an alkylene oxide with carbon dioxide in the presence of a phosphonium catalyst in which process (a) the alkylene oxide, carbon dioxide and phosphonium catalyst are continuously introduced into a reaction zone from which a product stream containing alkylene carbonate and phosphonium catalyst is withdrawn; (b) alkylene carbonate and a stream containing phosphoniura catalyst are separated from the product stream; (c) the alkylene carbonate, separated in step (b), is recovered as product; and (d) the stream containing phosphoniura catalyst, separated in step (b), is recycled to the reaction zone, in which process a treatment of alkylene carbonate and/or catalyst with a sorption agent comprising carbon is carried out.
摘要翻译：本发明涉及在鏻催化剂存在下，通过烯化氧与二氧化碳的反应制备碳酸亚烷基酯的方法，其中方法（a）将环氧烷，二氧化碳和鏻催化剂连续引入取出含有碳酸亚烷基酯和鏻催化剂的产物流的反应区; （b）将碳酸亚烃酯和含有膦酰氧基催化剂的物流与产物流分离; （c）在步骤（b）中分离的碳酸亚烃酯作为产物回收; 和（d）将在步骤（b）中分离的含有膦酰氧基催化剂的料流再循环到反应区，在该方法中，用含碳吸附剂处理碳酸亚烷基酯和/或催化剂。

3. 发明申请

US20110108762A1 PROCESS FOR THE PRODUCTION OF ALKYLENE CARBONATE 有权
标题翻译：生产亚烷基碳酸酯的方法
公开(公告)号：US20110108762A1
公开(公告)日：2011-05-12
申请号：US12993136
申请日：2009-05-19
申请人： Cyrille Paul Allais , Evert Van Der Heide , Gerardus Martinus Maria Van Kessel
发明人： Cyrille Paul Allais , Evert Van Der Heide , Gerardus Martinus Maria Van Kessel
IPC分类号： C07D317/36 , C09K3/00
CPC分类号： C07D317/36 , C07D317/38
摘要： The invention relates to a process for the production of an alkylene carbonate by the reaction of an alkylene oxide with carbon dioxide in the presence of a phosphonium catalyst in which process (a) the alkylene oxide, carbon dioxide and phosphonium catalyst are continuously introduced into a reaction zone from which a product stream containing alkylene carbonate and phosphonium catalyst is withdrawn; (b) alkylene carbonate and a stream containing phosphoniura catalyst are separated from the product stream; (c) the alkylene carbonate, separated in step (b), is recovered as product; and (d) the stream containing phosphoniura catalyst, separated in step (b), is recycled to the reaction zone, in which process a treatment of alkylene carbonate and/or catalyst with a sorption agent comprising carbon is carried out.
摘要翻译：本发明涉及在鏻催化剂存在下，通过烯化氧与二氧化碳的反应制备碳酸亚烷基酯的方法，其中方法（a）将环氧烷，二氧化碳和鏻催化剂连续引入取出含有碳酸亚烷基酯和鏻催化剂的产物流的反应区; （b）将碳酸亚烃酯和含有膦酰氧基催化剂的物流与产物流分离; （c）在步骤（b）中分离的碳酸亚烃酯作为产物回收; 和（d）将在步骤（b）中分离的含有膦酰氧基催化剂的料流再循环到反应区，在该方法中，用含碳吸附剂处理碳酸亚烷基酯和/或催化剂。

4. 发明授权

US08975432B2 Process for preparing alkanediol and dialkyl carbonate 有权
标题翻译：链烷二醇和碳酸二烷基酯的制备方法
公开(公告)号：US08975432B2
公开(公告)日：2015-03-10
申请号：US13509648
申请日：2010-11-15
申请人： Cyrille Paul Allais , Timothy Michael Nisbet , Garo Garbis Vaporciyan , Cornelis Leonardus Maria Vrouwenvelder
发明人： Cyrille Paul Allais , Timothy Michael Nisbet , Garo Garbis Vaporciyan , Cornelis Leonardus Maria Vrouwenvelder
IPC分类号： C07C68/06 , C07C29/48
CPC分类号： C07C68/065 , C07C69/96
摘要： The invention relates to a process for the preparation of an alkanediol and a dialkyl carbonate comprising: reacting an alkylene carbonate and an alkanol in the presence of a transesterification catalyst to obtain a reaction mixture comprising dialkyl carbonate, unconverted alkanol, alkanediol, unconverted alkylene carbonate and an alkoxy alkanol impurity; and subjecting the reaction mixture to distillation in a series of steps.
摘要翻译：本发明涉及一种制备链烷二醇和碳酸二烷基酯的方法，包括：在酯交换催化剂存在下使碳酸亚烷基酯和链烷醇反应，得到包含碳酸二烷基酯，未转化的链烷醇，链烷二醇，未转化的碳酸亚烃酯和烷氧基烷醇杂质; 并对反应混合物进行一系列步骤的蒸馏。

5. 发明申请

US20120226065A1 PROCESS FOR REMOVING AN ALKANOL IMPURITY FROM A DIALKYL CARBONATE STREAM 有权
标题翻译：从碳酸氢钠溶液中除去碱金属离子的方法
公开(公告)号：US20120226065A1
公开(公告)日：2012-09-06
申请号：US13390124
申请日：2010-08-10
申请人： Cyrille Paul Allais , Garo Garbis Vaporciyan
发明人： Cyrille Paul Allais , Garo Garbis Vaporciyan
IPC分类号： C07C69/00
CPC分类号： C07C68/08 , C07C67/03 , C07C68/06 , C07C69/96 , C07C69/86
摘要： The invention relates to a process for removing an alkanol impurity from a stream containing a dialkyl carbonate and the alkanol impurity, comprising contacting the stream with an aryl group containing ester and a catalyst to effect reaction of the alkanol impurity with the aryl group containing ester.
摘要翻译：本发明涉及一种从含有碳酸二烷基酯和链烷醇杂质的流中除去烷醇杂质的方法，包括使该物流与含芳基酯和催化剂接触以使链烷醇杂质与含芳基酯反应。

6. 发明授权

US08907116B2 Process for removing an alkanol impurity from a dialkyl carbonate stream 有权
标题翻译：从碳酸二烷基酯流中除去烷醇杂质的方法
公开(公告)号：US08907116B2
公开(公告)日：2014-12-09
申请号：US13390124
申请日：2010-08-10
申请人： Cyrille Paul Allais , Garo Garbis Vaporciyan
发明人： Cyrille Paul Allais , Garo Garbis Vaporciyan
IPC分类号： C07C68/06 , C07C67/03 , C07C68/08
CPC分类号： C07C68/08 , C07C67/03 , C07C68/06 , C07C69/96 , C07C69/86
摘要： The invention relates to a process for removing an alkanol impurity from a stream containing a dialkyl carbonate and the alkanol impurity, comprising contacting the stream with an aryl group containing ester and a catalyst to effect reaction of the alkanol impurity with the aryl group containing ester.
摘要翻译：本发明涉及一种从含有碳酸二烷基酯和链烷醇杂质的流中除去烷醇杂质的方法，包括使该物流与含芳基酯和催化剂接触以使链烷醇杂质与含芳基酯反应。

7. 发明申请

US20130066099A1 PROCESS FOR PREPARING ALKANEDIOL AND DIALKYL CARBONATE 有权
标题翻译：制备阿尔卡尼和碳酸二乙酯的方法
公开(公告)号：US20130066099A1
公开(公告)日：2013-03-14
申请号：US13509648
申请日：2010-11-15
申请人： Cyrille Paul Allais , Timothy Michael Nisbet , Garo Garbis Vaporciyan , Cornelis Leonardus Maria Vrouwenvelder
发明人： Cyrille Paul Allais , Timothy Michael Nisbet , Garo Garbis Vaporciyan , Cornelis Leonardus Maria Vrouwenvelder
IPC分类号： C07C68/06 , C07C29/48
CPC分类号： C07C68/065 , C07C69/96
摘要： The invention relates to a process for the preparation of an alkanediol and a dialkyl carbonate comprising: (a) reacting an alkylene carbonate and an alkanol in the presence of a transesterification catalyst to obtain a reaction mixture comprising dialkyl carbonate, unconverted alkanol, alkanediol, unconverted alkylene carbonate and an alkoxy alkanol impurity; (b) subjecting the reaction mixture to distillation in a first distillation column to obtain a top stream comprising dialkyl carbonate, alkanol and alkoxy alkanol impurity and a bottom stream comprising alkanediol and alkylene carbonate; (c) subjecting the bottom stream from the first distillation column to distillation in a second distillation column to obtain a top stream comprising alkanediol and a bottom stream comprising alkylene carbonate; (d) subjecting the lop stream from the first distillation column to distillation in a third distillation column in the presence of a catalyst to effect reaction of the alkoxy alkanol impurity with the dialkyl carbonate into a carbonate ether impurity, to obtain a top stream comprising alkanol and a bottom stream comprising dialkyl carbonate and carbonate ether impurity; and (e) subjecting the bottom stream from the third distillation column to distillation in a fourth distillation column to obtain a top stream comprising dialkyl carbonate and a bottom stream comprising dialkyl carbonate and carbonate ether impurity, and (f) recycling the bottom stream from the fourth distillation column to the first distillation column.
摘要翻译：本发明涉及一种制备链烷二醇和碳酸二烷基酯的方法，包括：（a）在酯交换催化剂存在下使碳酸亚烷基酯和链烷醇反应，得到包含碳酸二烷基酯，未转化的链烷醇，链烷二醇，未转化的反应混合物碳酸亚烷基酯和烷氧基烷醇杂质; （b）使反应混合物在第一蒸馏塔中进行蒸馏以获得包含碳酸二烷基酯，链烷醇和烷氧基链烷醇杂质的顶部料流和包含链烷二醇和碳酸亚烷基酯的底部料流; （c）使来自第一蒸馏塔的塔底物流在第二蒸馏塔中进行蒸馏以获得包含链烷二醇的顶流和包含碳酸亚烷基酯的塔底料流; （d）在催化剂存在下，使来自第一蒸馏塔的第一蒸馏塔的第一蒸馏塔在第三蒸馏塔中进行蒸馏，以使烷氧基链烷醇杂质与碳酸二烷基酯杂质反应，得到包含链烷醇和包含碳酸二烷基酯和碳酸酯醚杂质的底部料流; 和（e）使来自第三蒸馏塔的塔底物流在第四蒸馏塔中进行蒸馏以获得包含碳酸二烷基酯和包含碳酸二烷基酯和碳酸酯醚杂质的底部料流的顶部料流，和（f）将来自第四蒸馏塔至第一蒸馏塔。

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