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1. 发明授权

US07488699B2 Hollow mesoporous carbon electrode-catalyst for direct methanol fuel cell and preparation thereof 有权
标题翻译：用于直接甲醇燃料电池的中空介孔碳电极催化剂及其制备
公开(公告)号：US07488699B2
公开(公告)日：2009-02-10
申请号：US11311486
申请日：2005-12-20
申请人： Chun-Chieh Huang , Man-Yin Lo , Hong-Pin Lin
发明人： Chun-Chieh Huang , Man-Yin Lo , Hong-Pin Lin
IPC分类号： B01J21/18 , B01J23/00 , B01J23/40 , C01B31/00 , C01B31/02 , C09D13/00
CPC分类号： H01M4/92 , B01J21/18 , B01J23/40 , B01J35/1023 , B01J35/1028 , B01J35/1061 , B01J37/0018 , B01J37/084 , C04B35/522 , C04B35/524 , C04B38/0022 , C04B2111/00853 , C04B2235/48 , C04B2235/6028 , H01M4/90 , H01M4/9083 , H01M4/926 , H01M8/1011 , Y02E60/523 , C04B35/52 , C04B38/0051 , C04B38/045
摘要： The present invention discloses a novel electrode-catalyst for direct methanol fuel cell prepared by introducing a carbon precursor into pores of a wormhole-like molecular sieve template, carbonizing the carbon precursor, removing the molecular sieve template to obtain a wormhole-like mesoporous carbon having a high specific surface of 800-1000 m2/g and a pore size of 4-5 nm, and depositing catalyst metal such as Pt—Ru on the mesoporous carbon.
摘要翻译：本发明公开了一种直接甲醇燃料电池的新型电极催化剂，其通过将碳前体引入虫洞样分子筛模板的孔中，对碳前体进行碳化，除去分子筛模板，得到具有虫洞状介孔碳 800-1000m2 / g的高比表面积和4-5nm的孔径，并且在介孔碳上沉积诸如Pt-Ru的催化剂金属。

2. 发明申请

US20060166811A1 Hollow mesoporous carbon electrode-catalyst for direct methanol fuel cell and preparation thereof 有权
标题翻译：用于直接甲醇燃料电池的中空介孔碳电极催化剂及其制备
公开(公告)号：US20060166811A1
公开(公告)日：2006-07-27
申请号：US11311486
申请日：2005-12-20
申请人： Chun-Chieh Huang , Man-Yin Lo , Hong-Pin Lin
发明人： Chun-Chieh Huang , Man-Yin Lo , Hong-Pin Lin
IPC分类号： H01M4/88 , B01J21/18
CPC分类号： H01M4/92 , B01J21/18 , B01J23/40 , B01J35/1023 , B01J35/1028 , B01J35/1061 , B01J37/0018 , B01J37/084 , C04B35/522 , C04B35/524 , C04B38/0022 , C04B2111/00853 , C04B2235/48 , C04B2235/6028 , H01M4/90 , H01M4/9083 , H01M4/926 , H01M8/1011 , Y02E60/523 , C04B35/52 , C04B38/0051 , C04B38/045
摘要： The present invention discloses a novel electrode-catalyst for direct methanol fuel cell prepared by introducing a carbon precursor into pores of a wormhole-like molecular sieve template, carbonizing the carbon precursor, removing the molecular sieve template to obtain a wormhole-like mesoporous carbon having a high specific surface of 800-1000 m2/g and a pore size of 4-5 nm, and depositing catalyst metal such as Pt—Ru on the mesoporous carbon.
摘要翻译：本发明公开了一种直接甲醇燃料电池的新型电极催化剂，其通过将碳前体引入虫洞样分子筛模板的孔中，对碳前体进行碳化，除去分子筛模板，得到具有虫洞状介孔碳 800-1000m 2 / g的高比表面积和4-5nm的孔径，并且在介孔碳上沉积诸如Pt-Ru的催化剂金属。

3. 发明授权

US08460427B2 Method for manufacturing metal nano particles having hollow structure 有权
标题翻译：具有中空结构的金属纳米颗粒的制造方法
公开(公告)号：US08460427B2
公开(公告)日：2013-06-11
申请号：US11873982
申请日：2007-10-17
申请人： Li-Duan Tsai , Kan-Lin Hsueh , Sung-Chun Chang , Man-Yin Lo , Yu-Min Peng , Chun-Chieh Huang , Ru-Shi Liu , Hao-Ming Chen , Hsin-Chieh Peng
发明人： Li-Duan Tsai , Kan-Lin Hsueh , Sung-Chun Chang , Man-Yin Lo , Yu-Min Peng , Chun-Chieh Huang , Ru-Shi Liu , Hao-Ming Chen , Hsin-Chieh Peng
IPC分类号： B22F9/16 , B22F9/18 , B22F9/24
CPC分类号： B22F9/24 , B22F2001/0029 , Y10T428/2982
摘要： A method for manufacturing metal nano particles having a hollow structure is provided. First, a suitable reducing agent is added into a first metal salt solution, and first metal ions are reduced to form first metal nano particles. Next, after the reducing agent is decomposed, a second metal salt solution with a higher reduction potential than that of the first metal is added. Then, the first metal particles are oxidized to form first metal ions when the second metal ions are reduced on the surface of the first metal by electrochemical oxidation reduction reaction, and thus, second metal nano particles having a hollow structure and a larger surface area are obtained. The method is simple and the metal nano particles with uniform particle size are obtained by this method.
摘要翻译：提供了一种制造具有中空结构的金属纳米颗粒的方法。首先，将合适的还原剂加入到第一金属盐溶液中，并且将第一金属离子还原形成第一金属纳米颗粒。接着，在还原剂分解后，添加比第一金属还原电位高的第二金属盐溶液。然后，当通过电化学氧化还原反应在第一金属的表面上还原第二金属离子时，第一金属颗粒被氧化以形成第一金属离子，因此具有中空结构和较大表面积的第二金属纳米颗粒是获得。该方法简单，通过该方法可以获得粒径均匀的金属纳米颗粒。

4. 发明申请

US20090035575A1 METHOD FOR MANUFACTURING METAL NANO PARTICLES HAVING HOLLOW STRUCTURE AND METAL NANO PARTICLES MANUFACTURED BY THE METHOD 有权
标题翻译：制备具有中空结构的金属纳米颗粒的方法和方法制备的金属纳米颗粒
公开(公告)号：US20090035575A1
公开(公告)日：2009-02-05
申请号：US11873982
申请日：2007-10-17
申请人： Li-Duan Tsai , Kan-Lin Hsueh , Sung-Chun Chang , Man-Yin Lo , Yu-Min Peng , Chun-Chieh Huang , Ru-Shi Liu , Hao Ming Chen , Hsin-Chieh Peng
发明人： Li-Duan Tsai , Kan-Lin Hsueh , Sung-Chun Chang , Man-Yin Lo , Yu-Min Peng , Chun-Chieh Huang , Ru-Shi Liu , Hao Ming Chen , Hsin-Chieh Peng
IPC分类号： B32B15/02 , B22F9/16
CPC分类号： B22F9/24 , B22F2001/0029 , Y10T428/2982
摘要： A method for manufacturing metal nano particles having a hollow structure is provided. First, a suitable reducing agent is added into a first metal salt solution, and first metal ions are reduced to form first metal nano particles. Next, after the reducing agent is decomposed, a second metal salt solution with a higher reduction potential than that of the first metal is added. Then, the first metal particles are oxidized to form first metal ions when the second metal ions are reduced on the surface of the first metal by electrochemical oxidation reduction reaction, and thus, second metal nano particles having a hollow structure and a larger surface area are obtained. The method is simple and the metal nano particles with uniform particle size are obtained by this method.
摘要翻译：提供了一种制造具有中空结构的金属纳米颗粒的方法。首先，将合适的还原剂加入到第一金属盐溶液中，并且将第一金属离子还原形成第一金属纳米颗粒。接着，在还原剂分解后，添加比第一金属还原电位高的第二金属盐溶液。然后，当通过电化学氧化还原反应在第一金属的表面上还原第二金属离子时，第一金属颗粒被氧化以形成第一金属离子，因此具有中空结构和较大表面积的第二金属纳米颗粒是获得。该方法简单，通过该方法可以获得粒径均匀的金属纳米颗粒。

5. 发明申请

US20130029252A1 FUEL CELL AND ELECTROCATALYST 审中-公开
标题翻译：燃料电池和电解质
公开(公告)号：US20130029252A1
公开(公告)日：2013-01-31
申请号：US13361624
申请日：2012-01-30
申请人： Man-Yin Lo , Ying-Chieh Chen , Mei-Yuan Chang
发明人： Man-Yin Lo , Ying-Chieh Chen , Mei-Yuan Chang
IPC分类号： H01M4/92 , C01B25/08
CPC分类号： H01M4/921 , H01M8/1011 , Y02E60/523
摘要： An embodiment of the invention provides an electrocatalyst, including a four-element catalyst having a formula of XYZP, wherein X is Pt or Pd, Y and Z are different elements selected from Group 6, Group 8, Group 9, or Group 11 elements, and P is phosphorous, wherein Group 6 elements include Cr, Mo, or W, Group 8 elements include Fe, Ru, or Os, Group 9 elements include Co, Rh, or Ir, and Group 11 elements include Cu, Ag, or Au.
摘要翻译：本发明的一个实施方案提供一种电催化剂，其包括具有式XYZP的四元素催化剂，其中X是Pt或Pd，Y和Z是选自第6组，第8组，第9组或第11组元素的不同元素，并且P是磷，其中第6族元素包括Cr，Mo或W，第8族元素包括Fe，Ru或Os，第9族元素包括Co，Rh或Ir，第11族元素包括Cu，Ag或Au 。

6. 发明申请

US20070149396A1 Process for preparing platinum based electrode catalyst for use in direct methanol fuel cell 有权
标题翻译：制备直接甲醇燃料电池用铂基电极催化剂的方法
公开(公告)号：US20070149396A1
公开(公告)日：2007-06-28
申请号：US11448889
申请日：2006-06-08
申请人： Man-Yin Lo , I-Hsuan Liao
发明人： Man-Yin Lo , I-Hsuan Liao
IPC分类号： B01J23/42
CPC分类号： H01M4/921 , B01J23/42 , B01J35/0013 , H01M8/1011 , Y02E60/523
摘要： The present invention discloses a method for preparing platinum (Pt) based nano-size catalyst which is useful as an electrode catalyst of a direct methanol fuel cell (DMFC). This method includes the implementation of a reduction reaction of a platinum precursor and an optional ad-metal precursor with a reducing agent in a solvent and in the presence of a stabilizer to form a suspension containing colloidal particles of platinum or platinum/ad-metal; mixing the suspension with a co-solvent; subjecting the resultant mixture to a centrifugal treatment to form a platinum or platinum/ad-metal colloidal particle portion and a liquid portion, repeating the co-solvent mixing and centrifugal treatment to the platinum or platinum/ad-metal colloidal particle portion until the resultant liquid portion no longer contains the product of the reduction reaction; and drying the resultant platinum or platinum/ad-metal colloidal particle portion to obtain a platinum based nano-size catalyst.
摘要翻译：本发明公开了一种可用作直接甲醇燃料电池（DMFC）的电极催化剂的铂（Pt）基纳米尺寸催化剂的制备方法。该方法包括在溶剂中和在稳定剂存在下，用还原剂将铂前体和任选的ad金属前体还原反应，形成含有铂或铂/金属的胶体颗粒的悬浮液; 将悬浮液与共溶剂混合; 对所得混合物进行离心处理以形成铂或铂/金属 - 金属胶体颗粒部分和液体部分，重复对铂或铂/金属 - 金属胶体颗粒部分的共溶剂混合和离心处理，直到得到液体部分不再含有还原反应的产物; 并干燥得到的铂或铂/金属 - 金属胶体颗粒部分，得到铂基纳米尺寸催化剂。

7. 发明授权

US09051396B2 Partially hydrogenated polymer and method thereof 有权
标题翻译：部分氢化聚合物及其方法
公开(公告)号：US09051396B2
公开(公告)日：2015-06-09
申请号：US12870467
申请日：2010-08-27
申请人： Hung Chieh Hou , Man-Yin Lo
发明人： Hung Chieh Hou , Man-Yin Lo
IPC分类号： C08F212/32 , C08F8/04 , C08F297/04
CPC分类号： C08F8/04 , C08F297/04 , C08F112/08
摘要： The present invention discloses a method for partially hydrogenating polymer. The method comprises providing a polymer having at least one vinyl aromatic block; and hydrogenating the polymer in presence of a heterogeneous catalyst on a support selected from the group consisting of BaSO4, Al2O3, TiO2, ZrO2, active carbon and any combination thereof to obtain a hydrogenated polymer. The hydrogenated polymer comprises at least one hydrogenated vinyl aromatic block having a carbon ring linking with a backbone of the hydrogenated polymer, wherein the average weight percent of the hydrogenated vinyl aromatic block(s) having only one and two double bonds on the carbon ring is between 1-30 wt % based on the total weight of the hydrogenated polymer.
摘要翻译：本发明公开了一种部分氢化聚合物的方法。该方法包括提供具有至少一个乙烯基芳香族嵌段的聚合物; 在非均相催化剂存在下，在选自由BaSO 4，Al 2 O 3，TiO 2，ZrO 2，活性炭及其任意组合组成的组的载体上氢化聚合物，得到氢化聚合物。氢化聚合物包含至少一个具有与氢化聚合物主链连接的碳环的氢化乙烯基芳族嵌段，其中在碳环上仅具有一个和两个双键的氢化乙烯基芳族嵌段的平均重量百分数为基于氢化聚合物的总重量为1-30重量％。

8. 发明授权

US07867942B2 Highly dispersed carbon supported metal catalyst and method for manufacturing the same 有权
标题翻译：高度分散的碳负载型金属催化剂及其制造方法
公开(公告)号：US07867942B2
公开(公告)日：2011-01-11
申请号：US12060319
申请日：2008-04-01
申请人： Man-Yin Lo , Hsi-Yen Hsu , Yan Zhi Chen , Li Duan Tsai , Yu Min Peng
发明人： Man-Yin Lo , Hsi-Yen Hsu , Yan Zhi Chen , Li Duan Tsai , Yu Min Peng
IPC分类号： B01J21/18 , B01J23/00 , B01J23/40 , B01J23/74 , H01M4/02 , H01M4/36 , H01M4/92 , H01M4/94
CPC分类号： H01M4/92 , H01M4/921 , H01M4/926
摘要： The invention provides a method for manufacturing a highly dispersed carbon supported metal catalyst, including charging a carbon support and a dispersing agent in water. The carbon support is evenly dispersed in water with an average diameter of 10 nm to 2000 nm and a specific surface area of 50 m2/g to 1500 m2/g. A metal salt of Pd, Pt, or combinations thereof is formed on the carbon support surface and then reduced to a valance state less than (IV).
摘要翻译：本发明提供一种制造高度分散的碳载金属催化剂的方法，包括将碳载体和分散剂装入水中。碳载体均匀分散在平均直径为10nm至2000nm，比表面积为50m 2 / g至1500m 2 / g的水中。在碳载体表面上形成Pd，Pt的金属盐或其组合，然后还原成小于（Ⅳ）的化合态。

9. 发明授权

US07829496B2 Process for preparing platinum based electrode catalyst for use in direct methanol fuel cell 有权
标题翻译：制备直接甲醇燃料电池用铂基电极催化剂的方法
公开(公告)号：US07829496B2
公开(公告)日：2010-11-09
申请号：US11448889
申请日：2006-06-08
申请人： Man-Yin Lo , I-Hsuan Liao
发明人： Man-Yin Lo , I-Hsuan Liao
IPC分类号： B01J23/42 , B01J23/56
CPC分类号： H01M4/921 , B01J23/42 , B01J35/0013 , H01M8/1011 , Y02E60/523
摘要： The present invention discloses a method for preparing platinum (Pt) based nano-size catalyst which is useful as an electrode catalyst of a direct methanol fuel cell (DMFC). This method includes the implementation of a reduction reaction of a platinum precursor and an optional ad-metal precursor with a reducing agent in a solvent and in the presence of a stabilizer to form a suspension containing colloidal particles of platinum or platinum/ad-metal; mixing the suspension with a co-solvent; subjecting the resultant mixture to a centrifugal treatment to form a platinum or platinum/ad-metal colloidal particle portion and a liquid portion, repeating the co-solvent mixing and centrifugal treatment to the platinum or platinum/ad-metal colloidal particle portion until the resultant liquid portion no longer contains the product of the reduction reaction; and drying the resultant platinum or platinum/ad-metal colloidal particle portion to obtain a platinum based nano-size catalyst.
摘要翻译：本发明公开了一种可用作直接甲醇燃料电池（DMFC）的电极催化剂的铂（Pt）基纳米尺寸催化剂的制备方法。该方法包括在溶剂中和在稳定剂存在下，用还原剂将铂前体和任选的ad金属前体还原反应，形成含有铂或铂/金属的胶体颗粒的悬浮液; 将悬浮液与共溶剂混合; 对所得混合物进行离心处理以形成铂或铂/金属 - 金属胶体颗粒部分和液体部分，重复对铂或铂/金属 - 金属胶体颗粒部分的共溶剂混合和离心处理，直到得到液体部分不再含有还原反应的产物; 并干燥得到的铂或铂/金属 - 金属胶体颗粒部分，得到铂基纳米尺寸催化剂。

10. 发明申请

US20100160668A1 CATALYST AND PROCESS FOR PREPARING CARBOXYLIC ACID ESTERS 有权
标题翻译：催化剂和制备羧酸酯的方法
公开(公告)号：US20100160668A1
公开(公告)日：2010-06-24
申请号：US12716947
申请日：2010-03-03
申请人： Kindtoken Hwaider LIU , Man-Yin Lo , Wen-Chyi Lin , Mei -Yuan Chang
发明人： Kindtoken Hwaider LIU , Man-Yin Lo , Wen-Chyi Lin , Mei -Yuan Chang
IPC分类号： C07C67/00
CPC分类号： B01J23/628 , B01J21/08 , B01J23/6484 , B01J37/0207 , C07C67/39 , C07C69/54
摘要： A catalyst and a process for preparing carboxylic acid esters from an aldehyde and an alcohol in the presence of molecular oxygen are disclosed. The catalyst comprises metals supported on a silica-containing support, wherein the metals consist essentially of palladium, lead, an alkali or alkaline earth metal, and at least one of niobium and zirconium. The process for preparing a carboxylic acid ester comprises reacting an aldehyde with an alcohol in the presence of molecular oxygen and the aforementioned catalyst.
摘要翻译：公开了一种在分子氧存在下由醛和醇制备羧酸酯的催化剂和方法。催化剂包含负载在含二氧化硅的载体上的金属，其中金属基本上由钯，铅，碱金属或碱土金属和至少一种铌和锆组成。制备羧酸酯的方法包括在分子氧和上述催化剂的存在下使醛与醇反应。

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