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1. 发明授权

US09914287B2 Adhesion promoter for adhesive composites composed of plastic and of a polyisocyanate polyaddition product 有权
公开(公告)号：US09914287B2
公开(公告)日：2018-03-13
申请号：US13140161
申请日：2009-12-10
申请人： Christian Renner , Gerlinde Tischer , Rolf Illguth , Margit Gehring , Franz Xaver Redl
发明人： Christian Renner , Gerlinde Tischer , Rolf Illguth , Margit Gehring , Franz Xaver Redl
IPC分类号： B32B27/40 , B32B37/14 , C08G18/40 , C08G18/42 , B32B5/18 , B32B7/12 , B32B27/06 , B32B27/08 , B32B27/18 , C08G101/00
CPC分类号： B32B27/40 , B32B5/18 , B32B7/12 , B32B27/065 , B32B27/08 , B32B27/18 , B32B37/14 , B32B2266/0278 , B32B2307/206 , B32B2307/7265 , B32B2307/734 , B32B2419/00 , B32B2605/08 , B32B2605/18 , C08G18/4018 , C08G18/4216 , C08G2101/0058 , C08G2101/0083 , Y10T428/249953
摘要： The present invention relates to composite elements comprising (i) plastic, adhering to which there is (ii) a polyisocyanate polyaddition product, where the polyisocyanate polyaddition product is obtained via mixing of (a) isocyanate with (b) compounds having groups reactive toward isocyanates, (c) catalysts and optionally additional products to give a reaction mixture and converting the reaction mixture to a polyisocyanate polyaddition product, where the compounds (b) comprise a polyester polyalcohol as adhesion promoter, capable of production via polycondensation of an acid component and one or more low-molecular-weight diols whose molar mass is less than 500 g/mol, in excess, where the acid component comprises from 83 to 97 mol % of adipic acid and from 3 to 17 mol % of phthalic acid, isophthalic acid, and/or terephthalic acid. The present invention also relates to components in the fitting-out or aircraft, of vehicles, or of buildings, and to insulation comprising this type of composite element.

2. 发明申请

US20110250429A1 ADHESION PROMOTER FOR ADHESIVE COMPOSITES COMPOSED OF PLASTIC AND OF A POLYISOCYANATE POLYADDITION PRODUCT 有权
公开(公告)号：US20110250429A1
公开(公告)日：2011-10-13
申请号：US13140161
申请日：2009-12-10
申请人： Christian Renner , Gerlinde Tischer , Rolf Illguth , Margit Gehring , Franz Xaver Redl
发明人： Christian Renner , Gerlinde Tischer , Rolf Illguth , Margit Gehring , Franz Xaver Redl
IPC分类号： B32B3/26
CPC分类号： B32B27/40 , B32B5/18 , B32B7/12 , B32B27/065 , B32B27/08 , B32B27/18 , B32B37/14 , B32B2266/0278 , B32B2307/206 , B32B2307/7265 , B32B2307/734 , B32B2419/00 , B32B2605/08 , B32B2605/18 , C08G18/4018 , C08G18/4216 , C08G2101/0058 , C08G2101/0083 , Y10T428/249953
摘要： The present invention relates to composite elements comprising (i) plastic, adhering to which there is (ii) a polyisocyanate polyaddition product, where the polyisocyanate polyaddition product is obtained via mixing of (a) isocyanate with (b) compounds having groups reactive toward isocyanates, (c) catalysts, (d) if appropriate, blowing agent, and (e) if appropriate, further additives, to give a reaction mixture and permitting the reaction mixture to complete its reaction to give the polyisocyanate polyaddition product, where the compounds (b) having groups reactive toward isocyanates comprise a polyester polyalcohol as adhesion promoter, capable of production via polycondensation of an acid component and of one or more low-molecular-weight diols whose molar mass is less than 500 g/mol, in excess, where the acid component comprises from 83 to 97 mol % of adipic acid and from 3 to 17 mol % of phthalic acid, isophthalic acid, and/or terephthalic acid. The present invention further relates to composite elements comprising (i) plastic, adhering to which there is (ii) a polyisocyanate polyaddition product, where the polyisocyanate polyaddition product is obtained via mixing of (a) isocyanate with (b) compounds having groups reactive toward isocyanates, (c) catalysts, (d) if appropriate, blowing agent, and (e) if appropriate, further additives to give a reaction mixture and permitting the reaction mixture to complete its reaction to give the polyisocyanate polyaddition product, where the compounds (b) having groups reactive toward isocyanates comprise a polyester polyalcohol as adhesion promoter, capable of production via polycondensation of an acid component and of one or more low-molecular-weight diols whose molar mass is less than 500 g/mol, in excess, where the low-molecular-weight diols comprise from 5 to 66 mol % of 1,3-propanediol, based on the total amount of the diol. The present invention also relates to a process for the production of these composite elements, and to components in the fitting-out of aircraft, of vehicles, or of buildings, and to insulation comprising this type of composite element.

3. 发明申请

US20050203268A1 Method for producing polyesterpolyols of polyvalent alcohols 有权
标题翻译：多元醇的聚酯多元醇的制造方法
公开(公告)号：US20050203268A1
公开(公告)日：2005-09-15
申请号：US10512851
申请日：2003-05-21
申请人： Alexander Wartini , Matthias Dernbach , Gerlinde Tischer , Tilman Sirch
发明人： Alexander Wartini , Matthias Dernbach , Gerlinde Tischer , Tilman Sirch
IPC分类号： C07C29/80 , C08G6/00 , C08G18/42 , C08G63/12 , C08G63/78 , C08G63/02 , C07C29/44
CPC分类号： C07C29/80 , C08G18/4208 , C08G18/4219 , C08G63/12 , C08G63/78 , C07C31/20 , C07C31/22 , C07C31/205 , C07C31/245
摘要： The invention provides a process for preparing polyester polyols of polyhydric alcohols by mono- or polyesterification of at least one carboxylic acid having at least two acid groups and/or at least one derivative of a dicarboxylic acid with polyhydric alcohols, optionally with the addition of a catalyst, while removing the water of reaction, wherein the polyhydric alcohol used has a formaldehyde acetal content of less than 500 ppm.
摘要翻译：本发明提供了通过至少一种具有至少两个酸基的羧酸和/或至少一种二羧酸衍生物与多元醇进行单酯化或聚酯化制备多元醇的聚酯多元醇的方法，任选地加入催化剂，同时除去反应水，其中所用的多元醇具有小于500ppm的甲醛缩醛含量。

4. 发明申请

US20120059143A1 PREPARING POLYESTER ALCOHOLS 审中-公开
标题翻译：制备聚酯醇
公开(公告)号：US20120059143A1
公开(公告)日：2012-03-08
申请号：US13227068
申请日：2011-09-07
申请人： Gerlinde Tischer , Ulrike Mahn , Stefan Käshammer , Hermann Graf , Christian Seitz , Christian Nitschke , Dieter Rodewald
发明人： Gerlinde Tischer , Ulrike Mahn , Stefan Käshammer , Hermann Graf , Christian Seitz , Christian Nitschke , Dieter Rodewald
IPC分类号： C08G63/80 , C08G63/668
CPC分类号： C08G63/78 , C08G18/4252 , C08G63/672
摘要： The subject of the present invention is a process for preparing polyester alcohols by condensation of polytetrahydrofuran with aromatic dicarboxylic acids and/or their anhydrides in the presence of a transesterification catalyst in a multi-stage operation at different pressure levels with at least one reaction stage at atmospheric pressure and at least one reaction stage at reduced pressure, where distillate is removed from the reaction system, which process comprises heating the reaction mixture in two or more phases in the atmospheric-pressure reaction stage wherein the heating phases are interrupted by at least one phase in which the temperature is kept constant.
摘要翻译：本发明的主题是通过在不同压力水平的多级操作中在酯交换催化剂存在下，将聚四氢呋喃与芳族二羧酸和/或它们的酸酐缩合制备聚酯醇的方法，其中至少一个反应阶段在大气压力和至少一个反应阶段，其中从反应体系中除去馏出物，该方法包括在大气压反应阶段中将反应混合物加热至两相或更多阶段，其中加热阶段被至少一个温度保持恒定的相。

5. 发明授权

US5852104A Aqueous polyurethane dispersions containing structural units derived from alkenyl- or alkylsuccinic acid 失效
标题翻译：含有衍生自链烯基或烷基琥珀酸的结构单元的水性聚氨酯分散体
公开(公告)号：US5852104A
公开(公告)日：1998-12-22
申请号：US789539
申请日：1997-01-27
申请人： Nicholas Kokel , Karl Haberle , Kuno Beutler , Jurgen Reichert , Peter Weyland , Gabriele Dralle-Voss , Knut Oppenlander , Michael Zirnstein , Gerlinde Tischer , Bernd Guettes , Ulrike Licht
发明人： Nicholas Kokel , Karl Haberle , Kuno Beutler , Jurgen Reichert , Peter Weyland , Gabriele Dralle-Voss , Knut Oppenlander , Michael Zirnstein , Gerlinde Tischer , Bernd Guettes , Ulrike Licht
IPC分类号： B05D7/12 , B32B27/40 , C08G18/08 , C08G18/34 , C08G18/42 , C08G18/66 , C08G18/68 , C08L75/00 , C08L75/04 , C09D175/00 , C09D175/04 , C09J175/00 , C09J175/04 , C08J3/00 , B32B27/00 , C08K3/20
CPC分类号： C14C11/006 , C08G18/0804 , C08G18/0823 , C08G18/12 , C08G18/4202 , C08G18/6633 , C08G18/6659 , C08G18/68 , C08G2170/80 , Y10T428/31551
摘要： Aqueous dispersions containing a polyurethane built up from a) diisocyanates having 4 to 30 carbon atoms, b) diols, of which b.1) from 10 to 100 mol %, based on the total amount of the diols (b), have a molecular weight of from 500 to 5000 and are built up from b1.1) (C.sub.4 - to C.sub.30 -alkyl)succinic acid and/or (C.sub.4 - to C.sub.30 -alkenyl)succinic acid, b1.2) from 0 to 60 mol %, based on component (b1.1), of a dicarboxylic acid which is different from component (b1.1), and b1.3) a diol having a molecular weight of from 60 to 500 g/mol, b.2) from 0 to 90 mol %, based on the total amount of the diols (b), have a molecular weight of from 60 to 500 g/mol, and b.3) from 0 to 90 mol %, based on the total amount of the diols (b), have a molecular weight of from 500 to 5000 g/mol and are different from (b1), c) monomers which are different from the monomers (a) and (b) and contain at least 2 isocyanate groups or at least 2 isocyanate-reactive groups and which in addition carry at least one hydrophilic group or a potentially hydrophilic group, thus achieving the water-dispersibility of polyurethanes, d) if desired, further polyfunctional compounds which are different from the monomers (a) to (c) and contain reactive groups which are alcoholic hydroxyl groups, primary or secondary amino groups or isocyanate groups, and e) if desired, monofunctional compounds which are different from the monomers (a) to (c) and contain one reactive group, which is an alcoholic hydroxyl group, a primary or secondary amino group or an isocyanate group.
摘要翻译：含有a）的水性分散体，其由a）具有4〜30个碳原子的二异氰酸酯组成，b）二醇，其中b.1）为10〜100摩尔％，基于二醇（b）的总量，具有分子量重量从500至5000，由b1.1）（C4-至C30-烷基）琥珀酸和/或（C4-至C30-烯基）琥珀酸，b1.2）为0至60摩尔％基于组分（b1.1）的不同于组分（b1.1）的二羧酸，和b1.3）分子量为60至500g / mol的二醇，b.2）为0 相对于二醇（b）的总量为90摩尔％，分子量为60〜500g / mol，b.3为0〜90摩尔％，基于二醇（b）具有500至5000g / mol的分子量并且不同于（b1），c）不同于单体（a）和（b）并且含有至少2个异氰酸酯基团或至少 2个异氰酸酯反应性基团，并且另外携带至少一个亲水基团或潜在的亲水性基团，从而达到聚氨酯的水分散性，d）如果需要，还有与单体（a）至（c）不同的多官能化合物，并且含有醇羟基的反应性基团，伯或仲氨基基团或异氰酸酯基，以及e）如果需要，与单体（a）至（c）不同且含有一个反应性基团（其为醇羟基，伯或仲氨基或异氰酸酯基团）的单官能化合物。

6. 发明申请

US20110201716A1 POLYESTER POLYOLS BASED ON TEREPHTHALIC ACID 审中-公开
标题翻译：基于过敏酸的聚酯多元醇
公开(公告)号：US20110201716A1
公开(公告)日：2011-08-18
申请号：US13124217
申请日：2009-10-13
申请人： Lionel Gehinger , Gunnar Kampf , Gerlinde Tischer
发明人： Lionel Gehinger , Gunnar Kampf , Gerlinde Tischer
IPC分类号： C08G18/34 , C07C69/76 , C08J9/06
CPC分类号： C08G18/4219 , C08G18/4018 , C08G18/4288 , C08G63/127 , C08G63/48 , C08G2101/0025
摘要： Polyester polyol comprising the esterification product of a) from 10 to 70 mol % of a dicarboxylic acid composition comprising a1) from 50 to 100 mol % of a material based on terephthalic acid, selected from among terephthalic acid, dimethyl terephthalate, polyalkylene terephthalate and mixtures thereof, a2) from 0 to 50 mol % of phthalic acid, phthalic anhydride or isophthalic acid, a3) from 0 to 50 mol % of one or more dicarboxylic acids, b) from 2 to 30 mol % of one or more fatty acids and/or fatty acid derivatives and/or benzoic acid, c) from 10 to 70 mol % of one or more aliphatic or cycloaliphatic diols having from 2 to 18 carbon atoms or alkoxylates thereof, d) from 2 to 50 mol % of a higher-functional polyol selected from the group consisting of glycerol, alkoxylated glycerol, trimethylolpropane, alkoxylated trimethylolpropane, pentaerythritol and alkoxylated pentaerythritol, wherein at least 200 mmol, preferably at least 500 mmol and particularly preferably at least 800 mmol, of polyols d) having an OH functionality of 2.9 are reacted per kg of polyester polyol.
摘要翻译：包含a）10-70mol％二羧酸组合物的酯化产物的聚酯多元醇，其包含a1）50-100mol％的基于对苯二甲酸的材料，其选自对苯二甲酸，对苯二甲酸二甲酯，聚对苯二甲酸亚烷基酯和混合物 a2）0〜50摩尔％的邻苯二甲酸，邻苯二甲酸酐或间苯二甲酸，a3）0〜50摩尔％的一种或多种二羧酸，b）2〜30摩尔％的一种或多种脂肪酸和 /或脂肪酸衍生物和/或苯甲酸，c）10至70mol％的一种或多种具有2至18个碳原子的脂族或脂环族二醇或其烷氧基化物，d）2-50mol％选自甘油，烷氧基化甘油，三羟甲基丙烷，烷氧基化三羟甲基丙烷，季戊四醇和烷氧基化季戊四醇的官能多元醇，其中至少200mmol，优选至少500mmol，特别优选至少800mmol，的多官能度为2.9的多元醇d）与每千克聚酯多元醇反应。

7. 发明授权

US07241914B2 Method for producing polyesterpolyols of polyvalent alcohols 有权
标题翻译：多元醇的聚酯多元醇的制造方法
公开(公告)号：US07241914B2
公开(公告)日：2007-07-10
申请号：US10512851
申请日：2003-05-21
申请人： Alexander Wartini , Matthias Dernbach , Gerlinde Tischer , Tilman Sirch
发明人： Alexander Wartini , Matthias Dernbach , Gerlinde Tischer , Tilman Sirch
IPC分类号： C07C69/34
CPC分类号： C07C29/80 , C08G18/4208 , C08G18/4219 , C08G63/12 , C08G63/78 , C07C31/20 , C07C31/22 , C07C31/205 , C07C31/245
摘要： The invention provides a process for preparing polyester polyols of polyhydric alcohols by mono- or polyesterification of at least one carboxylic acid having at least two acid groups and/or at least one derivative of a dicarboxylic acid with polyhydric alcohols, optionally with the addition of a catalyst, while removing the water of reaction, wherein the polyhydric alcohol used has a formaldehyde acetal content of less than 500 ppm.
摘要翻译：本发明提供了通过至少一种具有至少两个酸基的羧酸和/或至少一种二羧酸衍生物与多元醇进行单酯化或聚酯化制备多元醇的聚酯多元醇的方法，任选地加入催化剂，同时除去反应水，其中所用的多元醇具有小于500ppm的甲醛缩醛含量。

8. 发明授权

US06753402B1 Polyester-polyether block copolymers 失效
标题翻译：聚酯 - 聚醚嵌段共聚物
公开(公告)号：US06753402B1
公开(公告)日：2004-06-22
申请号：US10110297
申请日：2002-04-10
申请人： Stephan Bauer , Georg Heinrich Grosch , Gerlinde Tischer , Kathrin Harre , Eva Baum , Thomas Ostrowski , Reinhard Lorenz , Regina Pretzsch , Michael Pcolinski , Stefan Dinsch , Inge Rotermund
发明人： Stephan Bauer , Georg Heinrich Grosch , Gerlinde Tischer , Kathrin Harre , Eva Baum , Thomas Ostrowski , Reinhard Lorenz , Regina Pretzsch , Michael Pcolinski , Stefan Dinsch , Inge Rotermund
IPC分类号： C08G1842
CPC分类号： C08G81/00 , C08G18/4018 , C08G18/42 , C08G18/4261 , C08G65/2609 , C08G65/2663 , C08G2101/0008 , C08G2101/0083 , C08G2130/00 , C08L71/02 , C08L2666/18
摘要： Polyester-polyether block copolymers can be prepared by catalytic addition of alkylene oxides onto H-functional initiator substances, using polyester alcohols as H-functional initiator substances and multimetal cyanide compounds as catalysts.
摘要翻译：聚酯 - 聚醚嵌段共聚物可以通过使用聚酯醇作为H官能引发剂物质和多金属氰化物作为催化剂将环氧烷催化加成到H官能引发剂物质上来制备。

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