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    • 10. 发明申请
    • Purification of organic compositions by sublimation
    • 通过升华纯化有机组合物
    • US20060289289A1
    • 2006-12-28
    • US11159781
    • 2005-06-23
    • Christian Kloc
    • Christian Kloc
    • B01D3/00
    • B01D7/00
    • A method purifies a starting solid or semi-solid organic composition located in a chamber. The method includes heating the starting organic composition such that molecules of one organic molecular species sublime out of the composition and molecules of a desired organic molecular species remain in the composition. The method includes pumping the chamber during the heating step to remove sublimed organic molecules. The method includes then, heating a remaining portion of the composition at one or more higher temperatures such that molecules of the desired organic molecular species sublime from the remaining portion of the composition. A separate region of the chamber is maintained under conditions that cause deposition of sublimed molecules of the desired species during the heating a remaining portion.
    • 方法净化位于室中的起始固体或半固体有机组合物。 该方法包括加热起始有机组合物,使得一种有机分子物质的分子在组合物中升华,并且所需有机分子物质的分子保留在组合物中。 该方法包括在加热步骤期间泵送室以除去升华的有机分子。 该方法包括然后在一个或多个较高温度下加热组合物的剩余部分,使得所需有机分子物质的分子从组合物的剩余部分中升华。 在加热剩余部分期间,室的单独区域保持在导致所需物质的升华分子沉积的条件下。