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1. 发明授权

US4888060A Enrichment of fructose syrups 失效
标题翻译：富含果糖糖浆
公开(公告)号：US4888060A
公开(公告)日：1989-12-19
申请号：US11417
申请日：1987-02-03
申请人： Carl W. Niekamp , Martin Seidman
发明人： Carl W. Niekamp , Martin Seidman
IPC分类号： C13K3/00
CPC分类号： C13K3/00
摘要： A process for manufacturing an enriched fructose syrup, which is characterized in that dextrose is crystallized from a syrup containing fructose and dextrose and then an alcohol is added to enhance separation of the dextrose crystals from the mother liquor.Process can be adjusted to yield dextrose monohydrate, anhydrous alpha dextrose or a 40 percent fructose crystalline product in addition to an enriched fructose syrup.
摘要翻译：一种富含果糖糖浆的制造方法，其特征在于，葡萄糖从含有果糖和葡萄糖的糖浆中结晶，然后加入醇以增加右旋糖结晶与母液的分离。除了浓缩的果糖糖浆之外，还可以调整过程以产生葡萄糖一水合物，无水α葡萄糖或40％果糖结晶产物。

2. 发明授权

US4464204A Alkylidenation of fructose with perfluorinated acid catalysts 失效
标题翻译：用全氟酸催化剂对果糖进行烷基化
公开(公告)号：US4464204A
公开(公告)日：1984-08-07
申请号：US445114
申请日：1982-11-29
申请人： Carl W. Niekamp , Martin Seidman
发明人： Carl W. Niekamp , Martin Seidman
IPC分类号： C07H3/02 , C07H9/04 , C07H1/06 , C13D3/14 , C13K11/00
CPC分类号： C07H9/04 , C07H3/02
摘要： Aqueous fructose and aldehydes, ketones and/or acetals may be effectively catalyzed into alkylidene fructose derivatives with immobilized acid catalysts. The reaction provides a means for enriching the fructose content of conventional high fructose corn syrups. Perfluorinated acid resins are especially effective catalysts for converting aqueous fructose and acetone solutions into diacetone fructose. Catalysis with the perfluorinated acid resins may be conducted at significantly lower conversion temperatures with superior reactant and reaction product exchange rates. Enrichment of high fructose corn syrups may be generally accomplished by catalyzing the fructose and acetone into a diacetone fructose solution with the perfluorinated acid resin, allowing the dextrose to precipitate from the diacetone solution, hydrolyzing the diacetone fructose to fructose and recovery of the enriched fructose product therefrom. The water-insoluble catalysts afford a reusable catalyst system which can be easily separated from the processed products. The perfluorinated acid resins produce a high quality, food-grade syrup products essentially free of ash, organoleptic bodies (e.g. flavoring, coloring, etc.) and other objectionable by-product contaminants.
摘要翻译：含水果糖和醛，酮和/或缩醛可以用固定化的酸催化剂有效地催化成亚烷基果糖衍生物。该反应提供了富集常规高果糖玉米糖浆的果糖含量的方法。全氟酸树脂是将水果果糖和丙酮溶液转化为双丙酮果糖的特别有效的催化剂。使用全氟酸树脂的催化可以在显着较低的转化温度下进行，具有优异的反应物和反应产物的交换速率。高果糖玉米糖浆的富集通常可以通过用全氟酸树脂将果糖和丙酮催化成双丙酮果糖溶液，使右旋糖从双丙酮溶液中沉淀出来，将双丙酮果糖水解成果糖并回收富含果糖的产物由此。水不溶性催化剂提供可重复使用的催化剂体系，其可以容易地与加工产物分离。全氟酸树脂产生基本上不含灰分，感官体（如调味剂，着色剂等）和其它令人反感的副产物污染物的高质量食品级糖浆产品。

3. 发明授权

US4465521A Diacetone fructose hydrolysis with water-insoluble catalysts 失效
标题翻译：双丙酮果糖水解用水不溶性催化剂
公开(公告)号：US4465521A
公开(公告)日：1984-08-14
申请号：US445113
申请日：1982-11-29
申请人： Martin Seidman , Carl W. Niekamp
发明人： Martin Seidman , Carl W. Niekamp
IPC分类号： C07H3/02 , C13K11/00 , C13D1/00
CPC分类号： C07H3/02 , C13K11/00
摘要： Diacetone fructose solutions may be effectively hydrolyzed to fructose by acid exchange resins. Hydrolysis of diacetone fructose with acid exchange resins substantially reduces the formation of objectionable flavoring, coloring and other hydrolyzate by-products. The immobilized acid catalysis provides a fructose product substantially free from ash residues and significantly reduces the carbon, cation and anion exchange requirements for the manufacture of enriched, food-grade fructose syrups. Perfluorinated acid exchange resins have been found to be particularly effective for hydrolyzing aqueous diacetone fructose solutions into fructose.
摘要翻译：双丙酮果糖溶液可以通过酸交换树脂有效地水解成果糖。用酸交换树脂水解双丙酮果糖大大减少了令人反感的调味料，着色剂和其他水解产物副产物的形成。固定化的酸催化提供了基本上不含灰分残留物的果糖产品，并显着降低了制造富含的食品级果糖糖浆的碳，阳离子和阴离子交换要求。已经发现全氟酸交换树脂对于将水解双丙酮果糖溶液水解成果糖特别有效。

4. 发明授权

US5039346A Fructose syrups and sweetened beverages 失效
标题翻译：果糖糖浆和甜味饮料
公开(公告)号：US5039346A
公开(公告)日：1991-08-13
申请号：US571009
申请日：1990-08-17
申请人： Dorothy C. White , Carl W. Niekamp
发明人： Dorothy C. White , Carl W. Niekamp
IPC分类号： A23L1/09 , A23L1/236 , C13K11/00
CPC分类号： C13K11/00 , A23L27/33 , A23L29/32 , Y10S426/804
摘要： Methods of preparing and using sweetener syrups comprised of crystalline saccharides are provided. A crystalline saccharide composition comprised of crystalline fructose is dissolved in a potable liquid to form a concentrated syrup. Anhydrous crystalline fructose and/or crystalline fructose dihydrate are used to prepare the syrups. At least about 42% by weight of the crystalline saccharide composition is fructose, the remainder preferably being crystalline dextrose. The use of crystalline saccharides yield color stable syrups especially useful in clear and/or colorless beverages.
摘要翻译：提供了制备和使用由结晶糖组成的甜味剂糖浆的方法。由结晶果糖组成的结晶糖组合物溶解在饮用液体中以形成浓缩糖浆。无水结晶果糖和/或结晶果糖二水合物用于制备糖浆。结晶糖组合物的至少约42重量％是果糖，其余的优选是结晶葡萄糖。结晶糖的使用产生特别用于透明和/或无色饮料的颜色稳定的糖浆。

5. 发明授权

US4618579A Raw starch saccharification 失效
标题翻译：生淀粉糖化
公开(公告)号：US4618579A
公开(公告)日：1986-10-21
申请号：US656051
申请日：1984-09-28
申请人： Bruce L. Dwiggins , Carl E. Pickens , Carl W. Niekamp
发明人： Bruce L. Dwiggins , Carl E. Pickens , Carl W. Niekamp
IPC分类号： A23L1/09 , C12N9/34 , C12P19/20 , C12R1/645 , C12P19/14
CPC分类号： C12N9/2428 , C12P19/20 , Y10S435/911
摘要： A multi-step process is provided for solubilizing and saccharifying granular starch slurries of between 20 and 60% d.s. starch. In a first step, an enzyme mixture exhibiting raw starch hydrolyzing activity is added to the slurry and maintained in contact therewith until at least a substantial portion but less than all of the starch is solubilized. The resulting syrup is separated from the remaining insoluble fraction. In a second step, the insoluble fraction is used to prepare a second slurry containing less than about 20% d.s. starch, and this second slurry is solubilized with a raw starch hydrolyzing enzyme preparation until substantially all (e.g., at least about 95% or more) of the starch is solubilized. The pooled syrup from the two steps is over about 20 weight percent saccharides, at least about 95% of which is glucose.
摘要翻译：提供了一种多步骤方法，用于增溶和糖化20-60％d.s的颗粒状淀粉浆。淀粉。在第一步中，将表现出生淀粉水解活性的酶混合物加入到浆料中并与之保持接触，直至至少大部分但少于所有淀粉溶解。将所得糖浆与剩余的不溶性部分分离。在第二步中，不溶级分用于制备含有少于约20％d.s的第二浆料。淀粉，并且用生淀粉水解酶制剂溶解该第二浆料，直到基本上全部（例如，至少约95％或更多）淀粉溶解。来自两个步骤的汇集的糖浆超过约20重量％的糖，其中至少约95％是葡萄糖。

6. 发明授权

US4634472A Enrichment of fructose syrups 失效
标题翻译：富含果糖糖浆
公开(公告)号：US4634472A
公开(公告)日：1987-01-06
申请号：US768892
申请日：1985-08-23
申请人： Carl W. Niekamp , James D. Wideman
发明人： Carl W. Niekamp , James D. Wideman
IPC分类号： A23L1/09 , C13K1/10 , C13K11/00 , F24C1/00
CPC分类号： C13K11/00 , A23L29/30 , C13K1/10
摘要： A process for manufacturing an enriched fructose syrup, which is characterized in that dextrose is crystallized from a relatively high solids feed syrup containing fructose and dextrose and then another relatively dilute (or lower solids) fructose containing diluent syrup is added to enhance separation of the dextrose crystals from the mother liquor.Process can be adjusted to yield dextrose monohydrate or anhydrous alpha dextrose crystalline product in addition to an enriched fructose syrup.
摘要翻译：一种富含果糖糖浆的制造方法，其特征在于，葡萄糖从含有果糖和葡萄糖的相对较高的固体饲料糖浆中结晶，然后加入另一种相对较稀的（或较低固含量）的含果糖稀释剂糖浆以增强葡萄糖的分离母液中的晶体。除了富集的果糖糖浆之外，可以调节过程以产生葡萄糖一水合物或无水α-葡萄糖结晶产物。

7. 发明授权

US4612284A Process for the enzymatic hydrolysis of non-gelatinized granular starch material directly to glucose 失效
标题翻译：将非胶凝颗粒淀粉材料直接酶水解成葡萄糖的方法
公开(公告)号：US4612284A
公开(公告)日：1986-09-16
申请号：US656117
申请日：1984-09-28
申请人： Carl E. Pickens , Carl W. Niekamp
发明人： Carl E. Pickens , Carl W. Niekamp
IPC分类号： C12P19/14 , C12P19/20 , C13K1/08 , C12P19/02
CPC分类号： C12P19/14 , C12P19/20 , C13K1/08
摘要： There is disclosed a process for enzymatically hydrolyzing a non-gelationized granular starch material directly to glucose. In another embodiment, granular starch remaining non-hydrolyzed following a direct, granular starch hydrolysis process and having liberated fat and/or protein residues coated, adsorbed or otherwise accumulated thereon is pasted, thinned separated from said fat and/or protein residues and recycled to said granular starch hydrolysis process for further hydrolysis to glucose therein.
摘要翻译：公开了一种将非凝胶化的颗粒淀粉材料直接水解成葡萄糖的方法。在另一个实施方案中，在直接的颗粒状淀粉水解方法之后保持非水解并且已经被包被，吸附或以其它方式积聚的释放的脂肪和/或蛋白质残留物的颗粒淀粉被从所述脂肪和/或蛋白质残余物中分离出来并被再次分配到所述颗粒状淀粉水解方法进一步水解成葡萄糖。

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