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1. 发明授权

US5519124A Production of alkylpolyglycosides 失效
标题翻译：烷基多糖苷的生产
公开(公告)号：US5519124A
公开(公告)日：1996-05-21
申请号：US152111
申请日：1993-11-12
申请人： Patrick M. McCurry, Jr. , Carl E. Pickens
发明人： Patrick M. McCurry, Jr. , Carl E. Pickens
IPC分类号： C07H1/00 , C07H15/04 , C08B37/00 , C07H1/06 , C07G3/00
CPC分类号： C07H15/04
摘要： An improvement in the process of preparation of an alkylpolyglycoside containing a long chain alkyl group of about 10 carbon atoms or more by reaction of a saccharide and a long chain alcohol in the presence of an acid catalyst, particularly an improvement in the process to inhibit or minimize condenser fouling during the processing either in the removal of water from the reactor to promote completion of the reaction or in subsequent processing of the reaction product stream wherein the stream is heated at elevated temperatures and vacuum to remove excess alcohol and residual water, or water introduced into the process stream by steam ejectors in an evaporator, after leaving the reactor. The improvement includes the addition of an alcohol having a carbon chain of a number less than the carbon chain of the alkyl group of the alkylpolyglycoside product either along with the reactant alcohol to produce the polyglycoside, or to the product stream at evaporation of the excess alcohol and residual water.
摘要翻译：在酸催化剂存在下，通过糖和长链醇的反应，制备含有约10个碳原子或更长链长烷基的烷基多糖苷的方法的改进，特别是抑制或抑制方法的改进在处理过程中使冷凝器结垢最小化，以便从反应器中除去水以促进反应的完成或反应产物流的后续处理，其中将物流在升高的温度和真空下加热以除去过量的醇和残留的水或水在离开反应器之后，通过蒸发器中的蒸汽喷射器引入工艺流。改进之处在于，连同反应物醇一起加入数量少于烷基多糖苷产物的烷基的碳链的醇以产生多糖苷，或者在蒸发过量的醇时向产物流中加入和残余水。

2. 发明授权

US4939245A Process for the direct production of glysoside product in the presence of solid saccharide 失效
标题翻译：在固体糖存在下直接生产糖苷产物的方法
公开(公告)号：US4939245A
公开(公告)日：1990-07-03
申请号：US287953
申请日：1988-12-21
申请人： John F. Rasche , Carl E. Pickens , Patrick M. McCurry, Jr.
发明人： John F. Rasche , Carl E. Pickens , Patrick M. McCurry, Jr.
IPC分类号： C07H15/04
CPC分类号： C07H15/04
摘要： The invention is a process for preparing a glycoside product by reacting an alcohol having 4 to 30 carbon atoms with a saccharide or oligosaccharide in the presence of an acid catalyst wherein an undissolved phase comprising the saccharide or oligosaccharide is present in the reaction mixture during the process.
摘要翻译：本发明是一种通过在酸催化剂存在下使具有4-30个碳原子的醇与糖或寡糖反应来制备糖苷产物的方法，其中在该过程中在反应混合物中存在包含糖或寡糖的未溶解相。

3. 发明授权

US4612284A Process for the enzymatic hydrolysis of non-gelatinized granular starch material directly to glucose 失效
标题翻译：将非胶凝颗粒淀粉材料直接酶水解成葡萄糖的方法
公开(公告)号：US4612284A
公开(公告)日：1986-09-16
申请号：US656117
申请日：1984-09-28
申请人： Carl E. Pickens , Carl W. Niekamp
发明人： Carl E. Pickens , Carl W. Niekamp
IPC分类号： C12P19/14 , C12P19/20 , C13K1/08 , C12P19/02
CPC分类号： C12P19/14 , C12P19/20 , C13K1/08
摘要： There is disclosed a process for enzymatically hydrolyzing a non-gelationized granular starch material directly to glucose. In another embodiment, granular starch remaining non-hydrolyzed following a direct, granular starch hydrolysis process and having liberated fat and/or protein residues coated, adsorbed or otherwise accumulated thereon is pasted, thinned separated from said fat and/or protein residues and recycled to said granular starch hydrolysis process for further hydrolysis to glucose therein.
摘要翻译：公开了一种将非凝胶化的颗粒淀粉材料直接水解成葡萄糖的方法。在另一个实施方案中，在直接的颗粒状淀粉水解方法之后保持非水解并且已经被包被，吸附或以其它方式积聚的释放的脂肪和/或蛋白质残留物的颗粒淀粉被从所述脂肪和/或蛋白质残余物中分离出来并被再次分配到所述颗粒状淀粉水解方法进一步水解成葡萄糖。

4. 发明授权

US5512666A Process for making alkyl polyglycosides 失效
标题翻译：制备烷基多糖苷的方法
公开(公告)号：US5512666A
公开(公告)日：1996-04-30
申请号：US278777
申请日：1994-07-22
申请人： Patrick M. McCurry, Jr. , Janet R. Varvil , Carl E. Pickens
发明人： Patrick M. McCurry, Jr. , Janet R. Varvil , Carl E. Pickens
IPC分类号： C07H15/04
CPC分类号： C07H15/04
摘要： A process has been discovered for making alkyl polyglycoside which comprises reacting a fatty alcohol having from about 8 to about 22 carbon atoms with a sugar, in the presence of an acid catalyst, to form a product of alkyl polyglycoside and excess fatty alcohol. The molar ratio of fatty alcohol to sugar, respectively, is at least 2:1. The excess fatty alcohol is then separated from the alkyl polyglycoside product. Once separated, the excess fatty alcohol is then reacted with a source of boric acid to form a mixture comprised of one or more borate esters of the fatty alcohol and inert compounds. The non-hydroxylic compounds are then separated from the borate esters. The substantially pure fatty alcohol is then returned to the beginning of the process for use in the formation of alkyl polyglycoside.
摘要翻译：已经发现制备烷基多糖苷的方法包括使具有约8至约22个碳原子的脂肪醇与糖在酸催化剂存在下反应，形成烷基多糖苷和过量脂肪醇的产物。脂肪醇与糖的摩尔比分别为至少2：1。然后将多余的脂肪醇与烷基多糖苷产物分离。一旦分离，然后将过量的脂肪醇与硼酸源反应，形成由一种或多种脂肪醇的硼酸酯和惰性化合物组成的混合物。然后将非羟基化合物与硼酸酯分离。然后将基本上纯的脂肪醇返回到用于形成烷基多糖苷的方法的开始。

5. 发明授权

US5496932A Process for the production of alkylpolyglycoside 失效
标题翻译：制备烷基多糖苷的方法
公开(公告)号：US5496932A
公开(公告)日：1996-03-05
申请号：US47217
申请日：1993-04-14
申请人： Patrick M. McCurry, Jr. , Brian A. Michel , Carl E. Pickens , Janet R. Varvil
发明人： Patrick M. McCurry, Jr. , Brian A. Michel , Carl E. Pickens , Janet R. Varvil
IPC分类号： C07H1/00 , C07H3/06 , C07H15/04 , C07H1/06 , C07H15/02
CPC分类号： C07H15/04 , C07H3/06
摘要： An improved process for preparing an alkylpolyglycoside wherein the alkyl group contains about 8 to about 20 carbon atoms, prepared by reacting a saccharide and an alcohol in the presence of an acid catalyst, and subsequently removing excess unreacted alcohol, the improvement comprising adding to the reaction product an oxide, such as MgO, and removing the excess unreacted alcohol by thin film evaporation under vacuum at temperatures up to about 240.degree. C. under sparging or non-sparging condition with an inert gas.
摘要翻译：制备烷基多糖苷的改进方法，其中烷基含有约8至约20个碳原子，通过糖和醇在酸催化剂存在下反应制备，随后除去过量的未反应醇，其改进包括加入反应产生氧化物，例如MgO，并且在鼓风或非喷射条件下用惰性气体在高达约240℃的真空下通过薄膜蒸发除去过量的未反应的醇。

6. 发明授权

US5457190A Process for the preparation of glycosides 失效
标题翻译：糖苷的制备方法
公开(公告)号：US5457190A
公开(公告)日：1995-10-10
申请号：US891305
申请日：1992-05-29
申请人： Michael W. Gibson , Patrick M. McCurry, Jr. , Carl E. Pickens
发明人： Michael W. Gibson , Patrick M. McCurry, Jr. , Carl E. Pickens
IPC分类号： C07H1/00 , C07H15/04 , C07H15/08
CPC分类号： C07H15/08 , C07H15/04
摘要： A process for preparing aliphatic polysaccharides in which a slurry of a hydrous saccharide source in a first portion of aliphatic alcohol is introduced into a second portion of the aliphatic alcohol maintained at an elevated temperature and under a reduced pressure to form a mixture of saccharide source and alcohol with a reduced water content, introducing an acid catalyst into the mixture with the reduced water content and reacting the aliphatic alcohol with the saccharide source to form an aliphatic glycoside.
摘要翻译：一种制备脂肪族多糖的方法，其中在脂肪族醇的第一部分中的含水糖源的浆料被引入脂肪醇的第二部分，保持在升高的温度和减压下，以形成糖源和具有降低的水含量的醇，将酸催化剂引入具有降低的水含量的混合物中，并使脂族醇与糖源反应以形成脂族糖苷。

7. 发明授权

US4950743A Process for preparation of alkylglycosides 失效
标题翻译：烷基糖苷的制备方法
公开(公告)号：US4950743A
公开(公告)日：1990-08-21
申请号：US79195
申请日：1987-07-29
申请人： Patrick M. McCurry, Jr. , Carl E. Pickens
发明人： Patrick M. McCurry, Jr. , Carl E. Pickens
IPC分类号： C07H15/04
CPC分类号： C07H15/04
摘要： A process for preparing alkylglycosides by reacting an 8 to 20 carbon atom monohydric alcohol with a monosaccharide in the presence of an acid catalyst, while under partial vacuum, followed by neutralizing the reactant product with an alkaline metal hydroxide in an amount about equal on a molar basis to the amount of catalyst, and removal of the residual unreacted alcohol.
摘要翻译：在部分真空下，在酸催化剂的存在下，使8〜20个碳原子的一元醇与单糖反应，然后用碱金属氢氧化物中和反应产物的摩尔数大约相等的方法制备烷基糖苷类的方法基于催化剂的量，并除去残留的未反应的醇。

8. 发明授权

US4618579A Raw starch saccharification 失效
标题翻译：生淀粉糖化
公开(公告)号：US4618579A
公开(公告)日：1986-10-21
申请号：US656051
申请日：1984-09-28
申请人： Bruce L. Dwiggins , Carl E. Pickens , Carl W. Niekamp
发明人： Bruce L. Dwiggins , Carl E. Pickens , Carl W. Niekamp
IPC分类号： A23L1/09 , C12N9/34 , C12P19/20 , C12R1/645 , C12P19/14
CPC分类号： C12N9/2428 , C12P19/20 , Y10S435/911
摘要： A multi-step process is provided for solubilizing and saccharifying granular starch slurries of between 20 and 60% d.s. starch. In a first step, an enzyme mixture exhibiting raw starch hydrolyzing activity is added to the slurry and maintained in contact therewith until at least a substantial portion but less than all of the starch is solubilized. The resulting syrup is separated from the remaining insoluble fraction. In a second step, the insoluble fraction is used to prepare a second slurry containing less than about 20% d.s. starch, and this second slurry is solubilized with a raw starch hydrolyzing enzyme preparation until substantially all (e.g., at least about 95% or more) of the starch is solubilized. The pooled syrup from the two steps is over about 20 weight percent saccharides, at least about 95% of which is glucose.
摘要翻译：提供了一种多步骤方法，用于增溶和糖化20-60％d.s的颗粒状淀粉浆。淀粉。在第一步中，将表现出生淀粉水解活性的酶混合物加入到浆料中并与之保持接触，直至至少大部分但少于所有淀粉溶解。将所得糖浆与剩余的不溶性部分分离。在第二步中，不溶级分用于制备含有少于约20％d.s的第二浆料。淀粉，并且用生淀粉水解酶制剂溶解该第二浆料，直到基本上全部（例如，至少约95％或更多）淀粉溶解。来自两个步骤的汇集的糖浆超过约20重量％的糖，其中至少约95％是葡萄糖。

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