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1. 发明授权

US06423880B1 Isopentane disproportionation 有权
标题翻译：异戊烷歧化
公开(公告)号：US06423880B1
公开(公告)日：2002-07-23
申请号：US09596456
申请日：2000-06-19
申请人： Bruce B. Randolph , Kenneth C. Hoover , Martyn E. Pfile
发明人： Bruce B. Randolph , Kenneth C. Hoover , Martyn E. Pfile
IPC分类号： C07C608
CPC分类号： C07C6/10 , C07C2527/054 , C07C2527/1206 , C07C2531/025
摘要： A novel i-pentane disproportionation process is provided and includes contacting i-pentane with an acidic disproportionation catalyst in the presence of a lower paraffin co-feed and, optionally, in the presence of an initiator.
摘要翻译：提供了一种新颖的戊烷歧化方法，包括在低级链烷烃共进料存在下，和任选地，在引发剂存在下，将异戊烷与酸性歧化催化剂接触。

2. 发明授权

US07906700B2 Alkylation of isobutene feeds 有权
标题翻译：异丁烯进料的烷基化
公开(公告)号：US07906700B2
公开(公告)日：2011-03-15
申请号：US11445354
申请日：2006-06-01
申请人： Bruce B. Randolph , Keith W. Hovis , Kenneth C. Hoover
发明人： Bruce B. Randolph , Keith W. Hovis , Kenneth C. Hoover
IPC分类号： C07C2/00
CPC分类号： C07C7/20 , C07C2/62 , C07C2527/054 , C07C2527/1206 , C07C9/16
摘要： A process for alkylating isobutene by introducing a feed containing isobutene and an isoparaffin, in the form of droplets, into an acid catalyst to produce an alkylation product, wherein the Sauter mean diameter of the droplets is greater than or equal to about 150 μm and is less than or equal to about 500 μm, is disclosed.
摘要翻译：通过将含有异丁烯和异链烷烃（以液滴的形式）的进料引入酸催化剂以产生烷基化产物来烷基化异丁烯的方法，其中所述液滴的Sauter平均直径大于或等于约150μm，并且是小于或等于约500μm。

3. 发明申请

US20070282150A1 Alkylation of isobutene feeds 有权
标题翻译：异丁烯进料的烷基化
公开(公告)号：US20070282150A1
公开(公告)日：2007-12-06
申请号：US11445354
申请日：2006-06-01
申请人： Bruce B. Randolph , Keith W. Hovis , Kenneth C. Hoover
发明人： Bruce B. Randolph , Keith W. Hovis , Kenneth C. Hoover
IPC分类号： C07C2/56
CPC分类号： C07C7/20 , C07C2/62 , C07C2527/054 , C07C2527/1206 , C07C9/16
摘要： A process for alkylating isobutene by introducing a feed containing isobutene and an isoparaffin, in the form of droplets, into an acid catalyst to produce an alkylation product, wherein the Sauter mean diameter of the droplets is greater than or equal to about 150 μm and is less than or equal to about 500 μm, is disclosed.
摘要翻译：通过将含有异丁烯和异链烷烃的进料（以液滴形式）引入酸催化剂中以产生烷基化产物来烷基化异丁烯的方法，其中所述液滴的沙特平均直径大于或等于约150μm，并且是小于或等于约500μm。

4. 发明授权

US5086163A Aromatic sulfide/sulfone polymer production 失效
标题翻译：芳香族硫化物/砜聚合物生产
公开(公告)号：US5086163A
公开(公告)日：1992-02-04
申请号：US674812
申请日：1991-03-22
申请人： Lacey E. Scoggins , Kenneth C. Hoover , Wei-Teh W. Shangi
发明人： Lacey E. Scoggins , Kenneth C. Hoover , Wei-Teh W. Shangi
IPC分类号： C08G75/02 , C08G75/20
CPC分类号： C08G75/20 , C08G75/0236 , C08G75/0259
摘要： A process is provided for the production of aromatic sulfide/sulfone polymers which comprises contacting under suitable polymerization reaction conditions: (1) at least one dihaloaromatic sulfone, (2) water, and (3) a complex comprising at least one alkali metal hydrosulfide.
摘要翻译：提供用于生产芳族硫化物/砜聚合物的方法，其包括在合适的聚合反应条件下接触：（1）至少一种二卤代芳砜，（2）水和（3）包含至少一种碱金属氢硫化物的络合物。

5. 发明授权

US5171831A Producing high molecular weight poly(arylene sulfide) polymers by adding second polar solvent prior to termination of polymerization 失效
标题翻译：通过在聚合终止前加入第二极性溶剂生产高分子量聚（亚芳基硫醚）聚合物
公开(公告)号：US5171831A
公开(公告)日：1992-12-15
申请号：US621413
申请日：1990-12-03
申请人： Afif M. Nesheiwat , Kenneth C. Hoover
发明人： Afif M. Nesheiwat , Kenneth C. Hoover
IPC分类号： C08G75/02
CPC分类号： C08G75/0259 , C08G75/0277 , C08G75/0286
摘要： A process for producing an easily recoverable poly(arylene sulfide) polymer having a melt flow of less than 130 g/10 min., which processes comprises:a) adding a second polar organic compound to a polymerization reaction mixture during polymerization immediately prior to termination of said polymerization, wherein said polymerization reaction mixture is formed by reacting reactants comprising a dihaloaromatic compound, a sulfur source and a first polar organic compound under suitable polymerization conditions, and wherein the molar ratio of second polar organic compound added to first polar organic compound is in the range of 0.05 to 2; and thereafterb) terminating said polymerization; andc) recovering said polymer.
摘要翻译：熔融流动小于130克/ 10分钟的容易恢复的聚（亚芳基硫醚）聚合物的制备方法，该方法包括：a）在终止前立即在聚合反应混合物中加入第二极性有机化合物的所述聚合反应，其中所述聚合反应混合物通过在合适的聚合条件下使包含二卤代芳族化合物，硫源和第一极性有机化合物的反应物反应而形成，并且其中加入第一极性有机化合物的第二极性有机化合物的摩尔比为在0.05〜2的范围内; 然后b）终止所述聚合; 和c）回收所述聚合物。

6. 发明授权

US5110902A Aromatic sulfide/sulfone polymer production with complex of alkali metal hydrosulfide and alkali metal amino alkanoate 失效
标题翻译：芳香硫化物/砜聚合物生产与碱金属氢硫化物和碱金属氨基链烷酸酯的复合物
公开(公告)号：US5110902A
公开(公告)日：1992-05-05
申请号：US673616
申请日：1991-03-22
申请人： Lacey E. Scoggins , Kenneth C. Hoover
发明人： Lacey E. Scoggins , Kenneth C. Hoover
IPC分类号： C08G75/02 , C08G75/20
CPC分类号： C08G75/20 , C08G75/0236 , C08G75/0259
摘要： A process is provided for the production of aromatic sulfide-sulfone polymers which comprises contacting under suitable polymerization reaction conditions: (1) at least one dihaloaromatic sulfone, (2) water, and (3) a complex comprising at least one alkali metal hydrosulfide.
摘要翻译：提供用于生产芳族硫醚砜聚合物的方法，其包括在合适的聚合反应条件下接触：（1）至少一种二卤代芳砜，（2）水和（3）包含至少一种碱金属氢硫化物的络合物。

7. 发明授权

US4839411A Solid state curing of poly(arylene sulfide) resins in reduced oxygen atmospheres 失效
标题翻译：减少氧气氛中聚（亚芳基硫醚）树脂的固态固化
公开(公告)号：US4839411A
公开(公告)日：1989-06-13
申请号：US99870
申请日：1987-09-22
申请人： Kenneth C. Hoover , Fred T. Sherk , Joseph E. Figard
发明人： Kenneth C. Hoover , Fred T. Sherk , Joseph E. Figard
IPC分类号： C08L81/02 , C08G75/02 , C08G75/06 , C08J3/12 , C08J3/24 , C08K7/04 , C08K7/14 , C08K13/04
CPC分类号： C08J3/24 , C08G75/0295 , C08J3/12 , C08J2381/02
摘要： Virgin poly(arylene sulfide) resins are oxidatively cured by heat treatment at an elevated temperature below the melting point of the resin, under an oxidizing atmosphere comprising less than a 20 volume % oxygen concentration. The resulting polymer exhibits drastically improved thermal stability with no apparent sacrifice in physical properties.

8. 发明授权

US5110901A Higher molecular weight arylene sulfide resin and process for its preparation 失效
标题翻译：较高分子量的亚芳基硫醚树脂及其制备方法
公开(公告)号：US5110901A
公开(公告)日：1992-05-05
申请号：US580720
申请日：1990-09-11
申请人： Kenneth C. Hoover , Earl Clark, Jr. , Roy E. Reger , Lacey E. Scoggins , Afif M. Nesheiwat
发明人： Kenneth C. Hoover , Earl Clark, Jr. , Roy E. Reger , Lacey E. Scoggins , Afif M. Nesheiwat
IPC分类号： C08G75/02
CPC分类号： C08G75/0259
摘要： In a first embodiment, arylene sulfide resins are provided by contacting, in a polymerization mixture, during a polymerization process, reactants comprising: an alkali metal sulfide, an organic amide, an alkali metal carboxylate, water and a monomer source which comprises at least one dihaloaromatic compound. The amount of alkali metal carboxylate present during the polymerization process ranges from about 0.01 to about 0.03 mole per each mole of sulfur present in the resulting arylene sulfide resin. The total amount of water present during the polymerization process ranges from about 1.02 to about 2.1 moles per each mole of sulfur present in the resulting arylene sulfide resin.In a second embodiment, arylene sulfide resins are provided by contacting, in a polymerization mixture, during a polymerization process, reactants comprising: an alkali metal sulfide, an organic amide, an alkali metal carboxylate, water and a monomer source which comprises a mixture of at least one dihaloaromatic compound and at least one polyhaloaromatic compound having more than two halogen substituents per molecule. The ranges of the amount of alkali metal carboxylate present during the polymerization process and the total amount of water present during the polymerization process are identical to those amounts disclosed in the first embodiment. The amount of polyhaloaromatic compound initially present ranges from about 0.0001 to about 0.01 mole per each mole of dihaloaromatic compound present prior to the initiation of the polymerization process.
摘要翻译：在第一个实施方案中，亚芳基硫醚树脂通过在聚合反应过程中使聚合反应中的反应物与碱金属硫化物，有机酰胺，碱金属羧酸盐，水和单体源接触来提供，所述反应物包括至少一种二卤化合物。在聚合过程中存在的碱金属羧酸盐的量为所得亚芳基硫醚树脂中存在的每摩尔硫的约0.01至约0.03摩尔。在聚合过程中存在的水的总量范围为所得亚芳基硫醚树脂中存在的每摩尔硫的约1.02至约2.1摩尔。在第二个实施方案中，亚芳基硫醚树脂是通过在聚合反应过程中使聚合反应中的反应物与碱金属硫化物，有机酰胺，碱金属羧酸盐，水和单体来源接触来提供的，至少一种二卤代芳族化合物和每分子具有多于两个卤素取代基的至少一种多卤芳族化合物。在聚合过程中存在的碱金属羧酸盐的量的范围和在聚合过程中存在的水的总量与第一实施方案中公开的量相同。在开始聚合过程之前，存在的每摩尔二卤代芳族化合物最初存在的多卤代芳族化合物的量为约0.0001至约0.01摩尔。

9. 发明授权

US5015725A Aromatic sulfide/sulfone polymer production 失效
标题翻译：芳香族硫化物/砜聚合物生产
公开(公告)号：US5015725A
公开(公告)日：1991-05-14
申请号：US401595
申请日：1989-08-31
申请人： Lacey E. Scoggins , Kenneth C. Hoover , Wei-Teh Wade Shang
发明人： Lacey E. Scoggins , Kenneth C. Hoover , Wei-Teh Wade Shang
IPC分类号： C08G75/02 , C08G75/20
CPC分类号： C08G75/0236 , C08G75/0259 , C08G75/20
摘要： A process is provided for the production of aromatic sulfide/sulfone polymers which comprises contacting under suitable polymerization reaction conditions: (1) at least one dihaloaromatic sulfone, (2) water, and (3) a complex comprising at least one alkali metal hydrosulfide.
摘要翻译：提供用于生产芳族硫化物/砜聚合物的方法，其包括在合适的聚合反应条件下接触：（1）至少一种二卤代芳砜，（2）水和（3）包含至少一种碱金属氢硫化物的络合物。

10. 发明授权

US4958004A Aromatic sulfide/sulfone polymer production 失效
标题翻译：芳香族硫化物/砜聚合物生产
公开(公告)号：US4958004A
公开(公告)日：1990-09-18
申请号：US80283
申请日：1987-07-31
申请人： Kenneth C. Hoover , Lacey E. Scoggins , Wei-Tech W. Shang , Afif M. Nesheiwat
发明人： Kenneth C. Hoover , Lacey E. Scoggins , Wei-Tech W. Shang , Afif M. Nesheiwat
IPC分类号： C08G75/00 , C08G75/02 , C08G75/06 , C08G75/20
CPC分类号： C08G75/0259 , C08G75/0236 , C08G75/20
摘要： A process is provided for the production of aromatic sulfide/sulfone polymers which involves contacting under suitable polymerization reaction conditions: (1) at least one dihaloaromatic sulfone, (2) at least one organic amide, (3) at least one alkali metal hydrosulfide, (4) water, and (5) at least one member selected from the group consisting of (a) alkali metal carbonates and (b) mixtures of alkali metal carbonates with alkali metal hydroxides wherein said mixtures have at least about 0.5 mole percent alkali metal carbonate.

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