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1. 发明授权

US5420039A Control of continuous microwave digestion process 失效
标题翻译：控制连续微波消解过程
公开(公告)号：US5420039A
公开(公告)日：1995-05-30
申请号：US999295
申请日：1992-12-31
申请人： Brian W. Renoe , Edward E. King , Dale A. Yurkovich
发明人： Brian W. Renoe , Edward E. King , Dale A. Yurkovich
IPC分类号： C02F1/30 , B01J19/12 , G01N1/00 , G01N1/28 , G01N1/44 , G01N27/22 , G01N35/08
CPC分类号： B01J19/126 , G01N1/44 , B01J2219/1218 , Y10T436/117497 , Y10T436/25125
摘要： A process and apparatus for controlled continuous microwave digestion of samples of materials to prepare them for subsequent analyses or other chemical operations. The material to be analyzed, in finely divided form and mixed with digesting liquid, such as a strong acid, is charged as a slug into a flowing liquid carrier stream, usually water, which stream, containing the slug, is passed in a tube through a zone in which the tube and contents are subjected to microwave radiation, to heat the digesting liquid and the material to be digested to promote the digestion. The process and apparatus are modified by inclusion of detecting and controlling steps and corresponding apparatus components to detect a condition of the flowing liquid without physically contacting it, as by determining the dielectric constant of contents of the tube, or a related property of such contents at one or more locations of the tube, usually outside the microwave zone, and controlling operations of the process and apparatus accordingly. Such controlled or controllable operations include charging of subsequent slugs to the system, feeding digested slugs or portions thereof to an autosampler, and backwashing of a filter, and in such operations the controlling device is preferably a microprocessor or computer activated by signals from the detection component and automatically operates appropriate valves, pumps and autosampler. Also within the invention is a procedure for converting a manual process, such as that described to an automatic one.
摘要翻译：用于受控连续微波消解材料样品以制备其用于随后分析或其他化学操作的方法和装置。待分析的材料以细分散的形式并与消化液（例如强酸）混合，作为块状物装入流动的液体载体物流中，通常是水，其中流动的物料流通过管道管和内容物经受微波辐射的区域，以加热消化液体和待消化的材料以促进消化。通过包括检测和控制步骤以及相应的装置部件来修改过程和装置，以便通过确定管的内容物的介电常数或这些内容物的相关性质来检测流动的液体的状态而不物理接触管的一个或多个位置，通常在微波区外，并相应地控制过程和装置的操作。这种受控或可控制的操作包括将后续的塞子充电到系统中，将消化的塞子或其部分进给到自动进样器，以及过滤器的反冲洗，并且在这种操作中，控制装置优选地是由来自检测部件的信号激活的微处理器或计算机并自动运行适当的阀门，泵和自动进样器。在本发明中也是将手动过程（例如所描述的过程）转换为自动过程的过程。

2. 发明申请

US20110102002A1 ELECTRODE AND SENSOR HAVING CARBON NANOSTRUCTURES 审中-公开
标题翻译：具有碳纳米管结构的电极和传感器
公开(公告)号：US20110102002A1
公开(公告)日：2011-05-05
申请号：US12889019
申请日：2010-09-23
申请人： Bill L. Riehl , Bonnie D. Riehl , Edward E. King , Jay M. Johnson , Kevin T. Schlueter
发明人： Bill L. Riehl , Bonnie D. Riehl , Edward E. King , Jay M. Johnson , Kevin T. Schlueter
IPC分类号： G01R27/08 , H01B5/00 , C40B60/12 , B82Y30/00
CPC分类号： H01G11/36 , B82Y30/00 , B82Y40/00 , C01B32/15 , C01B32/152 , G01N27/3277 , H01G9/058 , H01M8/16 , Y02E60/13 , Y02E60/527
摘要： An active electrode structure is disclosed that includes fullerenes produced by a carbo-thermal carbide conversion of a conductive carbide without a metal catalyst. Also disclosed is an electrode that includes a fullerene covalently bonded to a conductive carbide, the fullerene being an aligned or non-aligned array. The carbide substrate having a surface coating of covalently bonded fullerenes is characterized in that the peak separation of a cyclic voltammogram for the conductive carbide having a surface layer of the fullerene is less than about 150 mV at a scan rate of 5 mV/s in a 4 mM ferricyanide, 1M KCl solution. The fullerene may include about 50% or less non-crystalline carbon and about 5% or less of a transition metal that interferes with the ability of the active electrode structure to transfer electrons or detect an analyte.
摘要翻译：公开了一种活性电极结构，其包括通过不含金属催化剂的导电碳化物的碳 - 碳化碳转化产生的富勒烯。还公开了一种电极，其包括共价键合到导电碳化物的富勒烯，所述富勒烯是对准或非排列的阵列。具有共价键合的富勒烯的表面涂层的碳化物衬底的特征在于，具有富勒烯的表面层的导电碳化物的循环伏安图的峰值分离在5mV / s的扫描速率下小于约150mV 4mM铁氰化物，1M KCl溶液。富勒烯可以包括大约50％或更少的非结晶碳和约5％或更少的干扰活性电极结构转移电子或检测分析物的能力的过渡金属。

3. 发明授权

US07125721B2 Method and apparatus for rapid fat content determination 有权
公开(公告)号：US07125721B2
公开(公告)日：2006-10-24
申请号：US10065173
申请日：2002-09-24
申请人： Michael J. Collins , Edward E. King
发明人： Michael J. Collins , Edward E. King
IPC分类号： G01N33/02
CPC分类号： G01N24/08 , G01N1/44 , G01N5/04 , G01N24/081 , G01N24/085 , G01N33/06 , G01R33/44
摘要： A sample for NMR measurement of moisture and fat and oil contents is disclosed. The sample includes an organic portion containing at least some fats and oils, a pad that is substantially transparent to microwave radiation and is free of atoms that would interfere with or mask the NMR response of the protons in the fats and oils in the sample, and a sheet material that is free of atoms that would interfere with or mask the NMR response of the protons in the fats and oils in the sample, with the sheet material being wrapped around the organic portion and the pad.

4. 发明授权

US4356078A Process for blending coal with water immiscible liquid 失效
标题翻译：煤与水混溶液混合的工艺
公开(公告)号：US4356078A
公开(公告)日：1982-10-26
申请号：US184762
申请日：1980-09-08
申请人： Leonard J. Heavin , Edward E. King , Dennis L. Milliron
发明人： Leonard J. Heavin , Edward E. King , Dennis L. Milliron
IPC分类号： B65G51/04 , B65G53/30 , C10G1/00 , C10L20060101 , C10L1/32
CPC分类号： C10L1/322 , C10G1/00 , Y10T137/0391
摘要： A continuous process for blending coal with a water immiscible liquid produces a uniform, pumpable slurry. Pulverized raw feed coal and preferably a coal derived, water immiscible liquid are continuously fed to a blending zone (12 and 18) in which coal particles and liquid are intimately admixed and advanced in substantially plug flow to form a first slurry. The first slurry is withdrawn from the blending zone (12 and 18) and fed to a mixing zone (24) where it is mixed with a hot slurry to form the pumpable slurry. A portion of the pumpable slurry is continuously recycled to the blending zone (12 and 18) for mixing with the feed coal.
摘要翻译：将煤与水不混溶的液体混合的连续方法产生均匀的可泵送浆料。将粉碎的原料煤，优选煤衍生的，与水不混溶的液体连续地进料到混合区（12和18）中，其中煤颗粒和液体以基本上的活塞流紧密混合并前进以形成第一浆料。将第一浆料从共混区域（12和18）中取出并进料至混合区（24），在此混合区域与热浆料混合以形成可泵送的浆料。可泵送浆料的一部分被连续地再循环到混合区（12和18）以与进料煤混合。

5. 发明申请

US20100321046A1 WIPEABLE CONDUCTIVITY PROBE AND METHOD OF MAKING SAME 审中-公开
标题翻译：无线电导率探头及其制作方法
公开(公告)号：US20100321046A1
公开(公告)日：2010-12-23
申请号：US12814520
申请日：2010-06-14
申请人： Robert C. Randall , Christopher J. Palassis , Michael T. James , Edward E. King , Ben E. Barnett
发明人： Robert C. Randall , Christopher J. Palassis , Michael T. James , Edward E. King , Ben E. Barnett
IPC分类号： G01R27/08 , G01K1/00 , G01R3/00
CPC分类号： G01N27/07 , G01N33/18 , Y10T29/49002
摘要： A conductivity sensor is disclosed that comprises a forked electrode support that includes a first opposing arm and a second opposing arm spaced apart by a slot. Both the first arm and the second arm include a plurality of electrodes embedded in each arm. The first and second arms and the slot are capable of retaining a volume of fluid within the volume defined by the arms and the slot such that the conductivity of the fluid in the slot can be determined. The conductivity sensor is wipeable by a reciprocating wiper assembly positioned adjacent the forked electrode support such that the wiper element can travel through the slot and remove contaminants from the slot and the plurality of electrodes in each of the first and second arms. Also disclosed are methods of making the conductivity sensor.
摘要翻译：公开了一种电导率传感器，其包括叉形电极支撑件，其包括第一相对臂和由槽隔开的第二相对臂。第一臂和第二臂都包括嵌入每个臂中的多个电极。第一和第二臂和槽能够将一定体积的流体保持在由臂和狭槽限定的体积内，使得槽中的流体的导电性能被确定。电导率传感器可通过邻近叉形电极支架定位的往复式擦拭器组件进行擦拭，使得擦拭器元件能够穿过狭槽并从第一和第二臂中的每一个中的槽和多个电极中去除污染物。还公开了制造电导率传感器的方法。

6. 发明授权

US5840583A Microwave assisted chemical processes 失效
公开(公告)号：US5840583A
公开(公告)日：1998-11-24
申请号：US924628
申请日：1997-09-05
申请人： David A. Barclay , William Edward Jennings , Edward E. King
发明人： David A. Barclay , William Edward Jennings , Edward E. King
IPC分类号： G01N31/00 , B01J19/00 , B01J19/12 , G01N1/28 , G01N1/44 , G01N33/00 , G01N1/00 , G01N33/20 , G01N35/08
CPC分类号： B01J19/126 , B01J19/0013 , G01N1/44 , B01J2219/00063 , B01J2219/00101 , B01J2219/00141 , B01J2219/00162 , B01J2219/1218 , Y10T436/12 , Y10T436/16 , Y10T436/17 , Y10T436/176152 , Y10T436/176921 , Y10T436/25 , Y10T436/25125
摘要： A method for microwave assisted chemical processes is disclosed that comprises applying sufficient microwave radiation to a temperature-monitored mixture of reagents, with at least one of the reagents being thermally responsive to electromagnetic radiation in the microwave range, and based on the monitored temperature, to maintain the added reagents at or closely about a predetermined temperature while substantially avoiding thermal dilution (or before substantial thermal dilution can occur) that otherwise would have been caused by the addition of the reagents to one another.

7. 发明授权

US08530239B2 Sample combination for NMR measurements of fats and oils 有权
标题翻译：脂肪和油的NMR测量样品组合
公开(公告)号：US08530239B2
公开(公告)日：2013-09-10
申请号：US11486678
申请日：2006-07-14
申请人： Michael J. Collins , Edward E. King
发明人： Michael J. Collins , Edward E. King
IPC分类号： G01N33/02
CPC分类号： G01N24/08 , G01N1/44 , G01N5/04 , G01N24/081 , G01N24/085 , G01N33/06 , G01R33/44
摘要： A method and apparatus for rapidly and accurately determining the fat and oil content of a sample using microwave drying and NMR analysis is disclosed. The method and apparatus incorporate a low mass, porous, hydrophilic and lipophilic sample pad that ensures that the entire sample is subjected to NMR analysis. The method and apparatus according to the invention are suitable for rapidly determining the fat and oil content of samples collected during a production process and for process or quality control.
摘要翻译：公开了一种使用微波干燥和NMR分析快速准确地测定样品的油脂含量的方法和装置。该方法和设备结合了低质量，多孔，亲水和亲脂性样品垫，确保整个样品进行NMR分析。根据本发明的方法和设备适用于快速测定在生产过程中收集的样品的脂肪和油含量以及过程或质量控制。

8. 发明授权

US06548303B2 Method and apparatus for rapid fat content determination 有权
公开(公告)号：US06548303B2
公开(公告)日：2003-04-15
申请号：US09603487
申请日：2000-06-23
申请人： Michael J. Collins , Edward E. King
发明人： Michael J. Collins , Edward E. King
IPC分类号： G01N3306
CPC分类号： G01N24/08 , G01N1/44 , G01N5/04 , G01N24/081 , G01N24/085 , G01N33/06 , G01R33/44
摘要： A method and apparatus for rapidly and accurately determining the fat and oil content of a sample using microwave drying and NMR analysis is disclosed. The method and apparatus incorporate a low mass, porous, hydrophilic and lipophilic sample pad that ensures that the entire sample is subjected to NMR analysis. The method and apparatus according to the invention are suitable for rapidly determining the fat and oil content of samples collected during a production process and for process or quality control.

9. 发明申请

US20100252450A1 ELECTRODE AND SENSOR HAVING CARBON NANOSTRUCTURES 审中-公开
标题翻译：具有碳纳米管结构的电极和传感器
公开(公告)号：US20100252450A1
公开(公告)日：2010-10-07
申请号：US12763799
申请日：2010-04-20
申请人： Bill L. Riehl , Bonnie D. Riehl , Edward E. King , Jay M. Johnson , Kevin T. Schlueter
发明人： Bill L. Riehl , Bonnie D. Riehl , Edward E. King , Jay M. Johnson , Kevin T. Schlueter
IPC分类号： G01N27/26 , C25B11/04
CPC分类号： B82Y30/00 , B82Y15/00 , B82Y40/00 , C01B32/152 , C01B32/16 , C01B32/18 , C01B2202/36 , G01N27/3278 , H01M8/0234
摘要： An active electrode structure is disclosed that includes fullerenes produced by conversion from a carbide. Also disclosed is an electrode that includes a fullerene covalently bonded to a carbide, the fullerene being an aligned or non-aligned array. The fullerene is included in an active electrode structure of the electrode that also includes about 50% or less non-crystalline carbon and about 5% or less of a transition metal that interferes with the ability of the active electrode structure to transfer electrons or detect an analyte. The active electrode substrate or the electrode may be included in a sensor.
摘要翻译：公开了一种活性电极结构，其包括通过从碳化物转化而产生的富勒烯。还公开了一种电极，其包括共价键合到碳化物上的富勒烯，所述富勒烯是对准或不排列的阵列。富勒烯包括在电极的有源电极结构中，其还包括约50％或更少的非结晶碳和约5％或更少的干扰有源电极结构转移电子的能力的过渡金属或检测分析物。有源电极基板或电极可以包括在传感器中。

10. 发明授权

US07220591B2 Method and apparatus for rapid fat content determination 有权
标题翻译：用于快速脂肪含量测定的方法和装置
公开(公告)号：US07220591B2
公开(公告)日：2007-05-22
申请号：US10852621
申请日：2004-05-24
申请人： Michael J. Collins , Edward E. King
发明人： Michael J. Collins , Edward E. King
IPC分类号： G01N33/06 , G01N24/00
CPC分类号： G01R33/44 , G01N24/081 , G01N24/085 , Y10T436/24
摘要： A method and apparatus for rapidly and accurately determining the fat and oil content of a sample using microwave drying and NMR analysis is disclosed. The method and apparatus incorporate a low mass, porous, hydrophilic and lipophilic sample pad that ensures that the entire sample is subjected to NMR analysis. The method and apparatus according to the invention are suitable for rapidly determining the fat and oil content of samples collected during a production process and for process or quality control.
摘要翻译：公开了一种使用微波干燥和NMR分析快速准确地测定样品的油脂含量的方法和装置。该方法和设备结合了低质量，多孔，亲水和亲脂性样品垫，确保整个样品进行NMR分析。根据本发明的方法和设备适用于快速测定在生产过程中收集的样品的脂肪和油含量以及过程或质量控制。

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