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1. 发明授权

US5114612A Liquid crystal polyester thermosets 失效
标题翻译：液晶聚酯热固性材料
公开(公告)号：US5114612A
公开(公告)日：1992-05-19
申请号：US644856
申请日：1991-01-22
申请人： Brian C. Benicewicz , Andrea E. Hoyt
发明人： Brian C. Benicewicz , Andrea E. Hoyt
IPC分类号： C08G63/52 , C08G63/682 , C08G63/685 , C09K19/38
CPC分类号： C08G63/6858 , C08G63/52 , C08G63/6828 , C09K19/3804 , C09K19/3823
摘要： The present invention provides (1) curable liquid crystalline polyester monomers represented by the formula:R.sup.1 --A.sup.1 --B.sup.1 --A.sup.2 --B.sup.2 --A.sup.3 --R.sup.2where R.sup.1 and R.sup.2 are radicals selected from the group consisting of maleimide, substituted maleimide, nadimide, substituted naimide, ethynyl, and (C(R.sup.3).sub.2).sub.2 where R.sup.3 is hydrogen with the proviso that the two carbon atoms of (C(R.sup.3).sub.2).sub.2 are bound on the aromatic ring of A.sup.1 or A.sup.3 to adjacent carbon atoms, A.sup.1 and A.sup.3 are 1,4-phenylene and the same where said group contains one or more substituents selected from the group consisting of halo, e.g., fluoro, chloro, bromo, or iodo, nitro lower alkyl, e.g., methyl, ethyl, or propyl, alkoxy, e.g., methoxy, ethoxy, or propoxy, and fluoroalkyl, e.g., trifluoromethyl, pentafluoroethyl and the like, A.sup.2 is selected from the group consisting of 1,4-phenylene, 4,4'-biphenyl, 2,6-naphthylene and the same where said groups contain one or more substituents selected from the group consisting of halo, e.g., fluoro, chloro, bromo, or iodo, nitro, lower alkyl, e.g., methyl, ethyl, and propyl, lower alkoxy, e.g., methoxy, ethoxy, or propoxy, and fluoroalkyl or fluoroalkoxy, e.g., trifluoromethyl, pentafluoroethyl and the like, and B.sup.1 and B.sup.2 are selected from the group consisting of --C(O)--O-- and --O--C(O)--, (2) thermoset liquid crystalline polyester compositions comprised of heat-cured segments derived from monomers represented by the formula:R.sup.1 --A.sup.1 --B.sup.1 --A.sup.2 --B.sup.2 --A.sup.3 --R.sup.2as described above, (3) curable blends of at least two of the polyester monomers and (4) processes of preparing the curable liquid crystalline polyester monomers.
摘要翻译：本发明提供（1）由式：R1-A1-B1-A2-B2-A3-R2表示的可固化液晶聚酯单体，其中R 1和R 2是选自马来酰亚胺，取代的马来酰亚胺，（C（R3）2）2的两个碳原子在A1或A3的芳香环上键合到相邻的碳原子上，A1（A1）和A3是1,4-亚苯基，并且相同，其中所述基团含有一个或多个选自卤素，例如氟，氯，溴或碘，硝基低级烷基，例如甲基，乙基或丙基的取代基，烷氧基，例如甲氧基，乙氧基或丙氧基，以及氟代烷基，例如三氟甲基，五氟乙基等，A2选自1,4-亚苯基，4,4'-联苯基，2,6-亚萘基并且相同，其中所述基团含有一个或多个选自卤素，例如氟，氯，溴或碘，硝基，低级烷基，例如甲基，乙基和丙基，低级烷氧基，例如甲氧基，乙氧基或丙氧基，氟代烷基或氟代烷氧基，例如三氟甲基，五氟乙基等，而B1和B2选自由-C（O）-O-和-OC（O） - 组成的组，（2）热固性液晶聚酯组合物，其由衍生自由下式表示的单体的热固化链段组成：R1-A1-B1-A2-B2 -A 3-R 2，（3）至少两种聚酯单体的可固化共混物和（4）制备可固化液晶聚酯单体的方法。

2. 发明授权

US5198551A Polyamide thermosets 失效
标题翻译：聚酰胺热固性材料
公开(公告)号：US5198551A
公开(公告)日：1993-03-30
申请号：US711721
申请日：1991-06-07
申请人： Brian C. Benicewicz , Andrea E. Hoyt
发明人： Brian C. Benicewicz , Andrea E. Hoyt
IPC分类号： C07D207/44 , C07D207/452 , C07D209/76 , C08G73/14
CPC分类号： C07D207/452 , C07D209/76 , C08G73/14
摘要： The present invention provides (1) curable polyamide monomers represented by the formula: R.sup.1 -A.sup.1 -B.sup.1 -A.sup.2 -B.sup.2 -A.sup.3 -R.sup.2 where R.sup.1 and R.sup.2 are radicals selected from the group consisting of maleimide, substituted maleimide, nadimide, substituted nadimide, ethynyl, and (C(R.sup.3).sub.2).sub.2 where R.sup.3 is hydrogen with the proviso that the two carbon atoms of (C(R.sup.3).sub.2).sub.2 are bound on the aromatic ring of A.sup.1 or A.sup.3 to adjacent carbon atoms, A.sup.1 and A.sup.3 are 1,4-phenylene and the same where said group contains one or more substituents selected from the group consisting of halo, e.g., fluoro, chloro, bromo, or iodo, nitro, lower alkyl, e.g., methyl, ethyl, and propyl, lower alkoxy, e.g., methoxy, ethoxy, or propoxy, and fluoroalkyl or fluoroalkoxy, e.g., trifluoromethyl, pentafluoroethyl and the like, A.sup.2 is selected from the group consisting of 1,4-phenylene, 4,4'-biphenyl, 2,6-naphthylene and the same where said groups contain one or more substitutents selected from the group consisting of halo, e.g., fluoro, chloro, bromo, or iodo, nitro, lower alkyl, e.g., methyl, ethyl, and propyl, lower alkoxy, e.g., methoxy, ethoxy, or propoxy, and fluoroalkyl or fluoroalkoxy, e.g., trifluoromethyl, pentafluoroethyl and the like, and B.sup.1 and B.sup.2 are selected from the group consisting of --C(O)--N(H)-- and --N(H)--C(O)--, (2) thermoset polyamide compositions comprised of cured segments derived from monomers represented by the formula: R.sup.1 -A.sup.1 -B.sup.1 -A.sup.2 -B.sup.2 -A.sup.3 -R.sup.2 as described above, and curable blends of at least two of the polyamide monomers and (4) processes of preparing the curable polyamide monomers.
摘要翻译：本发明提供（1）由式：R1-A1-B1-A2-B2-A3-R2表示的可固化的聚酰胺单体，其中R 1和R 2是选自马来酰亚胺，取代的马来酰亚胺，酰亚胺，取代的酰亚胺，乙炔基和（C（R3）2）2，其中R3是氢，条件是（C（R3）2）2的两个碳原子在A1或A3的芳环上键合成相邻的碳原子，A1和A3 是1,4-亚苯基，并且相同，其中所述基团含有一个或多个选自卤素，例如氟，氯，溴或碘，硝基，低级烷基，例如甲基，乙基和丙基的取代基，低级烷氧基，例如甲氧基，乙氧基或丙氧基，以及氟代烷基或氟代烷氧基，例如三氟甲基，五氟乙基等，A2选自1,4-亚苯基，4,4'-联苯基，2,6 - 亚乙基，并且相同，其中所述基团含有一个或多个选自卤素，例如氟，氯，溴的取代基低级烷基，例如甲基，乙基和丙基，低级烷氧基，例如甲氧基，乙氧基或丙氧基，氟代烷基或氟代烷氧基，例如三氟甲基，五氟乙基等，而B1和B2是选自-C（O）-N（H） - 和-N（H）-C（O） - ，（2）热固性聚酰胺组合物，其包含衍生自由式R1- 如上所述的A1-B1-A2-B2-A3-R2，以及至少两种聚酰胺单体的可固化共混物和（4）制备可固化聚酰胺单体的方法。

3. 发明授权

US5315011A Polyamide thermosets 失效
标题翻译：聚酰胺热固性材料
公开(公告)号：US5315011A
公开(公告)日：1994-05-24
申请号：US941815
申请日：1992-09-08
申请人： Brian C. Benicewicz , Andrea E. Hoyt
发明人： Brian C. Benicewicz , Andrea E. Hoyt
IPC分类号： C07D207/44 , C07D207/452 , C07D209/76 , C08G73/14 , C07D403/10
CPC分类号： C07D207/452 , C07D209/76 , C08G73/14
摘要： The present invention provides (1) curable polyamide monomers represented by the formula: R.sup.1 --A.sup.1 --B.sup.1 --A.sup.2 --B.sup.2 --A.sup.3 --R.sup.2 where R.sup.1 and R.sup.2 are radicals selected from the group consisting of maleimide, substituted maleimide, nadimide, substituted nadimide, ethynyl, and (C(R.sup.3).sub.2).sub.2 where R.sub.3 is hydrogen with the proviso that the two carbon atoms of (C(R.sup.3).sub.2).sub.2 are bound on the aromatic ring of A.sup.1 or A.sup.3 to adjacent carbon atoms, A.sup.1 and A.sup.3 are 1,4-phenylene and the same where said group contains one or more substituents selected from the group consisting of halo, e.g., fluoro, chloro, bromo, or iodo, nitro, lower alkyl, e.g., methyl, ethyl, and propyl, lower alkoxy, e.g., methoxy, ethoxy, or propoxy, and fluoroalkyl or fluoroalkoxy, e.g., trifluoromethyl, pentafluoroethyl and the like, A.sup.2 is selected from the group consisting of 1,4-phenylene, 4,4'-biphenyl, 2,6-naphthylene and the same where said groups contain one or more substituents selected from the group consisting of halo, e.g., fluoro, chloro, bromo, or iodo, nitro, lower alkyl, e.g., methyl, ethyl, and propyl, lower alkoxy, e.g., methoxy, ethoxy, or propoxy, and fluoroalkyl or fluoroalkoxy, e.g., trifluoromethyl, pentafluoroethyl and the like, and B.sup.1 and B.sup.2 are selected from the group consisting of --C(O)--N(H)-- and --N(H)--C(O)--, (2) thermoset polyamide compositions comprised of cured segments derived from monomers represented by the formula: R.sup.1 --A.sup.1 --B.sup.1 --A.sup.2 --B.sup.2 --A.sup.3 --R.sup.2 as described above, and curable blends of at least two of the polyamide monomers and (4) processes of preparing the curable polyamide monomers.
摘要翻译：本发明提供（1）由式：R1-A1-B1-A2-B2-A3-R2表示的可固化的聚酰胺单体，其中R 1和R 2是选自马来酰亚胺，取代的马来酰亚胺，酰亚胺，取代的酰亚胺，乙炔基和（C（R3）2）2，其中R3是氢，条件是（C（R3）2）2的两个碳原子在A1或A3的芳环上键合成相邻的碳原子，A1和A3 是1,4-亚苯基，并且相同，其中所述基团含有一个或多个选自卤素，例如氟，氯，溴或碘，硝基，低级烷基，例如甲基，乙基和丙基的取代基，低级烷氧基，例如甲氧基，乙氧基或丙氧基，以及氟代烷基或氟代烷氧基，例如三氟甲基，五氟乙基等，A2选自1,4-亚苯基，4,4'-联苯基，2,6 - 亚乙烯基，其中所述基团含有一个或多个选自卤素，例如氟，氯，溴的取代基 O或碘，硝基，低级烷基，例如甲基，乙基和丙基，低级烷氧基，例如甲氧基，乙氧基或丙氧基，氟代烷基或氟代烷氧基，例如三氟甲基，五氟乙基等，而B1和B2是选自-C（O）-N（H） - 和-N（H）-C（O） - ，（2）热固性聚酰胺组合物，其包含衍生自由式R1- 如上所述的A1-B1-A2-B2-A3-R2，以及至少两种聚酰胺单体的可固化共混物和（4）制备可固化聚酰胺单体的方法。

4. 发明授权

US5795993A Acoustic-wave sensor for ambient monitoring of a photoresist-stripping agent 失效
标题翻译：用于光致抗蚀剂剥离剂环境监测的声波传感器
公开(公告)号：US5795993A
公开(公告)日：1998-08-18
申请号：US564764
申请日：1995-11-29
申请人： Kent B. Pfeifer , Andrea E. Hoyt , Gregory C. Frye
发明人： Kent B. Pfeifer , Andrea E. Hoyt , Gregory C. Frye
IPC分类号： G01N29/02
CPC分类号： G01N29/022 , G01N2291/014 , G01N2291/0256 , G01N2291/02809 , G01N2291/02881 , G01N2291/0422 , G01N2291/0423 , G01N2291/0426 , G01N2291/0427
摘要： The acoustic-wave sensor. The acoustic-wave sensor is designed for ambient or vapor-phase monitoring of a photoresist-stripping agent such as N-methylpyrrolidinone (NMP), ethoxyethylpropionate (EEP) or the like. The acoustic-wave sensor comprises an acoustic-wave device such as a surface-acoustic-wave (SAW) device, a flexural-plate-wave (FPW) device, an acoustic-plate-mode (APM) device, or a thickness-shear-mode (TSM) device (also termed a quartz crystal microbalance or QCM) having a sensing region on a surface thereof. The sensing region includes a sensing film for sorbing a quantity of the photoresist-stripping agent, thereby altering or shifting a frequency of oscillation of an acoustic wave propagating through the sensing region for indicating an ambient concentration of the agent. According to preferred embodiments of the invention, the acoustic-wave device is a SAW device; and the sensing film comprises poly(vinylacetate), poly(N-vinylpyrrolidinone), or poly(vinylphenol).
摘要翻译：声波传感器。声波传感器设计用于光致抗蚀剂剥离剂如N-甲基吡咯烷酮（NMP），乙氧基乙基丙酸酯（EEP）等的环境或气相监测。声波传感器包括诸如表面声波（SAW）装置，弯曲板波（FPW）装置，声板模式（APM）装置或厚度 - 剪切模式（TSM）装置（也称为石英晶体微天平或QCM），其表面具有感测区域。感测区域包括用于吸收一定量的光致抗蚀剂剥离剂的感测膜，从而改变或移动通过感测区域传播的声波的振荡频率，以指示试剂的环境浓度。根据本发明的优选实施例，声波器件是SAW器件; 并且感测膜包括聚（乙酸乙烯酯），聚（N-乙烯基吡咯烷酮）或聚（乙烯基苯酚）。

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