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1. 发明授权

US08465858B2 Development of a novel method for preparation of PEMFC electrodes 有权
标题翻译：开发制备PEMFC电极的新方法
公开(公告)号：US08465858B2
公开(公告)日：2013-06-18
申请号：US11191605
申请日：2005-07-28
申请人： Branko N. Popov , Hansung Kim
发明人： Branko N. Popov , Hansung Kim
IPC分类号： H01M8/02 , H01M4/86 , H01M4/88 , H01M4/96
CPC分类号： H01M4/8853 , C25D3/50 , C25D5/18 , C25D5/54 , C25D7/00 , H01M4/8807 , H01M4/8882 , H01M4/92 , H01M4/926 , H01M8/1007
摘要： A method based on pulse electrodeposition technique was developed for preparation of membrane electrode assemblies (MEAs). In this approach, platinum is deposited directly on the surface of the carbon electrode. The method ensures most of the platinum to be in close contact with the membrane. Using this method it is possible to increase the Pt/C ratio up to 75 wt % near the surface of the electrode resulting in a 5 μm thick catalyst layer. The MEA prepared by pulse electrodeposition exhibits a current density of 0.33 A/cm2 at 0.8 V with platinum loading of 0.25 mg of Pt/cm2. The results indicate that pulse deposition may be an attractive technique to replace the conventional powder-type MEA preparation methods and help achieve industry goals of reducing catalyst cost and increasing efficiency in polymer electrode membrane fuel cells (PEMFCs).
摘要翻译：开发了基于脉冲电沉积技术的方法来制备膜电极组件（MEA）。在这种方法中，铂直接沉积在碳电极的表面上。该方法可确保大部分铂与膜紧密接触。使用该方法，可以在电极表面附近增加高达75重量％的Pt / C比，导致5μm厚的催化剂层。通过脉冲电沉积制备的MEA在0.8V下表现出0.33A / cm 2的电流密度，铂负载为0.25mg Pt / cm 2。结果表明，脉冲沉积可能是取代常规粉末MEA制备方法的有吸引力的技术，有助于实现降低催化剂成本和提高聚合物电极膜燃料电池（PEMFC）的效率的行业目标。

2. 发明授权

US07618915B2 Composite catalysts supported on modified carbon substrates and methods of making the same 有权
标题翻译：负载在改性碳基板上的复合催化剂及其制备方法
公开(公告)号：US07618915B2
公开(公告)日：2009-11-17
申请号：US11800978
申请日：2007-05-08
申请人： Branko N. Popov , Nalini Subramanian , Hector R. Colon-Mercado
发明人： Branko N. Popov , Nalini Subramanian , Hector R. Colon-Mercado
IPC分类号： B01J31/00 , B01J21/18
CPC分类号： B01J37/082 , B01J21/18 , B01J23/42 , B01J23/75 , B01J37/0203 , B01J37/0207 , H01M4/90 , H01M4/9083 , H01M2004/8689 , H01M2008/1095
摘要： A method of producing a composite carbon catalyst is generally disclosed. The method includes oxidizing a carbon precursor (e.g., carbon black). Optionally, nitrogen functional groups can be added to the oxidized carbon precursor. Then, the oxidized carbon precursor is refluxed with a non-platinum transitional metal precursor in a solution. Finally, the solution is pyrolyzed at a temperature of at least about 500° C.
摘要翻译：通常公开了复合碳催化剂的制造方法。该方法包括氧化碳前体（例如炭黑）。任选地，可将氮官能团加入到氧化碳前体中。然后，将氧化碳前体与溶液中的非铂过渡金属前体一起回流。最后，溶液在至少约500℃的温度下热解。

3. 发明申请

US20090142664A1 POLYPYRROLE AND SILVER VANADIUM OXIDE COMPOSITE 有权
标题翻译： POLYPYRROLE和SILVER VANADIUM OXIDE COMPOSITE
公开(公告)号：US20090142664A1
公开(公告)日：2009-06-04
申请号：US12090292
申请日：2006-10-17
申请人： Branko N. Popov , Jong-Won Lee
发明人： Branko N. Popov , Jong-Won Lee
IPC分类号： H01M4/60 , C08G73/06
CPC分类号： H01M4/54 , H01M4/06 , H01M4/364 , H01M4/382 , H01M4/60 , H01M4/606 , H01M6/16
摘要： In one embodiment of the present disclosure, a composite electrode for a battery is provided. The composite electrode includes silver vanadium oxide present in an amount from about 75 weight percent to about 99 weight percent and polypyrrole present in an amount from about 1 weight percent to about 25 weight percent.
摘要翻译：在本公开的一个实施例中，提供了一种用于电池的复合电极。复合电极包括以约75重量％至约99重量％的量存在的银钒氧化物，并且存在量为约1重量％至约25重量％的聚吡咯。

4. 发明申请

US20120168687A1 Polypyrrole and Silver Vanadium Oxide Composite 有权
标题翻译：聚吡咯和银氧化钒复合材料
公开(公告)号：US20120168687A1
公开(公告)日：2012-07-05
申请号：US13411976
申请日：2012-03-05
申请人： Branko N. Popov , Jong-Won Lee
发明人： Branko N. Popov , Jong-Won Lee
IPC分类号： H01B1/08 , H01B1/04
CPC分类号： H01M4/54 , H01M4/06 , H01M4/364 , H01M4/382 , H01M4/60 , H01M4/606 , H01M6/16
摘要： In one embodiment of the present disclosure, a composite electrode for a battery is provided. The composite electrode includes silver vanadium oxide present in an amount from about 75 weight percent to about 99 weight percent and polypyrrole present in an amount from about 1 weight percent to about 25 weight percent.
摘要翻译：在本公开的一个实施例中，提供了一种用于电池的复合电极。复合电极包括以约75重量％至约99重量％的量存在的银钒氧化物，并且存在量为约1重量％至约25重量％的聚吡咯。

5. 发明授权

US08133611B2 Method of making polypyrrole and silver vanadium oxide composite 有权
标题翻译：制备聚吡咯和银钒氧化物复合材料的方法
公开(公告)号：US08133611B2
公开(公告)日：2012-03-13
申请号：US12090292
申请日：2006-10-17
申请人： Branko N. Popov , Jong-Won Lee
发明人： Branko N. Popov , Jong-Won Lee
IPC分类号： H01M4/04 , H01B1/12
CPC分类号： H01M4/54 , H01M4/06 , H01M4/364 , H01M4/382 , H01M4/60 , H01M4/606 , H01M6/16
摘要： In one embodiment of the present disclosure, a composite electrode for a battery is provided. The composite electrode includes silver vanadium oxide present in an amount from about 75 weight percent to about 99 weight percent and polypyrrole present in an amount from about 1 weight percent to about 25 weight percent.
摘要翻译：在本公开的一个实施例中，提供了一种用于电池的复合电极。复合电极包括以约75重量％至约99重量％的量存在的银钒氧化物，并且存在量为约1重量％至约25重量％的聚吡咯。

6. 发明授权

US07629285B2 Carbon-based composite electrocatalysts for low temperature fuel cells 有权
标题翻译：用于低温燃料电池的碳基复合电催化剂
公开(公告)号：US07629285B2
公开(公告)日：2009-12-08
申请号：US11930322
申请日：2007-10-31
申请人： Branko N. Popov , Jog-Won Lee , Nalini P. Subramanian , Swaminatha P. Kumaraguru , Hector R. Colon-Mercado , Vijayadurga Nallathambi , Xuguang Li , Gang Wu
发明人： Branko N. Popov , Jog-Won Lee , Nalini P. Subramanian , Swaminatha P. Kumaraguru , Hector R. Colon-Mercado , Vijayadurga Nallathambi , Xuguang Li , Gang Wu
IPC分类号： B01J31/00 , B01J21/18 , B01J27/06 , B01J23/00 , B01J23/02 , B01J23/06 , B01J23/40 , B01J23/74
CPC分类号： H01M4/92 , B01J21/18 , B01J37/086 , B01J37/12 , H01M4/9083 , H01M4/926 , H01M2008/1095
摘要： A process for synthesis of a catalyst is provided. The process includes providing a carbon precursor material, oxidizing the carbon precursor material whereby an oxygen functional group is introduced into the carbon precursor material, and adding a nitrogen functional group into the oxidized carbon precursor material.
摘要翻译：提供合成催化剂的方法。该方法包括提供碳前体材料，氧化碳前体材料，由此将氧官能团引入到碳前体材料中，并在氧化碳前体材料中加入氮官能团。

7. 发明授权

US08398951B2 Polypyrrole and silver vanadium oxide composite 有权
标题翻译：聚吡咯和银氧化钒复合材料
公开(公告)号：US08398951B2
公开(公告)日：2013-03-19
申请号：US13411976
申请日：2012-03-05
申请人： Branko N. Popov , Jong-Won Lee
发明人： Branko N. Popov , Jong-Won Lee
IPC分类号： H01M4/02
CPC分类号： H01M4/54 , H01M4/06 , H01M4/364 , H01M4/382 , H01M4/60 , H01M4/606 , H01M6/16
摘要： In one embodiment of the present disclosure, a composite electrode for a battery is provided. The composite electrode includes silver vanadium oxide present in an amount from about 75 weight percent to about 99 weight percent and polypyrrole present in an amount from about 1 weight percent to about 25 weight percent.
摘要翻译：在本公开的一个实施例中，提供了一种用于电池的复合电极。复合电极包括以约75重量％至约99重量％的量存在的银钒氧化物，并且存在量为约1重量％至约25重量％的聚吡咯。

8. 发明申请

US20090050258A1 DEVELOPMENT OF PEM FUEL CELL ELECTRODES USING PULSE ELECTRODEPOSITION 审中-公开
标题翻译：使用脉冲电沉积的PEM燃料电池电极的开发
公开(公告)号：US20090050258A1
公开(公告)日：2009-02-26
申请号：US12196630
申请日：2008-08-22
申请人： Branko N. Popov , Yoon-Seok Choi , Subasri M Ayyadurai , Jong-Won Lee
发明人： Branko N. Popov , Yoon-Seok Choi , Subasri M Ayyadurai , Jong-Won Lee
IPC分类号： B32B38/00 , C25D5/34 , C25D5/54
CPC分类号： B32B37/24 , B32B38/0008 , B32B38/0036 , B32B2037/243 , B32B2038/0092 , B32B2309/105 , B32B2310/14 , B32B2311/06 , B32B2457/18 , C25D5/18 , C25D5/48 , H01M4/8807 , H01M4/8821 , H01M4/8853 , H01M4/8882 , H01M4/8892 , H01M4/92 , H01M4/96 , H01M2008/1095
摘要： In one embodiment of the present disclosure a method for forming a PEM fuel cell electrode is provided. The method includes applying a hydrophilic wetting agent on an electrode surface. A catalyst layer is deposited on the wetted electrode surface by pulse electrodeposition, at least a portion of the catalyst penetrating the electrode surface. The electrode surface is heat treated.
摘要翻译：在本公开的一个实施例中，提供了一种用于形成PEM燃料电池电极的方法。该方法包括在电极表面上涂布亲水润湿剂。催化剂层通过脉冲电沉积沉积在润湿的电极表面上，至少一部分催化剂穿透电极表面。电极表面进行热处理。

9. 发明申请

US20080161183A1 Carbon-Based Composite Electrocatalysts for Low Temperature Fuel Cells 有权
标题翻译：用于低温燃料电池的碳基复合电催化剂
公开(公告)号：US20080161183A1
公开(公告)日：2008-07-03
申请号：US11930322
申请日：2007-10-31
申请人： Branko N. Popov , Jong-Won Lee , Nalini P. Subramanian , Swaminatha P. Kumaraguru , Hector R. Colon-Mercado , Vijayadurga Nallathambi , Xuguang Li , Gang WU
发明人： Branko N. Popov , Jong-Won Lee , Nalini P. Subramanian , Swaminatha P. Kumaraguru , Hector R. Colon-Mercado , Vijayadurga Nallathambi , Xuguang Li , Gang WU
IPC分类号： H01M4/88
CPC分类号： H01M4/92 , B01J21/18 , B01J37/086 , B01J37/12 , H01M4/9083 , H01M4/926 , H01M2008/1095
摘要： A process for synthesis of a catalyst is provided. The process includes providing a carbon precursor material, oxidizing the carbon precursor material whereby an oxygen functional group is introduced into the carbon precursor material, and adding a nitrogen functional group into the oxidized carbon precursor material.
摘要翻译：提供合成催化剂的方法。该方法包括提供碳前体材料，氧化碳前体材料，由此将氧官能团引入到碳前体材料中，并在氧化碳前体材料中加入氮官能团。

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