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1. 发明授权

US08110073B2 Process for the preparation of aromatic amines 有权
标题翻译：芳香胺的制备方法
公开(公告)号：US08110073B2
公开(公告)日：2012-02-07
申请号：US12001829
申请日：2007-12-13
申请人： Bernd Pennemann , Bill Brady , Rainer Buse
发明人： Bernd Pennemann , Bill Brady , Rainer Buse
IPC分类号： B01D3/02 , C07C209/36 , C07C209/86
CPC分类号： C07C209/36 , Y02P20/124 , Y10S203/08 , Y10S203/11 , Y10S203/20 , C07C211/50
摘要： Aromatic amines are produced by catalytic hydrogenation of aromatic nitro compounds. The reaction mixture generated by this hydrogenation is then worked up by distillation in a manner which makes it possible to substantially free the amine of water with increased energy efficiency. Water free of amine and low boilers and the low boiling materials are also obtained.
摘要翻译：芳族胺通过芳族硝基化合物的催化氢化产生。通过该氢化产生的反应混合物然后通过蒸馏来处理，使得可以以增加的能量效率基本上释放水的胺。也可获得不含胺和低沸点的水和低沸点物质。

2. 发明授权

US07307190B2 Process for the preparation of toluenediamine 有权
标题翻译：制备甲苯二胺的方法
公开(公告)号：US07307190B2
公开(公告)日：2007-12-11
申请号：US11482404
申请日：2006-07-07
申请人： Bernd Pennemann , Bill Brady , Rainer Buse , Gerd Greger
发明人： Bernd Pennemann , Bill Brady , Rainer Buse , Gerd Greger
IPC分类号： C07C209/00 , C07C249/00
CPC分类号： C07C209/36
摘要： Toluenediamine is produced and separated from by-products of the reaction by: a) hydrogenating dinitrotoluene in the presence of a catalyst, b) separating the catalyst, water and optionally solvent from the hydrogenation reaction mixture to give crude toluenediamine, and c) separating by distillation the crude toluenediamine in a separating wall column into at least four product streams P1, P2, P3 and P4. The product stream P1 is a stream containing low boilers. The product stream P2 is a stream containing o-toluenediamine. The product stream P3 is a stream containing m-toluenediamine. The product stream P4 is a stream containing high boilers and m-toluenediamine.
摘要翻译：制备甲苯二胺并通过以下方式与反应的副产物分离：a）在催化剂存在下氢化二硝基甲苯，b）从氢化反应混合物中分离催化剂，水和任选的溶剂，得到粗甲苯二胺，和c）通过将分离壁塔中的粗甲苯二胺蒸馏成至少四种产物流P 1，P 2，P 3和P 4。产物流P 1是含有低锅炉的物流。产物流P 2是含有邻甲苯二胺的物流。产物流P 3是含有间甲苯二胺的物流。产物流P 4是含有高锅炉和间甲苯二胺的物流。

3. 发明申请

US20080179176A1 Process for the preparation of aromatic amines 有权
标题翻译：芳香胺的制备方法
公开(公告)号：US20080179176A1
公开(公告)日：2008-07-31
申请号：US12001829
申请日：2007-12-13
申请人： Bernd Pennemann , Bill Brady , Rainer Buse
发明人： Bernd Pennemann , Bill Brady , Rainer Buse
IPC分类号： C02F1/04
CPC分类号： C07C209/36 , Y02P20/124 , Y10S203/08 , Y10S203/11 , Y10S203/20 , C07C211/50
摘要： Aromatic amines are produced by catalytic hydrogenation of aromatic nitro compounds. The reaction mixture generated by this hydrogenation is then worked up by distillation in a manner which makes it possible to substantially free the amine of water with increased energy efficiency. Water free of amine and low boilers and the low boiling materials are also obtained.
摘要翻译：芳族胺通过芳族硝基化合物的催化氢化产生。通过该氢化产生的反应混合物然后通过蒸馏来处理，使得可以以增加的能量效率基本上释放水的胺。也可获得不含胺和低沸点的水和低沸点物质。

4. 发明申请

US20070015940A1 Process for the preparation of toluenediamine 有权
公开(公告)号：US20070015940A1
公开(公告)日：2007-01-18
申请号：US11482404
申请日：2006-07-07
申请人： Bernd Pennemann , Bill Brady , Rainer Buse , Gerd Greger
发明人： Bernd Pennemann , Bill Brady , Rainer Buse , Gerd Greger
IPC分类号： C07C209/36
CPC分类号： C07C209/36
摘要： Toluenediamine is produced and separated from by-products of the reaction by: a) hydrogenating dinitrotoluene in the presence of a catalyst, b) separating the catalyst, water and optionally solvent from the hydrogenation reaction mixture to give crude toluenediamine, and c) separating by distillation the crude toluenediamine in a separating wall column into at least four product streams P1, P2, P3 and P4. The product stream P1 is a stream containing low boilers. The product stream P2 is a stream containing o-toluenediamine. The product stream P3 is a stream containing m-toluenediamine. The product stream P4 is a stream containing high boilers and m-toluenediamine.

5. 发明授权

US07575660B2 Process for the distillative separation of aqueous amine solutions 有权
标题翻译：胺水溶液的蒸馏分离方法
公开(公告)号：US07575660B2
公开(公告)日：2009-08-18
申请号：US11138991
申请日：2005-05-26
申请人： Friedhelm Steffens , Rainer Buse , Bill Brady
发明人： Friedhelm Steffens , Rainer Buse , Bill Brady
IPC分类号： B01D3/00 , C07C51/44 , C07C209/84 , C07C209/86
CPC分类号： C07C209/86 , Y10S203/20 , C07C211/47
摘要： The invention relates to an energy efficient process for the distillative working-up of aqueous amine solutions that occur in the catalytic hydrogenation of nitroaromatic compounds. In this process, the amine is freed from water and also the water is obtained free from amine and low-boiling compounds and the concentrated low-boiling compounds are obtained.
摘要翻译：本发明涉及在硝基芳族化合物的催化氢化中发生的胺水溶液的蒸馏处理的能量有效的方法。在该方法中，胺不含水，而且得不含胺和低沸点化合物的水，得到浓缩的低沸点化合物。

6. 发明申请

US20050263385A1 Process for the distillative separation of aqueous amine solutions 有权
标题翻译：胺水溶液的蒸馏分离方法
公开(公告)号：US20050263385A1
公开(公告)日：2005-12-01
申请号：US11138991
申请日：2005-05-26
申请人： Friedhelm Steffens , Rainer Buse , Bill Brady
发明人： Friedhelm Steffens , Rainer Buse , Bill Brady
IPC分类号： B01D3/14 , C07B63/00 , C07C209/86 , C07C211/47 , C07C211/50 , C07C51/44 , F25J3/00
CPC分类号： C07C209/86 , Y10S203/20 , C07C211/47
摘要： The invention relates to an energy efficient process for the distillative working-up of aqueous amine solutions that occur in the catalytic hydrogenation of nitroaromatic compounds. In this process, the amine is freed from water and also the water is obtained free from amine and low-boiling compounds and the concentrated low-boiling compounds are obtained.
摘要翻译：本发明涉及在硝基芳族化合物的催化氢化中发生的胺水溶液的蒸馏处理的能量有效的方法。在该方法中，胺不含水，而且得不含胺和低沸点化合物的水，得到浓缩的低沸点化合物。

7. 发明申请

US20060038306A1 Stirring device and process for carrying out a gas-liquid reaction 有权
标题翻译：搅拌装置和进行气液反应的方法
公开(公告)号：US20060038306A1
公开(公告)日：2006-02-23
申请号：US11199697
申请日：2005-08-09
申请人： Rainer Buse , Berthold Keggenhoff , Jurgen Munnig , Friedhelm Steffens , Joachim Ritter
发明人： Rainer Buse , Berthold Keggenhoff , Jurgen Munnig , Friedhelm Steffens , Joachim Ritter
IPC分类号： B01F3/04
CPC分类号： B01F3/04539 , B01F3/2215 , B01F7/00641 , B01F2003/04546 , B01F2003/04567 , B01F2015/061 , B01F2215/0427 , B01F2215/0431 , B01F2215/0472 , B01F2215/0481 , B01J19/0066 , B01J2219/00076
摘要： The invention describes a stirring device made from a gassing stirrer and a liquid mixer or two liquid mixers, which are arranged on a shaft and each have a feed and at least one exit opening, wherein the exit openings of the gassing stirrer and of the liquid mixer or the liquid mixers are at a distance from one another, the ratio, a/d, of the distance, a, between the exit openings to the diameter, d, of the gassing stirrer or liquid mixer being 0.02 to 0.5 and the ratio, b/d, of the distance, b, between the outer edges to the diameter, d, of the gassing stirrer or liquid mixer being 0.01 to 0.4.
摘要翻译：本发明描述了一种由排气搅拌器和液体混合器或两个液体混合器制成的搅拌装置，它们设置在轴上，每个具有进料和至少一个出口，其中排气搅拌器和液体的出口混合器或液体混合器彼此间隔一定距离，排气口与吹气搅拌器或液体混合器的直径d之间的距离a的比值a / d为0.02至0.5， b / d之间的距离b，在外边缘与排气搅拌器或液体混合器的直径d之间的距离b为0.01至0.4。

8. 发明授权

US07322565B2 Stirring device and process for carrying out a gas-liquid reaction 有权
标题翻译：搅拌装置和进行气液反应的方法
公开(公告)号：US07322565B2
公开(公告)日：2008-01-29
申请号：US11199697
申请日：2005-08-09
申请人： Rainer Buse , Berthold Keggenhoff , Jürgen Münnig , Friedhelm Steffens , Joachim Ritter
发明人： Rainer Buse , Berthold Keggenhoff , Jürgen Münnig , Friedhelm Steffens , Joachim Ritter
IPC分类号： B01F3/04
CPC分类号： B01F3/04539 , B01F3/2215 , B01F7/00641 , B01F2003/04546 , B01F2003/04567 , B01F2015/061 , B01F2215/0427 , B01F2215/0431 , B01F2215/0472 , B01F2215/0481 , B01J19/0066 , B01J2219/00076
摘要： The invention describes a stirring device made from a gassing stirrer and a liquid mixer or two liquid mixers, which are arranged on a shaft and each have a feed and at least one exit opening, wherein the exit openings of the gassing stirrer and of the liquid mixer or the liquid mixers are at a distance from one another, the ratio, a/d, of the distance, a, between the exit openings to the diameter, d, of the gassing stirrer or liquid mixer being 0.02 to 0.5 and the ratio, b/d, of the distance, b, between the outer edges to the diameter, d, of the gassing stirrer or liquid mixer being 0.01 to 0.4.
摘要翻译：本发明描述了一种由排气搅拌器和液体混合器或两个液体混合器制成的搅拌装置，它们设置在轴上，每个具有进料和至少一个出口，其中排气搅拌器和液体的出口混合器或液体混合器彼此间隔一定距离，排气口与吹气搅拌器或液体混合器的直径d之间的距离a的比值a / d为0.02至0.5， b / d之间的距离b，在外边缘与排气搅拌器或液体混合器的直径d之间的距离b为0.01至0.4。

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