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1. 发明授权

US5804349A Acrylonitrile-modified toner compositions and processes 失效
标题翻译：丙烯腈改性调色剂组合物和方法
公开(公告)号：US5804349A
公开(公告)日：1998-09-08
申请号：US907368
申请日：1997-08-07
申请人： Beng S. Ong , Grazyna E. Kmiecik-Lawrynowicz , Raj D. Patel , Walter Mychajlowskij , David J. Sanders , T. Hwee Ng
发明人： Beng S. Ong , Grazyna E. Kmiecik-Lawrynowicz , Raj D. Patel , Walter Mychajlowskij , David J. Sanders , T. Hwee Ng
IPC分类号： G03G9/08 , G03G9/087 , G03G9/097
CPC分类号： G03G9/08795 , G03G9/0806 , G03G9/08711 , G03G9/08731 , G03G9/09725
摘要： A toner comprised of pigment, and an addition polymer resin generated from about 55 to about 80 weight percent of styrene, from about 1 to about 25 weight percent of acrylate, from about 1 to about 20 weight percent of acrylonitrile, and from about 0.5 to about 5 weight percent of acrylic acid.
摘要翻译：由颜料组成的调色剂和由约55至约80重量％的苯乙烯，约1至约25重量％的丙烯酸酯，约1至约20重量％的丙烯腈和约0.5至约20重量％的丙烯腈产生的加成聚合物树脂约5重量％的丙烯酸。

2. 发明授权

US5683848A Acrylonitrile-modified toner composition and processes 失效
标题翻译：丙烯腈改性调色剂组合物和方法
公开(公告)号：US5683848A
公开(公告)日：1997-11-04
申请号：US720736
申请日：1996-10-02
申请人： Beng S. Ong , Grazyna E. Kmiecik-Lawrynowicz , Raj D. Patel , Walter Mychajlowskij , David J. Sanders , T. Hwee Ng
发明人： Beng S. Ong , Grazyna E. Kmiecik-Lawrynowicz , Raj D. Patel , Walter Mychajlowskij , David J. Sanders , T. Hwee Ng
IPC分类号： G03G9/08 , G03G9/087 , G03G9/097
CPC分类号： G03G9/08795 , G03G9/0806 , G03G9/08711 , G03G9/08731 , G03G9/09725
摘要： A toner comprised of pigment, and an addition polymer resin generated from about 55 to about 80 weight percent of styrene, from about 1 to about 25 weight percent of acrylate, from about 1 to about 20 weight percent of acrylonitrile, and from about 0.5 to about 5 weight percent of acrylic acid.
摘要翻译：由颜料组成的调色剂和由约55至约80重量％的苯乙烯，约1至约25重量％的丙烯酸酯，约1至约20重量％的丙烯腈和约0.5至约20重量％的丙烯腈产生的加成聚合物树脂约5重量％的丙烯酸。

3. 发明授权

US5763133A Toner compositions and processes 失效
标题翻译：调色剂组成和工艺
公开(公告)号：US5763133A
公开(公告)日：1998-06-09
申请号：US825451
申请日：1997-03-28
申请人： Beng S. Ong , Walter Mychajlowskij , Grazyna E. Kmiecik-Lawrynowicz , Raj D. Patel , David J. Sanders , Stephan V. Drappel
发明人： Beng S. Ong , Walter Mychajlowskij , Grazyna E. Kmiecik-Lawrynowicz , Raj D. Patel , David J. Sanders , Stephan V. Drappel
IPC分类号： G03G9/08 , G03G9/087 , G03G9/09 , G03G9/097
CPC分类号： G03G9/08793 , G03G9/0804 , G03G9/08708 , G03G9/08711 , G03G9/08728 , G03G9/08731 , G03G9/08733
摘要： A process for the preparation of toner comprising (i) blending (a) an aqueous pigment dispersion containing a first ionic surfactant and an optional charge control agent with (b) a latex blend comprised of linear polymer and crosslinked polymer particles, optional nonionic surfactant and a second ionic surfactant with a charge polarity opposite to that of said first ionic surfactant in said pigment dispersion; (ii) heating the resulting mixture at about below the glass transition temperature (Tg) of the linear latex polymer to form toner sized aggregates; and (iii) subsequently heating said aggregate suspension about above the Tg of the linear latex polymer to effect fusion or coalescence of said aggregates.
摘要翻译：一种制备调色剂的方法，包括（i）将（a）含有第一离子型表面活性剂和任选的电荷控制剂的水性颜料分散体与（b）由线性聚合物和交联聚合物颗粒组成的胶乳共混物，任选的非离子表面活性剂和在所述颜料分散体中具有与所述第一离子型表面活性剂相反的电荷极性的第二离子表面活性剂; （ii）将所得混合物加热至低于线性胶乳聚合物的玻璃化转变温度（Tg），以形成调色剂尺寸的聚集体; 和（iii）随后将所述聚集体悬浮液加热至高于线性胶乳聚合物的Tg，以实现所述聚集体的熔融或聚结。

4. 发明授权

US5582951A Carrier processes 失效
标题翻译：运营商流程
公开(公告)号：US5582951A
公开(公告)日：1996-12-10
申请号：US498284
申请日：1995-07-03
申请人： Raj D. Patel , Grazyna E. Kmiecik-Lawrynowicz , Michael A. Hopper , Walter Mychajlowskij , Beng S. Ong
发明人： Raj D. Patel , Grazyna E. Kmiecik-Lawrynowicz , Michael A. Hopper , Walter Mychajlowskij , Beng S. Ong
IPC分类号： G03G9/107 , G03G9/113
CPC分类号： G03G9/1133 , G03G9/107 , G03G9/1132
摘要： A process for the preparation of carrier particles which comprises mixing a dispersion of water, submicron magnetic particles, and ionic surfactant with a latex comprised of resin particles suspended in an aqueous solution containing a surfactant that is counterionic in charge to said ionic surfactant, and a nonionic surfactant; thereafter heating the resulting mixture below about the latex resin glass transition temperature (Tg) while stirring to form aggregates, followed by increasing the temperature of said mixture to about above the latex resin Tg, and subsequently adding additional counterionic or nonionic surfactant solution to minimize, or avoid any further growth in particle size during heating of the mixture about above the latex resin Tg, and wherein said resin Tg is in the range of from between about 45.degree. C. to about 100.degree. C.
摘要翻译：一种制备载体颗粒的方法，其包括将水，亚微米磁性颗粒和离子表面活性剂的分散体与悬浮在含有负离子表面活性剂的水溶液中的树脂颗粒混合到所述离子表面活性剂上的胶乳混合，以及非离子表面活性剂然后在搅拌下将所得混合物在胶乳树脂玻璃化转变温度（Tg）以下加热以形成聚集体，随后将所述混合物的温度升高至胶乳树脂Tg的大约，然后加入另外的抗衡离子或非离子表面活性剂溶液，或者避免混合物加热到胶乳树脂Tg以上时粒径的任何进一步增长，并且其中所述树脂Tg在约45℃至约100℃的范围内。

5. 发明授权

US5858601A Toner processes 有权
标题翻译：墨粉处理
公开(公告)号：US5858601A
公开(公告)日：1999-01-12
申请号：US127851
申请日：1998-08-03
申请人： Beng S. Ong , T. Hwee Ng , Walter Mychajlowskij , Raj D. Patel , Patricia A. Burns
发明人： Beng S. Ong , T. Hwee Ng , Walter Mychajlowskij , Raj D. Patel , Patricia A. Burns
IPC分类号： G03G9/08 , G03G9/093
CPC分类号： G03G9/093 , G03G9/0804
摘要： A process for the preparation of toner comprising(i) blending (a) a colorant dispersion containing a first ionic surfactant with (b) a latex emulsion comprised of an aqueous dispersion of core-shell polymer particles with a crosslinked polymer core and a linear polymer shell, and optional nonionic surfactant and a second ionic surfactant with a charge polarity opposite to that of said first ionic surfactant in said colorant dispersion;(ii) heating the resulting mixture at about below the glass transition temperature (Tg) of the linear latex shell polymer to form aggregates; and(iii) subsequently heating said aggregates about above the Tg of the linear latex shell polymer to effect coalescence and fusion of said aggregates.
摘要翻译：一种制备调色剂的方法，包括（i）将（a）含有第一离子表面活性剂的着色剂分散体与（b）由核 - 壳聚合物颗粒的水性分散体与交联的聚合物核心和线性聚合物组成的胶乳乳液壳和任选的非离子表面活性剂和在所述着色剂分散体中具有与所述第一离子表面活性剂的电荷极性相反的电荷的第二离子表面活性剂; （ii）将所得混合物加热至低于线性胶乳壳聚合物的玻璃化转变温度（Tg）以形成聚集体; 和（iii）随后将所述聚集体加热至高于线性胶乳壳聚合物的Tg，以实现所述聚集体的聚结和熔融。

6. 发明授权

US5981651A Ink processes 失效
标题翻译：墨水处理
公开(公告)号：US5981651A
公开(公告)日：1999-11-09
申请号：US922078
申请日：1997-09-02
申请人： Raj D. Patel , Grazyna E. Kmiecik-Lawrynowicz , Michael A. Hopper , Walter Mychajlowskij
发明人： Raj D. Patel , Grazyna E. Kmiecik-Lawrynowicz , Michael A. Hopper , Walter Mychajlowskij
IPC分类号： C09D11/02 , C08F2/00 , C08F12/08 , C09D11/00
CPC分类号： C08F12/08 , C09D11/30 , Y10S977/788
摘要： A process comprising (1) polymerizing an organic phase of monomer in the presence of a carboxylic acid, an oil soluble chain transfer agent, and a partially water soluble chain transfer agent; and which polymerizing is accomplished in the presence of (2) an aqueous phase containing a nonionic surfactant, and an anionic surfactant, and wherein there is added to the aqueous phase an aqueous initiator solution of an inorganic persulfate, and wherein the resulting latex contains particles of polymer with carboxylic acid; aggregating said latex particles with colorant; thereafter adding an effective amount of anionic surfactant and heating the mixture resulting about equal to, or about above the polymer Tg resulting from said monomer, or said monomers.
摘要翻译：一种方法，其包括（1）在羧酸，油溶性链转移剂和部分水溶性链转移剂的存在下聚合单体的有机相; 并且在（2）含有非离子表面活性剂的水相和阴离子表面活性剂的存在下进行聚合，并且其中在水相中加入无机过硫酸盐的引发剂水溶液，并且其中所得的胶乳含有颗粒的聚合物与羧酸; 用着色剂聚集所述胶乳颗粒; 然后加入有效量的阴离子表面活性剂并加热产生的约等于或约高于由所述单体或所述单体产生的聚合物Tg的混合物。

7. 发明授权

US5869215A Toner compositions and processes thereof 失效
标题翻译：调色剂组合物及其工艺
公开(公告)号：US5869215A
公开(公告)日：1999-02-09
申请号：US6508
申请日：1998-01-13
申请人： Beng S. Ong , Walter Mychajlowskij , Patricia A. Burns , Raj D. Patel , David J. Sanders
发明人： Beng S. Ong , Walter Mychajlowskij , Patricia A. Burns , Raj D. Patel , David J. Sanders
IPC分类号： G03G9/08 , G03G9/087
CPC分类号： G03G9/08793 , G03G9/0804 , G03G9/08795 , G03G9/08797
摘要： A process for the preparation of toner including(i) blending an aqueous colorant dispersion with a latex blend comprised of a linear polymer and a soft crosslinked polymer;(ii) heating the resulting mixture at about below, or about equal to the glass transition temperature (Tg) of the linear latex polymer to form aggregates; and(iii) subsequently heating said aggregate suspension about above, or about equal to the Tg of the linear latex polymer to effect fusion or coalescence of said aggregates.
摘要翻译：一种制备调色剂的方法，包括（i）将水性着色剂分散体与由线性聚合物和软交联聚合物组成的胶乳共混物共混; （ii）将所得混合物加热至约低于或等于线性胶乳聚合物的玻璃化转变温度（Tg），以形成聚集体; 和（iii）随后将所述聚集体悬浮液加热至约上述或约等于线性胶乳聚合物的Tg，以实现所述聚集体的熔融或聚结。

8. 发明授权

US5683847A Toner aggregation latex processes 失效
标题翻译：调色剂聚集胶乳工艺
公开(公告)号：US5683847A
公开(公告)日：1997-11-04
申请号：US619055
申请日：1996-03-20
申请人： Raj D. Patel , Grazyna E. Kmiecik-Lawrynowicz , Walter Mychajlowskij , Michael A. Hopper
发明人： Raj D. Patel , Grazyna E. Kmiecik-Lawrynowicz , Walter Mychajlowskij , Michael A. Hopper
IPC分类号： G03G9/08 , G03G9/087
CPC分类号： G03G9/08711 , G03G9/0804
摘要： A process comprising: (i) preparing a pigment dispersion, which dispersion is comprised of a pigment, a cationic surfactant, and optionally a charge control agent; (ii) shearing said pigment dispersion with a latex comprised of water, resin, a counterionic or anionic surfactant with a charge polarity of opposite sign to that of said cationic surfactant, and a nonionic surfactant, and wherein said latex is prepared by the addition of monomers containing a chain transfer agent and a organic soluble initiator to a water phase containing a anionic surfactant, and said nonionic surfactant, followed by the addition of a water soluble initiator, and subsequently heating; (iii) heating the above sheared blend below about the glass transition temperature (Tg) of the resin to form electrostatically bound toner size aggregates; and (iv) heating said bound aggregates above about the Tg of the resin.
摘要翻译：一种方法，包括：（i）制备颜料分散体，该分散体由颜料，阳离子表面活性剂和任选的电荷控制剂组成; （ii）用包含水，树脂，具有与所述阳离子表面活性剂相反的电荷极性的反离子或阴离子表面活性剂的胶乳和非离子表面活性剂剪切所述颜料分散体，并且其中所述胶乳通过加入含有链转移剂和有机可溶性引发剂的单体与含有阴离子表面活性剂的水相和所述非离子表面活性剂，然后加入水溶性引发剂，随后加热; （iii）将上述剪切混合物加热至低于树脂的玻璃化转变温度（Tg）以形成静电结合的调色剂尺寸聚集体; 和（iv）在树脂的Tg附近加热所述结合的聚集体。

9. 发明授权

US5698223A Toner process 失效
标题翻译：调色剂过程
公开(公告)号：US5698223A
公开(公告)日：1997-12-16
申请号：US829551
申请日：1997-03-28
申请人： Walter Mychajlowskij , Guerino G. Sacripante , Raj D. Patel , Grazyna E. Kmiecik-Lawrynowicz
发明人： Walter Mychajlowskij , Guerino G. Sacripante , Raj D. Patel , Grazyna E. Kmiecik-Lawrynowicz
IPC分类号： G03G9/08 , G03G9/087
CPC分类号： G03G9/0804 , G03G9/08768
摘要： A process for the preparation of toner comprising (i) solubilizing an imide based resin in water at pH of from about 10 to about 13 and which solubilizing is accomplished in the presence of nonionic surfactants and anionic surfactants; followed by precipitating the resulting dissolved imide resin into colloidal particles with a size diameter of from about 20 nanometers to about 500 nanometers, and which precipitating is accomplished with a high shearing device operating at a speed of from about 500 to about 2,000 revolutions per minute; acidifying the resulting mixture to a pH of from about 2 to about 4; (ii) preparing a pigment dispersion in water, which dispersion is comprised of a pigment, an oppositely charged ionic surfactant and optionally charge control agent; (iii) shearing (i) and (ii), thereby causing a flocculation of the resin, pigment, surfactants, and optional charge control agent; (iv) heating the resulting flocculent mixture of (iii) with stirring at a temperature of from about 25.degree. C. to about 1.degree. C. below the glass transition temperature (Tg) of the imide resin to effect formation of electrostatically bounded toner sized aggregates, and wherein the imide resin has a Tg of from about 45.degree. C. to about 65.degree. C.; (v) heating the resulting aggregate suspension of (iv) in the presence of additional anionic surfactant selected in an amount of from about 0.01 to about 5 weight percent based on the weight percent of the total reaction mixture solids, and which heating is at a temperature of from about 10.degree. C. to about 55.degree. C. above the Tg of the imide resin; and optionally cooling, and optionally (vi) separating said toner by washing, and thereafter drying said toner.
摘要翻译：一种制备调色剂的方法，包括（i）将酰亚胺基树脂溶解在约10至约13的pH下，并且在非离子表面活性剂和阴离子表面活性剂存在下进行增溶; 然后将所得溶解的酰亚胺树脂沉淀成尺寸直径为约20纳米至约500纳米的胶体颗粒，并且以约500至约2000转/分钟的速度运行的高剪切装置完成沉淀; 将所得混合物酸化至约2至约4的pH; （ii）在水中制备颜料分散体，该分散体由颜料，相反电荷的离子表面活性剂和任选的电荷控制剂组成; （iii）剪切（i）和（ii），从而引起树脂，颜料，表面活性剂和任选的电荷控制剂的絮凝; （iv）在低于酰亚胺树脂的玻璃化转变温度（Tg）的约25℃至约1℃的温度下搅拌加热得到的（ⅲ）絮状混合物，以形成静电有界调色剂尺寸聚集体，并且其中所述酰亚胺树脂的Tg为约45℃至约65℃。（v）在所选择的另外的阴离子表面活性剂存在下加热得到的（iv）聚集体悬浮液，其量为总反应混合物固体的重量百分比为约0.01至约5重量％，加热为温度高于酰亚胺树脂的Tg约10℃至约55℃; 并任选地冷却，并且任选地（vi）通过洗涤分离所述调色剂，然后干燥所述调色剂。

10. 发明授权

US5919595A Toner process with cationic salts 失效
标题翻译：具有阳离子盐的调色剂
公开(公告)号：US5919595A
公开(公告)日：1999-07-06
申请号：US6553
申请日：1998-01-13
申请人： Walter Mychajlowskij , Daniel A. Foucher , Guerino G. Sacripante , Raj D. Patel , Beng S. Ong
发明人： Walter Mychajlowskij , Daniel A. Foucher , Guerino G. Sacripante , Raj D. Patel , Beng S. Ong
IPC分类号： C09D167/02 , G03G9/08 , G03G9/087
CPC分类号： G03G9/08755 , G03G9/0804
摘要： A process for the preparation of toner comprising mixing an emulsion latex, a colorant dispersion, and monocationic salt, and which mixture possesses an ionic strength of from about 0.001 molar (M) to about 5 molar, and optionally cooling.
摘要翻译：一种制备调色剂的方法，包括混合乳液胶乳，着色剂分散体和单体盐，并且该混合物具有约0.001摩尔（M）至约5摩尔的离子强度，并任选地冷却。

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