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1. 发明申请

US20080161511A1 PROCESS FOR PRODUCING FLUOROPOLYMER 失效
标题翻译：生产氟聚合物的方法
公开(公告)号：US20080161511A1
公开(公告)日：2008-07-03
申请号：US11618088
申请日：2006-12-29
申请人： Atsushi WATAKABE , Susumu Saito , Adam Luke Safir
发明人： Atsushi WATAKABE , Susumu Saito , Adam Luke Safir
IPC分类号： C08F2/00 , C08F16/24
CPC分类号： C08F214/182 , C08F214/26 , C08F214/262
摘要： It is to provide a process for producing a polymer for an electrolyte material to prepare polymer electrolyte fuel cells which can be operated at a high temperature and with which high output can be obtained, with a stable composition.A process for producing a fluoropolymer by polymerization reaction of tetrafluoroethylene and a fluoromonomer represented by the following formula (m), wherein the polymerization reaction is carried out by continuously charging the reactor with tetrafluoroethylene and the fluoromonomer: wherein m1 is an integer of from 1 to 6.
摘要翻译：本发明提供一种电解质材料用聚合物的制造方法，其特征在于，以稳定的组成制备可在高温下进行操作且能够获得高产出的聚合物电解质型燃料电池。一种通过四氟乙烯和由下式（m）表示的含氟单体的聚合反应制备含氟聚合物的方法，其中聚合反应是通过用四氟乙烯和含氟单体连续地加入反应器进行的：其中m1为1〜 6。

2. 发明申请

US20110071272A1 FLUOROSULFONYL GROUP-CONTAINING MONOMER AND ITS POLYMER, AND SULFONIC ACID GROUP-CONTAINING POLYMER 有权
标题翻译：含氟基团的单体及其聚合物和含有磺酸基团的聚合物
公开(公告)号：US20110071272A1
公开(公告)日：2011-03-24
申请号：US12955443
申请日：2010-11-29
申请人： Atsushi WATAKABE , Hiromasa Yamamoto , Masao Iwaya , Susumu Saito
发明人： Atsushi WATAKABE , Hiromasa Yamamoto , Masao Iwaya , Susumu Saito
IPC分类号： C08G75/14
CPC分类号： C07D317/42 , C08G75/23
摘要： A fluorosulfonyl group-containing monomer having a high polymerization reactivity and plural fluorosulfonyl groups, a fluorosulfonyl group-containing polymer and a sulfonic acid group-containing polymer, obtained by using the monomer.
摘要翻译：具有高聚合反应性的氟磺酰基的单体和多个氟磺酰基，含氟磺酰基的聚合物和含磺酸基的聚合物通过使用该单体获得。

3. 发明申请

US20110027677A1 FUEL CELL SYSTEM 有权
标题翻译：燃油电池系统
公开(公告)号：US20110027677A1
公开(公告)日：2011-02-03
申请号：US12828710
申请日：2010-07-01
申请人： Satoru HOMMURA , Susumu SAITO , Tetsuji SHIMOHIRA , Atsushi WATAKABE , Junichi TAYANAGI
发明人： Satoru HOMMURA , Susumu SAITO , Tetsuji SHIMOHIRA , Atsushi WATAKABE , Junichi TAYANAGI
IPC分类号： H01M8/04 , H01M8/10
CPC分类号： H01M8/1067 , C08J5/2237 , C08J2327/12 , H01M8/04358 , H01M8/04768 , H01M8/04835 , H01M8/1025 , H01M8/1039
摘要： To provide a fuel cell system provided with a polymer electrolyte fuel cell which is excellent in the power generation characteristics under high temperature and low or no humidity conditions.A fuel cell system 20 comprising a polymer electrolyte fuel cell 22 having a membrane/electrode assembly 10 having a catalyst layer containing a polymer (H) which has repeating units based on a perfluoromonomer having an alicyclic structure and has ion exchange groups, a temperature controlling means for controlling temperature of the polymer electrolyte fuel cell 22, a temperature sensor 38 for detecting temperature of the polymer electrolyte fuel cell 22, and a controlling device 40 for controlling the temperature controlling means based on temperature information from the temperature sensor 38 so that the maximum temperature of the polymer electrolyte fuel cell 22 becomes within the range of from 90 to 140° C.
摘要翻译：提供一种设置有在高温低湿条件下发电特性优异的聚合物电解质型燃料电池的燃料电池系统。一种燃料电池系统20，包括具有膜/电极组件10的聚合物电解质燃料电池22，所述膜/电极组件10具有含有聚合物（H）的催化剂层，所述聚合物（H）具有基于具有脂环结构的全氟单体的重复单元并具有离子交换基团，温度控制用于控制聚合物电解质燃料电池22的温度的装置，用于检测聚合物电解质燃料电池22的温度的温度传感器38，以及用于基于来自温度传感器38的温度信息来控制温度控制装置的控制装置40，聚合物电解质燃料电池22的最高温度在90〜140℃的范围内。

4. 发明申请

US20090048424A1 FLUOROSULFONYL GROUP-CONTAINING MONOMER AND ITS POLYMER, AND SULFONIC ACID GROUP-CONTAINING POLYMER 审中-公开
标题翻译：含氟基团的单体及其聚合物和含有磺酸基团的聚合物
公开(公告)号：US20090048424A1
公开(公告)日：2009-02-19
申请号：US12186947
申请日：2008-08-06
申请人： Atsushi WATAKABE , Hiromasa YAMAMOTO , Masao IWAYA , Susumu SAITO
发明人： Atsushi WATAKABE , Hiromasa YAMAMOTO , Masao IWAYA , Susumu SAITO
IPC分类号： C08G75/20 , C07D317/10
CPC分类号： C07D317/42 , C08G75/23
摘要： To provide a fluorosulfonyl group-containing monomer having a high polymerization reactivity and plural fluorosulfonyl groups. Further, to provide a fluorosulfonyl group-containing polymer and a sulfonic acid group-containing polymer, obtained by using the monomer.A perfluoro(2-methylene-1,3-dioxolane) derivative which is represented by the following formula (3) and which has two fluorosulfonyl groups, and its production process and its synthetic intermediate. A fluorosulfonyl group-containing polymer having monomer units represented by the following formula (3U) obtained by polymerizing the compound (3) by itself or with a comonomer, and a sulfonic acid group-containing polymer having the following units (5U) obtained by hydrolyzing a fluorosulfonyl group of the polymer. In the following formulae, each of Rf1 and Rf2 which are independent of each other, is a C1-8 perfluoroalkylene group which may have an etheric oxygen atom between carbon atoms.
摘要翻译：提供具有高聚合反应性的氟代磺酰基单体和多个氟磺酰基。此外，提供通过使用该单体获得的含氟磺酰基的聚合物和含磺酸基的聚合物。由下式（3）表示并具有两个氟磺酰基的全氟（2-亚甲基-1,3-二氧戊环）衍生物及其制备方法及其合成中间体。具有由下述通式（3U）表示的具有单体单元的含氟磺酰基的聚合物，其单独或共聚单体与共聚单体聚合得到的含有磺酸基的聚合物和通过水解聚合物的氟磺酰基。在下式中，R 1和R f 2彼此独立的是碳原子之间可以具有醚性氧原子的C1-8全氟亚烷基。

5. 发明申请

US20110305971A1 SOLID POLYMER ELECTROLYTE MATERIAL, LIQUID COMPOSITION, SOLID POLYMER FUEL CELL AND FLUOROPOLYMER 有权
标题翻译：固体聚合物电解质材料，液体组合物，固体聚合物燃料电池和氟聚合物
公开(公告)号：US20110305971A1
公开(公告)日：2011-12-15
申请号：US13214273
申请日：2011-08-22
申请人： Atsushi WATAKABE , Takeshi Eriguchi , Toshihiro Tanuma , Yasuhiro Kunisa
发明人： Atsushi WATAKABE , Takeshi Eriguchi , Toshihiro Tanuma , Yasuhiro Kunisa
IPC分类号： H01M8/10
CPC分类号： H01M8/1067 , B01D71/32 , B01D71/44 , B01D71/72 , B01D71/76 , C08F216/1466 , C08F228/02 , C08J5/2268 , C08J2327/18 , C08J2365/00 , C08J2387/00 , C08L65/00 , H01B1/122 , H01M6/181 , H01M8/1004 , H01M8/1023 , H01M8/1039 , H01M10/0525 , H01M10/0565
摘要： A solid polymer electrolyte material made of a copolymer comprising a repeating unit based on a fluoromonomer A which gives a polymer having an alicyclic structure in its main chain by radical polymerization, and a repeating unit based on a fluoromonomer B of the following formula (1): CF2═CF(Rf)jSO2X (1) wherein j is 0 or 1, X is a fluorine atom, a chlorine atom or OM {wherein M is a hydrogen atom, an alkali metal atom or a group of NR1R2R3R4 (wherein each of R1, R2, R3 and R4 which may be the same or different, is a hydrogen atom or a monovalent organic group)}, and Rf is a C1-20 polyfluoroalkylene group having a straight chain or branched structure which may contain ether oxygen atoms.
摘要翻译：一种由共聚物制成的固体聚合物电解质材料，该共聚物包含基于通过自由基聚合在主链中具有脂环结构的聚合物的基于含氟单体A的重复单元和基于下式（1）的含氟单体B的重复单元，：CF2 = CF（Rf）jSO2X（1）其中j为0或1，X为氟原子，氯原子或OM（其中M为氢原子，碱金属原子或NR1R2R3R4基团 R 1，R 2，R 3和R 4可以相同或不同，为氢原子或一价有机基团}}，R f为可含有醚氧原子的具有直链或支链结构的C1-20多氟亚烷基。

6. 发明申请

US20110008710A1 MATERIAL FOR CATALYST LAYER FOR POLYMER ELECTROLYTE FUEL CELL 审中-公开
标题翻译：用于聚合物电解质燃料电池的催化剂层材料
公开(公告)号：US20110008710A1
公开(公告)日：2011-01-13
申请号：US12884675
申请日：2010-09-17
申请人： Atsushi WATAKABE , Satoru Hommura
发明人： Atsushi WATAKABE , Satoru Hommura
IPC分类号： H01M8/10 , H01M4/88 , B01J31/06
CPC分类号： H01M4/8668 , H01M4/9083 , H01M8/1004 , H01M2008/1095
摘要： To improve the utilization efficiency of a noble metal catalyst in a catalyst layer of an electrode for a polymer electrolyte fuel cell.A precursor material obtained by polymerizing a perfluoromonomer having a fluorosulfonyl group in the presence of noble metal catalyst fine particles supported carbon particles, a material for a catalyst layer obtained by converting the fluorosulfonyl groups of the precursor material to sulfonic acid groups, and a membrane/electrode assembly for a polymer electrolyte fuel cell having a catalyst layer using the material for a catalyst layer.
摘要翻译：为了提高聚合物电解质型燃料电池用电极的催化剂层中的贵金属催化剂的利用效率。在贵金属催化剂微粒担载碳颗粒存在下聚合具有氟磺酰基的全氟单体获得的前体材料，通过将前体材料的氟磺酰基转化为磺酸基得到的催化剂层的材料，以及膜/ 用于具有使用该催化剂层的材料的催化剂层的聚合物电解质燃料电池的电极组件。

7. 发明申请

US20080014490A1 SOLID POLYMER ELECTROLYTE MATERIAL LIQUID COMPOSITION, SOLID POLYMER FUEL CELL AND FLUOROPOLYMER 有权
标题翻译：固体聚合物电解质材料液体组合物，固体聚合物燃料电池和氟聚合物
公开(公告)号：US20080014490A1
公开(公告)日：2008-01-17
申请号：US11671665
申请日：2007-02-06
申请人： Atsushi WATAKABE , Takeshi Eriguchi , Toshihiro Tanuma , Yasuhiro Kunisa
发明人： Atsushi WATAKABE , Takeshi Eriguchi , Toshihiro Tanuma , Yasuhiro Kunisa
IPC分类号： H01M8/10
CPC分类号： H01M8/1067 , B01D71/32 , B01D71/44 , B01D71/72 , B01D71/76 , C08F216/1466 , C08F228/02 , C08J5/2268 , C08J2327/18 , C08J2365/00 , C08J2387/00 , C08L65/00 , H01B1/122 , H01M6/181 , H01M8/1004 , H01M8/1023 , H01M8/1039 , H01M10/0525 , H01M10/0565
摘要： A solid polymer electrolyte material made of a copolymer comprising a repeating unit based on a fluoromonomer A which gives a polymer having an alicyclic structure in its main chain by radical polymerization, and a repeating unit based on a fluoromonomer B of the following formula (1): CF2═CF(Rf)jSO2X (1) wherein j is 0 or 1, X is a fluorine atom, a chlorine atom or OM {wherein M is a hydrogen atom, an alkali metal atom or a group of NR1R2R3R4 (wherein each of R1, R2, R3 and R4 which may be the same or different, is a hydrogen atom or a monovalent organic group)}, and Rf is a C1-20 polyfluoroalkylene group having a straight chain or branched structure which may contain ether oxygen atoms.
摘要翻译：一种由共聚物制成的固体聚合物电解质材料，该共聚物包含基于通过自由基聚合在主链中具有脂环结构的聚合物的基于含氟单体A的重复单元和基于下式（1）的含氟单体B的重复单元，：<？in-line-formula description =“In-line Formulas”end =“lead”？> CF -CF（R）其中j为0或1，X为氟原子，X为1或2，，氯原子或OM（其中M为氢原子，碱金属原子或NR 1 R 2 O 3 R 3的基团） 4（其中R 1，R 2，R 3和R 4中的每一个）其可以相同或不同，是氢原子或一价有机基团）}，并且R f是具有直链的C 1〜20个多氟亚烷基或可以含有醚氧原子的支链结构。

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