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1. 发明授权

US06214469B1 Films comprising metallocene catalyzed polyethylene 失效
标题翻译：包含茂金属催化聚乙烯的薄膜
公开(公告)号：US06214469B1
公开(公告)日：2001-04-10
申请号：US09000173
申请日：1998-01-15
申请人： Ashish M. Sukhadia , David C. Rohlfing , Jay Janzen , Paul J. DesLauriers , Jim D. Byers , Louis Moore, Jr. , M. Bruce Welch , Syriac J. Palackal , William M. Whitte , William R. Coutant , Kiplin D. Cowan
发明人： Ashish M. Sukhadia , David C. Rohlfing , Jay Janzen , Paul J. DesLauriers , Jim D. Byers , Louis Moore, Jr. , M. Bruce Welch , Syriac J. Palackal , William M. Whitte , William R. Coutant , Kiplin D. Cowan
IPC分类号： B32B2732
CPC分类号： B32B27/32 , B32B7/02 , B32B27/08 , B32B2323/04 , C08F10/02 , C08F110/02 , C08F210/16 , C08J5/18 , C08J2323/04 , C08L15/02 , C08L23/0815 , C08L27/12 , C08L2314/04 , C08L2314/06 , Y10T428/3154 , Y10T428/31544 , Y10T428/31913 , Y10T428/31938 , C08L2666/04 , C08L2666/08 , C08F2500/12 , C08F2500/03 , C08F2500/14 , C08F2500/10 , C08F210/08 , C08F210/14
摘要： A high clarity film containing three layers wherein the polymer of each outer layer is the same or different polyethylene selected from polyethylenes having a density of at least 0.925 g/cc, and a molecular weight distribution of less than 4, and being further characterized by being substantially free of branches having 6 or more carbon atoms, polyethylenes of the outer layers optionally containing a fluoroelastomer.
摘要翻译：包含三层的高透明度膜，其中每个外层的聚合物是相同或不同的聚乙烯，其选自密度为至少0.925g / cc，分子量分布小于4的聚乙烯，其进一步的特征在于：基本上不含具有6个或更多个碳原子的分支，外层的聚乙烯任选地含有含氟弹性体。

2. 发明授权

US06355359B1 Polyethylene film 有权
标题翻译：聚乙烯薄膜
公开(公告)号：US06355359B1
公开(公告)日：2002-03-12
申请号：US09702908
申请日：2000-10-31
申请人： Ashish M. Sukhadia , William R. Coutant , Jim D. Byers , Louis Moore, Jr. , M. Bruce Welch , Syriac J. Palackal , Kiplin D. Cowan , David C. Rohlfing , Jay Janzen , Paul J. DesLauriers , William M. Whitte
发明人： Ashish M. Sukhadia , William R. Coutant , Jim D. Byers , Louis Moore, Jr. , M. Bruce Welch , Syriac J. Palackal , Kiplin D. Cowan , David C. Rohlfing , Jay Janzen , Paul J. DesLauriers , William M. Whitte
IPC分类号： C08F11002
CPC分类号： B32B27/32 , B32B7/02 , B32B27/08 , B32B2323/04 , C08F10/02 , C08F110/02 , C08F210/16 , C08J5/18 , C08J2323/04 , C08L15/02 , C08L23/0815 , C08L27/12 , C08L2314/04 , C08L2314/06 , Y10T428/3154 , Y10T428/31544 , Y10T428/31913 , Y10T428/31938 , C08L2666/04 , C08L2666/08 , C08F2500/12 , C08F2500/03 , C08F2500/14 , C08F2500/10 , C08F210/08 , C08F210/14
摘要： A self supporting film having one or more layers wherein at least one layer has a percent haze of less than 17.8 and the polymer of that layer consists essentially of a polyethylene having a density of at least 0.925 grams per cc, a molecular weight distribution of no more than 4, optionally containing a fluoroelastomer, and methods for making such film are disclosed.
摘要翻译：具有一层或多层的自支撑膜，其中至少一层具有小于17.8的雾度百分比，并且该层的聚合物基本上由密度为至少0.925克/厘米3的聚乙烯组成，分子量分布为无大于4，任选地含有含氟弹性体，并且公开了制备这种膜的方法。

3. 发明授权

US5710224A Method for producing polymer of ethylene 失效
标题翻译：乙烯聚合物的制备方法
公开(公告)号：US5710224A
公开(公告)日：1998-01-20
申请号：US399119
申请日：1995-03-03
申请人： Helmut G. Alt , Syriac J. Palackal , M. Bruce Welch , David C. Rohlfing , Jay Janzen
发明人： Helmut G. Alt , Syriac J. Palackal , M. Bruce Welch , David C. Rohlfing , Jay Janzen
IPC分类号： B01J31/14 , B01J31/16 , B01J31/22 , C07C13/567 , C07C51/31 , C07C51/373 , C07C51/377 , C07F5/06 , C07F17/00 , C08F4/619 , C08F4/6192 , C08F4/639 , C08F4/6392 , C08F4/64 , C08F4/659 , C08F4/6592 , C08F10/00 , C08F10/02 , C08F110/02 , C08F110/06 , C08F210/16 , G08F4/64 , G08F10/02
CPC分类号： C08F10/02 , B01J31/143 , B01J31/2295 , C07C13/567 , C07C51/31 , C07C51/373 , C07C51/377 , C07F17/00 , C07F5/068 , C08F10/00 , B01J2531/48 , B01J31/1608 , C07B2200/11 , C07C2101/10 , C07C2103/18 , C08F110/02 , C08F110/06 , C08F210/16 , C08F4/61912 , C08F4/61916 , C08F4/61927 , C08F4/63912 , C08F4/63922 , C08F4/65912 , C08F4/65927
摘要： A process for preparing a polymer of ethylene having a flow activation energy higher than that of a substantially linear ethylene polymer of the same molecular weight involving using bridged sandwich-bonded fluorenyl-containing metallocenes and the polymers resulting therefrom.
摘要翻译：一种制备乙烯聚合物的方法，其流动活化能高于相同分子量的基本上线性的乙烯聚合物的流动活化能，其涉及使用桥连的含夹心键合的含芴基金属茂和由此产生的聚合物。

4. 发明授权

US06384161B1 Method and catalyst system for producing polyolefins with broadened molecular weight distributions 失效
标题翻译：用于生产具有更宽分子量分布的聚烯烃的方法和催化剂体系
公开(公告)号：US06384161B1
公开(公告)日：2002-05-07
申请号：US09474864
申请日：1999-12-30
申请人： M. Bruce Welch , David W. Dockter , Syriac J. Palackal , Bryan E. Hauger , David C. Rohlfing
发明人： M. Bruce Welch , David W. Dockter , Syriac J. Palackal , Bryan E. Hauger , David C. Rohlfing
IPC分类号： C08F402
CPC分类号： C08F110/02 , C08F4/65904 , C08F4/65912 , C08F4/65927 , Y10S526/943 , C08F4/65916 , C08F2500/04 , C08F2500/12
摘要： The present invention provides a process for preparing a supported metallocene catalyst system that can be used to catalyze formation of polyolefins having a wide molecular weight range. In accordance with the process of the present invention, a first portion of an inorganic oxide is dried under a first set of conditions, wherein upon treatment with an organoaluminoxide and a metallocene, a first catalyst system is formed usable to produce a polyolefin product having a first molecular weight average distribution. A second portion of an inorganic oxide under a second set of conditions, wherein upon treatment with an organoaluminoxane and a metallocene, a second catalyst system is formed usable to produce polyolefin product having a second molecular weight distribution. An amount of the first portion is mixed with an amount of the second portion to produce a final inorganic oxide support. The final inorganic oxide support is combined with an organoaluminoxane and a metallocene to produce a supported metallocene catalyst system usable to catalyze formation of polyolefins with a broadened molecular weight average distribution. In another aspect, the present invention provides a process for polymerizing polyolefins using the inventive supported metallocene catalyst system. The process comprises preparing the final catalyst as mentioned above and then contacting an olefin with the final metallocene catalyst system under conditions supporting polymerization.
摘要翻译：本发明提供了一种制备负载型茂金属催化剂体系的方法，该体系可用于催化具有宽分子量范围的聚烯烃的形成。根据本发明的方法，在第一组条件下将无机氧化物的第一部分干燥，其中在用有机铝氧化物和茂金属处理时，形成可用于生产聚烯烃产品的第一催化剂体系，所述聚烯烃产物具有第一分子量平均分布。在第二组条件下的无机氧化物的第二部分，其中在用有机铝氧烷和茂金属处理时，形成可用于制备具有第二分子量分布的聚烯烃产物的第二催化剂体系。将第一部分的量与第二部分的量混合以产生最终的无机氧化物载体。最终的无机氧化物载体与有机铝氧烷和茂金属组合以产生可用于催化分子量平均分布扩大的聚烯烃形成的负载金属茂催化剂体系。另一方面，本发明提供使用本发明聚合聚烯烃的方法负载金属茂催化剂体系。该方法包括如上所述制备最终催化剂，然后在支持聚合的条件下使烯烃与最终茂金属催化剂体系接触。

5. 发明授权

US06867278B2 Olefin polymers, method of making, and use thereof 有权
标题翻译：烯烃聚合物，制备方法及其用途
公开(公告)号：US06867278B2
公开(公告)日：2005-03-15
申请号：US10373648
申请日：2003-02-24
申请人： Max P. McDaniel , Elizabeth A. Benham , Al R. Wolfe , Paul J. DesLauriers , Pamela L. Meager , William R. Coutant , David C. Rohlfing , Steven J. Secora
发明人： Max P. McDaniel , Elizabeth A. Benham , Al R. Wolfe , Paul J. DesLauriers , Pamela L. Meager , William R. Coutant , David C. Rohlfing , Steven J. Secora
IPC分类号： C08F4/12 , C08F4/22 , C08F4/24 , C08F4/52 , C08F4/69 , C08F10/00 , C08F210/16 , C08F210/14
CPC分类号： F16L9/127 , C08F10/00 , C08F210/16 , Y10T428/139 , C08F4/69 , C08F210/14 , C08F2500/12 , C08F2500/07 , C08F2500/13 , C08F2500/04 , C08F4/025
摘要： The present invention is directed to homo-polymers and copolymers of mono-1-olefins, a method of making such polymers,and uses of such polymers. Polymers of the present invention are formed by contacting at least one mono-1-olefin having from 2 to about 20 carbon atoms per molecule and at least one mono-1-olefin co-monomer having from 2 to about 10 carbon atoms per molecule in a reaction zone under polymerization conditions in the presence of a hydrocarbon diluent, a catalyst system, and a cocatalyst. In another aspect of the present invention, ethylene copolymers are employed to produce PE-100 pipe. Further, these ethylene copolymers may be employed to produce PE-100 pipe having both small diameters and diameters in excess of 42 inches substantially without sagging or other gravitational deformation. Copolymers of ethylene and 1-hexene are disclosed which are used to produce PE-100 pipe.
摘要翻译：本发明涉及单-1-烯烃的均聚物和共聚物，制备这种聚合物的方法以及这种聚合物的用途。本发明的聚合物通过使每分子具有2至约20个碳原子的至少一种单-1-烯烃和至少一种每分子具有2至约10个碳原子的单-1-烯烃共聚物接触而形成在烃稀释剂，催化剂体系和助催化剂的存在下在聚合条件下的反应区。在本发明的另一方面，乙烯共聚物用于生产PE-100管。此外，这些乙烯共聚物可用于生产具有超过42英寸的小直径和直径的PE-100管，基本上不会下垂或其它引力变形。公开了用于生产PE-100管的乙烯和1-己烯的共聚物。

6. 发明授权

US07829646B2 Olefin polymers, method of making, and use thereof 有权
标题翻译：烯烃聚合物，制备方法及其用途
公开(公告)号：US07829646B2
公开(公告)日：2010-11-09
申请号：US11227786
申请日：2005-09-15
申请人： Paul J. DesLauriers , Max P. McDaniel , Al R. Wolfe , Pamela L. Maeger , William R. Coutant , David C. Rohlfing , Steven J. Secora , William B. Beaulieu , Elizabeth A. Benham , David F. Register
发明人： Paul J. DesLauriers , Max P. McDaniel , Al R. Wolfe , Pamela L. Maeger , William R. Coutant , David C. Rohlfing , Steven J. Secora , William B. Beaulieu , Elizabeth A. Benham , David F. Register
IPC分类号： C08F210/16 , C08F210/14 , C08F10/14 , F16L9/12
CPC分类号： C08F10/00 , C08F210/16 , Y10T428/139 , C08F4/24 , C08F4/69 , C08F210/14 , C08F2500/12 , C08F2500/07 , C08F2500/13 , C08F2500/04 , C08F4/025
摘要： The present invention is directed to PE-100 ethylene copolymers and pipe made thereof having a Tabor abrasion between about 0.01 and about 0.001 grams lost/1000 revolutions. These copolymers are formed by contacting ethylene with at least one mono-1-olefin comonomer having from 2 to about 10 carbon atoms per molecule in a reaction zone under polymerization conditions in the presence of a hydrocarbon diluent, a catalyst system, and a cocatalyst. Additionally, the comonomers may be selected from mono-1-olefins having 4 to 10 carbon atoms, such as, 1-hexene, 1-butene, 4-methyl-1-pentene, 1-octene, and 1-decene. Further, these ethylene copolymers may be employed to produce PE-100 pipe having both small diameters and diameters in excess of 42 inches substantially without sagging or other gravitational deformation. Copolymers of ethylene and 1-hexene are disclosed which are used to produce PE-100 pipe.
摘要翻译：本发明涉及PE-100乙烯共聚物和由其制成的管，其具有在约0.01至约0.001克损失/ 1000转之间的泰博尔磨损。这些共聚物是通过在烃类稀释剂，催化剂体系和助催化剂的存在下，在聚合条件下，在反应区中使乙烯与至少一种每分子具有2至约10个碳原子的单-1-烯烃共聚单体接触而形成的。此外，共聚单体可以选自具有4-10个碳原子的单-1-烯烃，例如1-己烯，1-丁烯，4-甲基-1-戊烯，1-辛烯和1-癸烯。此外，这些乙烯共聚物可用于生产具有超过42英寸的小直径和直径的PE-100管，基本上不会下垂或其它引力变形。公开了用于生产PE-100管的乙烯和1-己烯的共聚物。

7. 发明申请

US20100319440A1 METHOD FOR EMPLOYING SEC-FTIR DATA TO PREDICT MECHANICAL PROPERTIES OF POLYETHYLENE 有权
标题翻译：使用SEC-FTIR数据预测聚乙烯的机械性能的方法
公开(公告)号：US20100319440A1
公开(公告)日：2010-12-23
申请号：US12868552
申请日：2010-08-25
申请人： Paul J. DesLauriers , David C. Rohlfing
发明人： Paul J. DesLauriers , David C. Rohlfing
IPC分类号： G01N9/00
CPC分类号： C08F10/00 , C08F2400/02 , C08L23/04 , G01N21/3563 , G01N30/02 , G01N33/442 , G01N2021/3595 , Y10T436/25 , C08F2/00 , C08L2666/04 , B01D15/34
摘要： The present invention provides several methods of determining values of physical or chemical properties of polymers. In these methods, at least two polymer training samples are provided. Characteristics of the polymer microstructures of the training samples are correlated with values of physical or chemical properties of the training samples. These correlations are subsequently applied to the respective characteristics of polymer test samples in order to determine the values of physical or chemical properties of the test samples.
摘要翻译：本发明提供了确定聚合物的物理或化学性质的几种方法。在这些方法中，提供至少两种聚合物训练样品。训练样本的聚合物微观结构的特征与训练样本的物理或化学性质的值相关。随后将这些相关性应用于聚合物测试样品的相应特征，以确定测试样品的物理或化学性质的值。

8. 发明授权

US07803629B2 Method for employing SEC-FTIR data to predict mechanical properties of polyethylene 有权
标题翻译：采用SEC-FTIR数据预测聚乙烯机械性能的方法
公开(公告)号：US07803629B2
公开(公告)日：2010-09-28
申请号：US11476339
申请日：2006-06-27
申请人： Paul J. DesLauriers , David C. Rohlfing
发明人： Paul J. DesLauriers , David C. Rohlfing
IPC分类号： G01N33/00
CPC分类号： C08F10/00 , C08F2400/02 , C08L23/04 , G01N21/3563 , G01N30/02 , G01N33/442 , G01N2021/3595 , Y10T436/25 , C08F2/00 , C08L2666/04 , B01D15/34
摘要： The present invention provides several methods of determining values of physical or chemical properties of polymers. In these methods, at least two polymer training samples are provided. Characteristics of the polymer microstructures of the training samples are correlated with values of physical or chemical properties of the training samples. These correlations are subsequently applied to the respective characteristics of polymer test samples in order to determine the values of physical or chemical properties of the test samples.
摘要翻译：本发明提供了确定聚合物的物理或化学性质的几种方法。在这些方法中，提供至少两种聚合物训练样品。训练样本的聚合物微观结构的特征与训练样本的物理或化学性质的值相关。随后将这些相关性应用于聚合物测试样品的相应特征，以确定测试样品的物理或化学性质的值。

9. 发明授权

US08048679B2 Method for employing SEC-FTIR data to predict mechanical properties of polyethylene 有权
标题翻译：采用SEC-FTIR数据预测聚乙烯机械性能的方法
公开(公告)号：US08048679B2
公开(公告)日：2011-11-01
申请号：US12868552
申请日：2010-08-25
申请人： Paul J. DesLauriers , David C. Rohlfing
发明人： Paul J. DesLauriers , David C. Rohlfing
IPC分类号： G01N33/00
CPC分类号： C08F10/00 , C08F2400/02 , C08L23/04 , G01N21/3563 , G01N30/02 , G01N33/442 , G01N2021/3595 , Y10T436/25 , C08F2/00 , C08L2666/04 , B01D15/34
摘要： The present invention provides several methods of determining values of physical or chemical properties of polymers. In these methods, at least two polymer training samples are provided. Characteristics of the polymer microstructures of the training samples are correlated with values of physical or chemical properties of the training samples. These correlations are subsequently applied to the respective characteristics of polymer test samples in order to determine the values of physical or chemical properties of the test samples.
摘要翻译：本发明提供了确定聚合物的物理或化学性质的几种方法。在这些方法中，提供至少两种聚合物训练样品。训练样本的聚合物微观结构的特征与训练样本的物理或化学性质的值相关。随后将这些相关性应用于聚合物测试样品的相应特征，以确定测试样品的物理或化学性质的值。

10. 发明申请

US20100160579A1 PROCESS FOR PRODUCING BROADER MOLECULAR WEIGHT DISTRIBUTION POLYMERS WITH A REVERSE COMONOMER DISTRIBUTION AND LOW LEVELS OF LONG CHAIN BRANCHES 有权
标题翻译：用于生产广泛分子量分布聚合物的方法，具有反向共享分布和长链分支的低水平
公开(公告)号：US20100160579A1
公开(公告)日：2010-06-24
申请号：US12338225
申请日：2008-12-18
申请人： Qing Yang , Max P. McDaniel , Joel L. Martin , Tony R. Crain , Randy S. Muninger , Jerry T. Lanier , Jeff S. Fodor , Paul J. Deslauriers , Chung C. Tso , David C. Rohlfing
发明人： Qing Yang , Max P. McDaniel , Joel L. Martin , Tony R. Crain , Randy S. Muninger , Jerry T. Lanier , Jeff S. Fodor , Paul J. Deslauriers , Chung C. Tso , David C. Rohlfing
IPC分类号： C08F4/76 , C08F4/06 , C08F4/12 , C08F4/18 , C08F210/00
CPC分类号： C08F210/16 , C08F4/65912 , C08F4/65916 , Y10S526/905 , Y10S526/943 , Y10T428/1352 , Y10T428/139 , Y10T428/2913 , Y10T428/2915 , C08F4/65927 , C08F210/14 , C08F2500/12 , C08F2500/04 , C08F2500/09 , C08F2500/10
摘要： The present invention provides a polymerization process which is conducted by contacting an olefin monomer and at least one olefin comonomer in the presence of hydrogen and a metallocene-based catalyst composition. Polymers produced from the polymerization process are also provided, and these polymers have a reverse comonomer distribution, low levels of long chain branches, and a ratio of Mw/Mn from about 3 to about 6.
摘要翻译：本发明提供聚合方法，其通过使烯烃单体和至少一种烯烃共聚单体在氢和茂金属基催化剂组合物的存在下接触进行。还提供了由聚合反应生成的聚合物，这些聚合物具有反相共聚单体分布，低水平的长支链，Mw / Mn约为3至6的比例。

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