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1. 发明授权

US5514307A Process for the reducing emissions during prilling of material such as ammonium nitrate 失效
标题翻译：在造粒诸如硝酸铵等材料时减少排放的过程
公开(公告)号：US5514307A
公开(公告)日：1996-05-07
申请号：US280245
申请日：1994-07-25
申请人： Arthur R. Shirley, Jr. , Phillip A. Forsythe , William M. Giles , John A. Phillips
发明人： Arthur R. Shirley, Jr. , Phillip A. Forsythe , William M. Giles , John A. Phillips
IPC分类号： B01J2/04 , C05C1/02 , C05C9/00 , C05G3/00
CPC分类号： C05G3/0058 , B01J2/04 , C05C1/02 , C05C9/005
摘要： This invention relates to an improvement in prilling whereby water is atomized into a prill tower to affect faster solidification of the prill, and in particular, the outside surface of the prill by providing an increased rate of surface cooling while reducing the required air flows in the tower. This results in a major reduction in air pollution potential in the form of both fume and particulate while at the same time allowing substantial production rate increases. Specifically, the invention relates to quick freezing the outside surface of the prill by flash evaporation of finely atomized water particles on the surface of the prill or in extremely close proximity to the prill to greatly lower the vapor pressure at the prill's surface and by continued flash evaporation to enhance cooling so as to allow upward flowing air to be reduced to a point where micro-prills which are formed in prilling can settle in the prill tower while obtaining the same or increased production rates. More specifically, the present invention relates to an improvement in melt prilling of water sensitive materials, in particular, ammonium nitrate, urea, potassium nitrate and other water soluble melts which normally absorb water or go into solution readily at ambient conditions in their solid state.
摘要翻译：本发明涉及造粒的改进，其中水被雾化成造粒塔，以通过提供增加的表面冷却速率来影响颗粒的更快凝固，特别是造粒的外表面，同时减少所需的空气流塔。这导致大气中的烟气和微粒形式的空气污染潜力的大幅减少，同时允许大量的生产率增加。具体而言，本发明涉及通过在颗粒表面上微细雾化的水颗粒的闪蒸或者非常接近于颗粒的方式快速冷冻颗粒的外表面，以大大降低颗粒表面的蒸汽压力并持续闪光蒸发以增强冷却，以允许向上流动的空气减少到在造粒中形成的微小颗粒可以在获得相同或增加的生产率的同时沉淀在造粒塔中。更具体地说，本发明涉及水溶性材料，特别是硝酸铵，尿素，硝酸钾和其它水溶性熔体的熔融造粒的改进，其通常在固态环境条件下吸收水或溶解在溶液中。

2. 发明授权

US4793783A Apparatus for producing prills 失效
标题翻译：用于制造颗粒的装置
公开(公告)号：US4793783A
公开(公告)日：1988-12-27
申请号：US5507
申请日：1987-01-20
申请人： A. Michael Huey , Arthur R. Shirley, Jr. , Phillip A. Forsythe
发明人： A. Michael Huey , Arthur R. Shirley, Jr. , Phillip A. Forsythe
IPC分类号： B01J2/02 , B01J2/04 , B01J2/16 , B29B9/00 , C07C37/70 , C07C39/15 , B22D11/01
CPC分类号： B01J2/16 , B01J2/04
摘要： A prilling apparatus and process for producing seed material for size enlargement processes such as a granulation process for bisphenol. The apparatus includes a fluidized bed system with a spray header therein for producing spray droplets of material in a gaseous stream such as nitrogen to form prills of less than about 1 mm diameter.

3. 发明授权

US4935173A Process for producing prills 失效
标题翻译：生产饲料的方法
公开(公告)号：US4935173A
公开(公告)日：1990-06-19
申请号：US290716
申请日：1988-12-23
申请人： A. Michael Huey , Arthur R. Shirley, Jr. , Phillip A. Forsythe
发明人： A. Michael Huey , Arthur R. Shirley, Jr. , Phillip A. Forsythe
IPC分类号： B01J2/04 , B01J2/16 , C07C37/70
CPC分类号： C07C37/70 , B01J2/04 , B01J2/16
摘要： A prilling apparatus and process for producing seed material for size enlargement processes such as a granulation process for bisphenol. The apparatus includes a fluidized bed system with a spray header therein for producing spray droplets of material in a gaseous stream such as nitrogen to form prills of less than about 1 mm diameter.
摘要翻译：一种用于生产用于尺寸增大过程的种子材料的造粒装置和方法，例如双酚的造粒方法。该装置包括其中具有喷射头的流化床系统，用于在诸如氮气的气流中产生材料的喷雾液滴，以形成小于约1mm直径的颗粒。

4. 发明授权

US4424176A Process for granulation of molten materials 失效
标题翻译：熔融材料造粒工艺
公开(公告)号：US4424176A
公开(公告)日：1984-01-03
申请号：US427723
申请日：1982-09-29
申请人： Arthur R. Shirley, Jr. , Frederick T. Carney, Jr.
发明人： Arthur R. Shirley, Jr. , Frederick T. Carney, Jr.
IPC分类号： B01J2/12
CPC分类号： B01J2/12 , C01B17/0216 , C01B17/0237 , Y02P20/124
摘要： The granulation of molten material using a heat transfer process whereby solid particles are heated, dried, or cooled by a gas: Particles are repeatedly lifted and dropped as, for example, in flighted rotary drums. By forced recirculation, gas is passed through showering particles generally perpendicular to their plane of fall. Examples show gas forced to contact particles in this manner imparts an overall volumetric heat transfer coefficient to a rotary drum superior to that expected from classical literature or presently operating rotary drum heat exchangers. Disclosure teaches gas temperature adjustment between forced recirculations. Technique usage will reduce exchanger capital cost, increase energy efficiency, and reduce pollution problems. Also, prewetting of the particles in certain instances can be utilized to effect substantially increased pseudo volumetric heat transfer coefficients when cooling non-hygroscopic materials.
摘要翻译：使用传热过程对熔融材料进行造粒，其中固体颗粒被加热，干燥或被气体冷却：颗粒被重复地提升和下降，例如在旋转的转鼓中。通过强制再循环，气体通过大致垂直于其下降平面的淋浴颗粒。实施例显示以这种方式强制接触颗粒的气体赋予旋转鼓的总体积传热系数优于传统文献或目前操作的旋转鼓式热交换器所预期的。泄露教导了强制循环之间的气体温度调节。技术使用将降低交换机资本成本，提高能源效率，减少污染问题。而且，当冷却非吸湿性材料时，在某些情况下，可以利用颗粒的预润湿来实现显着提高的假体积传热系数。

5. 发明授权

UST980005I4 Granulation and coating by improved method of heat removal 失效
标题翻译：通过改进的除热方法制粒和涂层
公开(公告)号：UST980005I4
公开(公告)日：1979-03-06
申请号：US850588
申请日：1977-11-11
申请人： Arthur R. Shirley, Jr.
发明人： Arthur R. Shirley, Jr.
IPC分类号： B01J2/00 , B01J2/12 , C01B17/02 , C05C9/00
CPC分类号： B01J2/12 , B01J2/006 , C01B17/0237 , C01B17/0248 , C05C9/005
摘要： an improved process for the granulation or coating of hygroscopic or nonhygroscopic materials where melt is sprayed onto cascading granules of common or uncommon substrate in an enclosed vessel such as a rotary drum preferably with lifting flights which provide maximum mixing of the granules and the atmosphere enclosed in the unit and where heat given off by solidification of the melt is absorbed by evaporation of water which is atomized as an extremely fine mist into areas of the vessel which are not subtended by falling granules. Evaporation is effected without impingement of the mist on the granules or vessel internals. Air for evaporation is pulled through the vessel concurrent with the flow of granules and its moisture content is regulated below the critical humidity of the granules throughout the vessel. Some recycle of undersize granules discharged from the vessel is maintained for size control; however, examples show the recycle rate decreased by 87 percent over recycle cooled processes as 73 percent of the heat evolved is removed by evaporation of water mist. An equation is developed which mathematically represents the thermodynamics of the process and specific values are presented for variables when granulating sulfur or urea.

6. 发明授权

US5395449A Apparatus and process for coating particles 失效
标题翻译：用于涂覆颗粒的装置和方法
公开(公告)号：US5395449A
公开(公告)日：1995-03-07
申请号：US977205
申请日：1992-11-16
申请人： Sayeeda J. Quadir , Russell I. Derrah , Arthur R. Shirley, Jr. , Keith D. Cochran , Terence B. Lynch , Zdzislaw M. Tulimowski
发明人： Sayeeda J. Quadir , Russell I. Derrah , Arthur R. Shirley, Jr. , Keith D. Cochran , Terence B. Lynch , Zdzislaw M. Tulimowski
IPC分类号： B01J2/16 , B01J8/24 , B01J8/26 , B05C19/02 , C05C13/00 , C05G3/00 , C05G5/00 , B05C5/00
CPC分类号： B01J2/16 , B01J8/26 , C05G3/0029 , Y10S118/05
摘要： An apparatus and method for continuously producing polymer coated particles, and in particular, a polymer coated fertilizer, wherein the coating material used is, for example, an aqueous film forming latex. The coating process is conducted with a plurality of fluidized beds, connected in series, under conditions such that, preferably, the relative humidity of the air in the initial coating zones is maintained below the critical relative humidity of the particle to be coated. The apparatus and process provides a method to prepare coated particles having a narrow coating weight distribution, and thus allows for the economical production of a slow release fertilizer.
摘要翻译：用于连续生产聚合物涂覆的颗粒，特别是聚合物涂覆的肥料的设备和方法，其中使用的涂料是例如水性成膜胶乳。涂覆过程是在多个流化床中串联连续进行的，这些条件使得初始涂层区域中的空气的相对湿度优选保持在待涂覆颗粒的临界相对湿度以下。该设备和方法提供了制备具有窄涂层重量分布的涂覆颗粒的方法，因此允许经济地生产缓释肥料。

7. 发明授权

US5108034A Spray header and nozzle assembly 失效
标题翻译：喷头和喷嘴组件
公开(公告)号：US5108034A
公开(公告)日：1992-04-28
申请号：US233932
申请日：1988-08-15
申请人： Andrew M. Huey , Arthur R. Shirley, Jr.
发明人： Andrew M. Huey , Arthur R. Shirley, Jr.
IPC分类号： B01J2/12 , B05B1/24
CPC分类号： B01J2/12 , B05B1/24
摘要： A spray header and nozzle assembly which includes a first elongated tubular member and a second elongated tubular member of a smaller diameter than the first tubular member coaxially disposed within the first tubular member to form an annular space between the first and second tubular members and a plurality of spray nozzle assemblies in fluid communication with the inside of the second tubular member. The spray nozzle assemblies are perpendicularly disposed to the axis of both tubular members and recessed into the annular space. Also, the nozzle assemblies include a first tube extending a predetermined distance beyond the circumference of the first tubular member and a second tube of a smaller diameter than the first tube coaxially disposed within the first tube and recessed into the first tube.
摘要翻译：一种喷雾头和喷嘴组件，其包括第一细长管状构件和直径小于同轴地设置在第一管状构件内的第一管状构件的第二细长管状构件，以在第一和第二管状构件之间形成环形空间，并且多个的喷嘴组件与第二管状构件的内部流体连通。喷嘴组件垂直地设置在两个管状构件的轴线上并且凹入环形空间中。此外，喷嘴组件包括延伸超过第一管状构件的圆周的预定距离的第一管和直径小于同轴地设置在第一管内并凹入第一管的第一管的直径的第二管。

8. 发明授权

US08758474B2 Urea fertilizer containing central volatilization inhibitor particles to reduce release of ammonia and processes for making same 有权
标题翻译：尿素肥料含有中心挥发抑制剂颗粒以减少氨的释放和制备相同的工艺
公开(公告)号：US08758474B2
公开(公告)日：2014-06-24
申请号：US13071286
申请日：2011-03-24
申请人： Taylor Pursell , Arthur R. Shirley, Jr. , Keith D. Cochran , Joseph M. Miller , Timothy G. Holt , Gregory S. Peeden
发明人： Taylor Pursell , Arthur R. Shirley, Jr. , Keith D. Cochran , Joseph M. Miller , Timothy G. Holt , Gregory S. Peeden
IPC分类号： C05D9/00 , C05D9/02 , C01C1/18 , C05C3/00 , A01N25/00 , C05C9/00 , C05G3/00 , C05B1/00 , B01J2/00 , B01J2/30
CPC分类号： C05G3/08 , B01J2/003 , B01J2/30 , C05B1/00 , C05C9/00 , C05C9/005 , C05D9/02 , C05G3/0041
摘要： A urea fertilizer having reduced ammonia volatilization upon application to soil including a central particle having an outer surface and comprising ammonia volatilization inhibiting compounds containing one or more of boron and iodine, and a coating of urea on the outer surface of the central particle, and further a process of making the fertilizer including the steps of: granulating ammonia volatilization inhibiting compounds containing one or more of boron and iodine, with a binder to produce volatilization inhibitor particles; screening the inhibitor particles to a preselected particle size; spraying melted urea onto the surface of the inhibitor particles to produce a coating on the inhibitor particles; granulating the coated inhibitor particles with sprayed melted urea to produce granules of urea coated central volatilization particles; and cooling the granules.
摘要翻译：一种尿素肥料，其在施用于土壤时具有减少的氨挥发，包括具有外表面的中心颗粒，并且包含含有硼和碘中的一种或多种的氨挥发抑制化合物和在中心颗粒的外表面上的尿素涂层，制造肥料的方法包括以下步骤：将含有硼和碘的一种或多种的氨挥发抑制化合物与粘合剂一起制成以产生挥发抑制剂颗粒; 将抑制剂颗粒筛选到预选的粒度; 将熔融的尿素喷洒到抑制剂颗粒的表面上以在抑制剂颗粒上产生涂层; 用喷射的熔融尿素对涂覆的抑制剂颗粒进行造粒，生成尿素包覆的中心挥发颗粒的颗粒; 并冷却颗粒。

9. 发明授权

US5399186A Apparatus and process for coating particles 失效
公开(公告)号：US5399186A
公开(公告)日：1995-03-21
申请号：US977102
申请日：1992-11-16
申请人： Russell Derrah , Sayeeda Quadir , Arthur R. Shirley, Jr. , Keith D. Cochran , Terence B. Lynch , Zdzislaw M. Tulimowski
发明人： Russell Derrah , Sayeeda Quadir , Arthur R. Shirley, Jr. , Keith D. Cochran , Terence B. Lynch , Zdzislaw M. Tulimowski
IPC分类号： B01J2/16 , B01J8/24 , B01J8/26 , B05C19/02 , C05C13/00 , C05G3/00 , C05G5/00 , B05D7/00
CPC分类号： B01J2/16 , B01J8/26 , C05G3/0029 , Y10S118/05
摘要： An apparatus and method for continuously producing polymer coated particles, and in particular, a polymer coated fertilizer, wherein the coating material used is, for example, an aqueous film forming latex. The coating process is conducted with a plurality of fluidized beds, connected in series, under conditions such that, preferably, the relative humidity of the air in the initial coating zones is maintained below the critical relative humidity of the particle to be coated. The apparatus and process provides a method to prepare coated particles having a narrow coating weight distribution, and thus allows for the economical production of a slow release fertilizer.

10. 发明授权

US5211985A Multi-stage process for continuous coating of fertilizer particles 失效
标题翻译：多级颗粒连续涂层的多阶段工艺
公开(公告)号：US5211985A
公开(公告)日：1993-05-18
申请号：US773273
申请日：1991-10-09
申请人： Arthur R. Shirley, Jr. , Keith D. Cochran , Terence B. Lynch , Russell I. Derrah , Sayeeda J. Quadir , Zdzislaw M. Tulimowski
发明人： Arthur R. Shirley, Jr. , Keith D. Cochran , Terence B. Lynch , Russell I. Derrah , Sayeeda J. Quadir , Zdzislaw M. Tulimowski
IPC分类号： B01J2/16 , B01J8/24 , B01J8/26 , B05C19/02 , C05C13/00 , C05G3/00 , C05G5/00
CPC分类号： B01J2/16 , B01J8/26 , C05G3/0029 , Y10S118/05
摘要： An apparatus and method for continuously producing polymer coated particles, and in particular, a polymer coated fertilizer, wherein the coating material used is, for example, an aqueous film forming latex. The coating process is conducted with a plurality of fluidized beds, connected in series, under conditions such that, preferably, the relative humidity of the air in the initial coating zones is maintained below the critical relative humidity of the particle to be coated.
摘要翻译：用于连续生产聚合物涂覆的颗粒，特别是聚合物涂覆的肥料的设备和方法，其中使用的涂料是例如水性成膜胶乳。涂覆过程是在多个流化床中串联连续进行的，这些条件使得初始涂层区域中的空气的相对湿度优选保持在待涂覆颗粒的临界相对湿度以下。

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