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    • 1. 发明授权
    • Low temperature vacuum distillation and concentration process
    • 低温真空蒸馏浓缩过程
    • US5955135A
    • 1999-09-21
    • US840347
    • 1997-04-28
    • Armand R. BoucherPhilip N. Hambrick
    • Armand R. BoucherPhilip N. Hambrick
    • B01D1/02B01D1/22B01D3/06B01D3/10B01D3/38B01D3/42C12G3/08C12G3/12C12H3/02
    • B01D3/065B01D1/02B01D1/22B01D3/06B01D3/10B01D3/38B01D3/4205C12G3/08C12G3/12Y10S203/06
    • An apparatus and method for stripping volatiles from a feed stream and concentrating the volatiles in the overhead vapors forming a condensate product and simultaneously producing a low percent volatiles outlet stream as a concentrate product. The volatiles separator and concentrator, ("VSC"), unit has many applications in the reduction and the concentration of volatiles in the beverage, fuel, and industrial alcohol industries, as well as in chemical applications for removing or stripping volatiles from heat sensitive feed substrates which require low temperatures and a short residence time to prevent degradation of the product. The preferred embodiment of the VSC unit utilizes a short feed stream preheat contact time in combination with turbulent high velocity flow at temperatures below 100.degree. F. to provide flash vaporization for volatiles separation with reboil capability to adjust volatiles concentration in the residue and product. The application of high vacuum in the range of 27" to 28.5" of Hg further enhances volatiles separation by allowing lower processing temperatures and reduced residence time. The low pressures and temperatures are energy efficient and serve to minimize heat degradation producing a non-heat sensitized product/residue. Because of the design of the equipment utilized in the VSC unit, a plurality of VSC modular units can be connected in a series providing a processing system having compact dimensions.
    • 一种用于从进料流中汽提挥发物并将挥发物浓缩在塔顶蒸气中形成冷凝物的装置和方法,同时产生作为浓缩物产物的低百分比挥发物出口流。 挥发物分离器和浓缩器(“VSC”)单元在饮料,燃料和工业酒精工业中的挥发物的还原和浓缩以及用于从热敏感进料中除去或汽提挥发物的化学应用中具有许多应用 需要低温和短停留时间以防止产品降解的底物。 VSC装置的优选实施例使用短的进料流预热接触时间与低于100°F的湍流高速流动相结合,以提供用于挥发物分离的闪蒸蒸发,其具有再沸性能以调节残余物和产物中的挥发物浓度。 通过允许较低的加工温度和减少的停留时间,在Hg的27“至28.5”范围内的高真空度的应用进一步增强了挥发物的分离。 低压和低温是节能的并且用于最小化产生非热敏产物/残渣的热降解。 由于在VSC单元中使用的设备的设计,可以串联连接多个VSC模块单元,提供具有紧凑尺寸的处理系统。
    • 4. 发明授权
    • Volatiles separator and concentrator
    • 挥发分离器和浓缩器
    • US5458739A
    • 1995-10-17
    • US191873
    • 1994-02-04
    • Armand R. BoucherPhilip N. Hambrick
    • Armand R. BoucherPhilip N. Hambrick
    • B01D1/02B01D1/22B01D3/06B01D3/10B01D3/38B01D3/42C12G3/08C12G3/12C12H3/02B01D3/32
    • B01D3/065B01D1/02B01D1/22B01D3/06B01D3/10B01D3/38B01D3/4205C12G3/08C12G3/12Y10S203/06
    • An apparatus and method for stripping volatiles from a feed stream and concentrating the volatiles in the overhead vapors forming a condensate product and simultaneously producing a low percent volatiles outlet stream as a concentrate product. The volatiles separator and concentrator, ("VSC"), unit has many applications in the reduction and the concentration of volatiles in the beverage, fuel, and industrial alcohol industries, as well as in chemical applications for removing or stripping volatiles from heat sensitive feed substrates which require low temperatures and a short residence time to prevent degradation of the product.The preferred embodiment of the VSC unit utilizes a short feed stream preheat contact time in combination with turbulent high velocity flow at temperatures below 100.degree. F. to provide flash aporization for volatiles separation with reboil capability to adjust volatiles concentration in the residue and product. The application of high vacuum in the range of 27" to 28.5" of Hg further enhances volatiles separation by allowing lower processing temperatures and reduced residence time. The low pressures and temperatures are energy efficient and serve to minimize heat degradation producing a non-heat sensitized product/residue. Because of the design of the equipment utilized in the VSC unit, a plurality of VSC modular units can be connected in a series providing a processing system having compact dimensions.
    • 一种用于从进料流中汽提挥发物并将挥发物浓缩在塔顶蒸气中形成冷凝物的装置和方法,同时产生作为浓缩物产物的低百分比挥发物出口流。 挥发物分离器和浓缩器(“VSC”)单元在饮料,燃料和工业酒精工业中的挥发物的还原和浓缩以及用于从热敏感进料中除去或汽提挥发物的化学应用中具有许多应用 需要低温和短停留时间以防止产品降解的底物。 VSC装置的优选实施例在低于100°F的温度下,与短时间的进料流预热接触时间结合湍流高速流动,以提供用于挥发物分离的闪蒸装置,其中再沸器能够调节残余物和产物中的挥发物浓度。 通过允许较低的加工温度和减少的停留时间,在Hg的27“至28.5”范围内的高真空度的应用进一步增强了挥发物的分离。 低压和低温是节能的并且用于最小化产生非热敏产物/残渣的热降解。 由于在VSC单元中使用的设备的设计,可以串联连接多个VSC模块单元,提供具有紧凑尺寸的处理系统。
    • 5. 发明授权
    • Volatiles separator and concentrator
    • 挥发分离器和浓缩器
    • US5624534A
    • 1997-04-29
    • US477650
    • 1995-06-07
    • Armand R. BoucherPhilip N. Hambrick
    • Armand R. BoucherPhilip N. Hambrick
    • B01D1/02B01D1/22B01D3/06B01D3/10B01D3/38B01D3/42C12G3/08C12G3/12C12H3/02B01D3/32
    • B01D3/065B01D1/02B01D1/22B01D3/06B01D3/10B01D3/38B01D3/4205C12G3/08C12G3/12Y10S203/06
    • An apparatus and method for stripping volatiles from a feed stream and concentrating the volatiles in the overhead vapors forming a condensate product and simultaneously producing a low percent volatiles outlet stream as a concentrate product. The volatiles separator and concentrator, ("VSC"), unit has many applications in the reduction and the concentration of voiatiles in the beverage, fuel, and industrial alcohol industries, as well as in chemical applications for removing or stripping volatiles from heat sensitive feed substrates which require low temperatures and a short residence time to prevent degradation of the product. For heat sensitive applications, the VSC unit utilizes a short feed stream preheat contact time in combination with turbulent high velocity flow to separate and concentrate volatile and nonvolatile components at temperatures below 100.degree. F. utilizing flash vaporization for volatiles separation with reboil capability to adjust volatiles concentration in the residue and product. The application of high vacuum in the range of 27" to 28.5" of Hg further enhances volatiles separation by allowing lower processing temperatures and reduced residence time. The low pressures and temperatures are energy efficient and serve to minimize heat degradation producing a non-heat sensitized product/residue. Because of the design of the equipment utilized in the VSC unit, a plurality of VSC modular units can be connected in a series providing a processing system having compact dimensions for vacuum or atmospheric operations. Combining multiple VSC units with columns utilizing the principals provides a means for fractional or selective distillation.
    • 一种用于从进料流中汽提挥发物并将挥发物浓缩在塔顶蒸气中形成冷凝物的装置和方法,同时产生作为浓缩物产物的低百分比挥发物出口流。 挥发物分离器和浓缩器(“VSC”)单元在饮料,燃料和工业酒精工业中的还原和浓缩中具有许多应用,以及用于从热敏饲料中除去或汽提挥发物的化学应用 需要低温和短停留时间以防止产品降解的底物。 对于热敏应用,VSC装置利用短的进料流预热接触时间与湍流的高速流动结合,以在低于100°F的温度下分离和浓缩挥发性和非挥发性组分。利用闪蒸蒸发挥发物与再沸能力分离以调节挥发物 残留物和产品中的浓度。 通过允许较低的加工温度和减少的停留时间,在Hg的27“至28.5”范围内的高真空度的应用进一步增强了挥发物的分离。 低压和低温是节能的并且用于最小化产生非热敏产物/残渣的热降解。 由于VSC单元中使用的设备的设计,多个VSC模块单元可以串联连接,提供具有用于真空或大气操作的紧凑尺寸的处理系统。 将多个VSC装置与利用原料的塔组合提供了分馏或选择性蒸馏的方法。