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1. 发明授权

US08288005B2 Fluoropolymer compositions and method of making and using thereof 有权
标题翻译：含氟聚合物组合物及其制备和使用方法
公开(公告)号：US08288005B2
公开(公告)日：2012-10-16
申请号：US13056135
申请日：2009-04-16
申请人： Anthony P. Manzara , Yvan A. Bogaert , Michael D. Crandall , Robert E. Eggers , Aron Y. Goodner , Werner M. A. Grootaert
发明人： Anthony P. Manzara , Yvan A. Bogaert , Michael D. Crandall , Robert E. Eggers , Aron Y. Goodner , Werner M. A. Grootaert
IPC分类号： B32B27/00
CPC分类号： C08K5/28 , Y10T428/139 , Y10T428/1397 , Y10T428/3154 , Y10T428/31544 , C08L27/12
摘要： Compositions having a fluoropolymer with a nitrile-containing cure site and at least a) a mono azide with at least one functional group in the beta position, or b) a polyazide, as a curing agent as well as methods and articles thereof are described. Articles of this disclosure are found to exhibit excellent chemical resistance and thermal stability.
摘要翻译：具有具有含腈固化部位的含氟聚合物和至少a）在β位具有至少一个官能团的单叠氮化物的组合物，或b）作为固化剂的聚叠氮化合物及其制备方法。发现本公开的制品表现出优异的耐化学性和热稳定性。

2. 发明授权

US08445601B2 Polymeric compositions and method of making and articles thereof 有权
标题翻译：聚合物组合物及其制备方法及其制品
公开(公告)号：US08445601B2
公开(公告)日：2013-05-21
申请号：US12271222
申请日：2008-11-14
申请人： Michael D. Crandall , Yvan A. Bogaert , Aron Y. Goodner , Werner M. A. Grootaert , Anthony P. Manzara
发明人： Michael D. Crandall , Yvan A. Bogaert , Aron Y. Goodner , Werner M. A. Grootaert , Anthony P. Manzara
IPC分类号： C08C19/22
CPC分类号： C09D133/00 , C08F220/12 , C08F220/18 , C08F220/34 , C08K5/28 , C08L2312/00 , C08F220/06 , C08F238/00 , C08F220/14
摘要： Described herein are substantially linear copolymeric compositions having at least two azide groups and at least two non-activated acetylene groups. The azide groups and the non-activated acetylene groups are reacted to cure the substantially linear copolymer composition. Also, described are methods of making and using such substantially linear copolymeric compositions.
摘要翻译：本文描述的是具有至少两个叠氮基和至少两个非活化乙炔基团的基本上线性的共聚组合物。使叠氮化物基团和非活化乙炔基团反应以固化基本上线性的共聚物组合物。还描述了制备和使用这种基本上线性的共聚组合物的方法。

3. 发明申请

US20080116603A1 DUAL CURE HYDROTALCITE CONTAINING FLUOROPOLYMER COMPOSITIONS 失效
标题翻译：含有氟聚合物组合物的双酚水合物
公开(公告)号：US20080116603A1
公开(公告)日：2008-05-22
申请号：US11561677
申请日：2006-11-20
申请人： Werner M. A. Grootaert , Robert E. Eggers
发明人： Werner M. A. Grootaert , Robert E. Eggers
IPC分类号： C08K3/10
CPC分类号： C08K3/10 , C08K3/26 , C08K5/14 , C08L27/12
摘要： Provided is a curable fluoropolymer composition comprising a fluoropolymer comprising interpolymerized units of tetrafluoroethylene, perfluoro(aliphatic vinyl)ether, and a nitrogen-containing cure site monomer; a catalyst to form cross-links with the nitrogen-containing cure site monomer; an organic peroxide; a co-agent to participate in a peroxide cure; and a hydrotalcite compound. Also provided is an article comprising the cured fluoropolymer reaction product of the curable composition and a method for forming a shaped article.
摘要翻译：本发明提供一种含氟聚合物的可固化含氟聚合物组合物，其包含四氟乙烯，全氟（脂族乙烯基）醚和含氮固化点单体的共聚单元; 与含氮固化位点单体形成交联的催化剂; 有机过氧化物; 参与过氧化物治疗的助剂; 和水滑石化合物。还提供了包含可固化组合物的固化的氟聚合物反应产物和用于形成成型制品的方法的制品。

4. 发明授权

US07592386B2 Dual cure hydrotalcite containing fluoropolymer compositions 失效
标题翻译：双固化水滑石含氟聚合物组合物
公开(公告)号：US07592386B2
公开(公告)日：2009-09-22
申请号：US11561677
申请日：2006-11-20
申请人： Werner M. A. Grootaert , Robert E. Eggers
发明人： Werner M. A. Grootaert , Robert E. Eggers
IPC分类号： C08K3/26
CPC分类号： C08K3/10 , C08K3/26 , C08K5/14 , C08L27/12
摘要： Provided is a curable fluoropolymer composition comprising a fluoropolymer comprising interpolymerized units of tetrafluoroethylene, perfluoro(aliphatic vinyl)ether, and a nitrogen-containing cure site monomer; a catalyst to form cross-links with the nitrogen-containing cure site monomer; an organic peroxide; a co-agent to participate in a peroxide cure; and a hydrotalcite compound. Also provided is an article comprising the cured fluoropolymer reaction product of the curable composition and a method for forming a shaped article.
摘要翻译：本发明提供一种含氟聚合物的可固化含氟聚合物组合物，其包含四氟乙烯，全氟（脂族乙烯基）醚和含氮固化点单体的共聚单元; 与含氮固化位点单体形成交联的催化剂; 有机过氧化物; 参与过氧化物治疗的助剂; 和水滑石化合物。还提供了包含可固化组合物的固化的氟聚合物反应产物和用于形成成型制品的方法的制品。

5. 发明申请

US20110009569A1 PERFLUOROELASTOMERS WITH LOW CARBONYL ENDGROUP RATIOS 有权
标题翻译：具有低碳骨结构比例的全氟聚合物
公开(公告)号：US20110009569A1
公开(公告)日：2011-01-13
申请号：US12919783
申请日：2009-02-02
申请人： Werner M. A. Grootaert , Kai H. Lochhaas
发明人： Werner M. A. Grootaert , Kai H. Lochhaas
IPC分类号： C08F8/40 , C08F8/34 , C08F8/30 , C08F4/00 , C08F4/32 , C08F16/24
CPC分类号： C08F214/262 , C08F214/18
摘要： A composition and method of making having a perfluoroelastomer gum with a nitrogen-containing cure site and an end group represented by —CF3—CF2H, —CFH2, and/or —CH3, and having a low carbonyl-containing end group ratio, which yield cured fluoroelastomers with improved retained sealing force and articles therefrom.
摘要翻译：具有由含氟固化位点和由-CF 3 -CF 2 H，-CFH 2和/或-CH 3表示的端基的全氟弹性体胶和具有低羰基端基比的组成和方法，其产率固化的含氟弹性体具有改进的保持密封力和其制品。

6. 发明授权

US07208553B2 Fluoropolymer curing system 有权
标题翻译：含氟聚合物固化体系
公开(公告)号：US07208553B2
公开(公告)日：2007-04-24
申请号：US10944926
申请日：2004-09-20
申请人： Werner M. A. Grootaert , Robert E. Kolb , Klaus Hintzer
发明人： Werner M. A. Grootaert , Robert E. Kolb , Klaus Hintzer
IPC分类号： C08F8/34
CPC分类号： C08K5/19 , C08L27/18 , C08L2205/02 , C08L27/12 , C08L2666/04
摘要： A composition of a fluoropolymer comprising interpolymerized units of nitrogen-containing cure site monomer and a catalyst comprising a compound having the formula: wherein HA is an acid, each R1, R2, and R3 is independently a C1–C20 alkyl group, which may be cyclic or heterocyclic, or Rf(CH2)x— wherein Rf is a C1–C8 linear or branched and at least partially fluorinated, and x is 1 to 4, and one R group may be a bond to another R group such that the nitrogen is bonded to or part of an alkenyl, cycloalkenyl, or aromatic group. This may further comprise a catalyst composition comprising a compound of the formula R1C(OR2)═NH, and salts thereof, where each R1 and R2 is, independently, a substituted or unsubstituted alkyl, aryl, aralkyl, alkenyl, cycloalkyl, or cycloalkenyl. Also provided are a method of making a fluoropolymer composition and articles prepared from the compositions.
摘要翻译：含氟聚合物的组合物，其包含含氮固化位点单体的互聚单元和包含具有下式的化合物的催化剂：其中HA是酸，每个R 1，R 2

7. 发明授权

US07094839B2 Process for making a fluoroelastomer 有权
标题翻译：制备含氟弹性体的方法
公开(公告)号：US07094839B2
公开(公告)日：2006-08-22
申请号：US10627149
申请日：2003-07-25
申请人： Werner M. A. Grootaert , Klaus Hintzer , Bernhard Hirsch , Harald Kaspar , Robert E. Kolb , Gernot Löhr , Werner Schwertfeger
发明人： Werner M. A. Grootaert , Klaus Hintzer , Bernhard Hirsch , Harald Kaspar , Robert E. Kolb , Gernot Löhr , Werner Schwertfeger
IPC分类号： C08L27/12
CPC分类号： C08F214/18 , C08F14/18
摘要： Aqueous microemulsions obtained from a perfluorinated alkane sulphonic or carboxylic acid or salt thereof, a liquid fluorinated monomer comprising a cure-site and optionally an inert liquid and highly fluorinated hydrocarbon compound. The aqueous microemulsion may be formed by mixing together water, a perfluorinated alkane sulphonic or carboxylic acid or salt thereof, optionally an inert liquid and highly fluorinated hydrocarbon compound and a liquid fluorinated monomer having a cure-site.
摘要翻译：由全氟化烷烃磺酸或其羧酸或其盐获得的水性微乳液，包含固化部位和任选的惰性液体和高度氟化烃化合物的液体氟化单体。水性微乳液可以通过将水，全氟化烷烃磺酸或其羧酸或其盐，任选的惰性液体和高度氟化的烃化合物和具有固化位点的液体氟化单体混合在一起而形成。

8. 发明授权

US06933357B2 Ultra-clean fluoropolymers 有权
标题翻译：超清洁含氟聚合物
公开(公告)号：US06933357B2
公开(公告)日：2005-08-23
申请号：US10785450
申请日：2004-02-24
申请人： Werner M. A. Grootaert , Georg Burkard , William D. Coggio , Klaus Hintzer , Bernhard Hirsch , Robert E. Kolb , Albert Killich , Gernot Loehr
发明人： Werner M. A. Grootaert , Georg Burkard , William D. Coggio , Klaus Hintzer , Bernhard Hirsch , Robert E. Kolb , Albert Killich , Gernot Loehr
IPC分类号： C08K5/00 , C08F6/16 , C08F6/22 , C08F14/18 , C08K5/14 , C08L27/12 , C08L27/18 , C09D127/18 , C08F114/18
CPC分类号： C09D127/18 , C08F6/16 , C08F6/22 , C08F14/18 , C08K5/14 , C08L27/12 , C08L27/18 , C08L2205/02 , C09D127/12 , C08F2/16 , C08L2666/04 , C08F2/22
摘要： High purity fluoropolymers are obtained by the emulsion polymerization process, removing essentially all ions and coagulating the polymer essentially without adding ions. These polymers are useful in the field of electronic devices.
摘要翻译：通过乳液聚合方法获得高纯度含氟聚合物，基本上除去所有离子并基本上凝结聚合物而不添加离子。这些聚合物在电子设备领域是有用的。

9. 发明授权

US06794457B2 Fluoropolymer curing system containing a nitrogen cure site monomer 有权
标题翻译：含有氮固化点单体的含氟聚合物固化体系
公开(公告)号：US06794457B2
公开(公告)日：2004-09-21
申请号：US10136020
申请日：2002-04-29
申请人： Werner M. A. Grootaert , Robert E. Kolb , Klaus Hintzer
发明人： Werner M. A. Grootaert , Robert E. Kolb , Klaus Hintzer
IPC分类号： C08F832
CPC分类号： C08K5/19 , C08L27/18 , C08L2205/02 , C08L27/12 , C08L2666/04
摘要： A composition comprising a fluoropolymer comprising interpolymerized units derived from a nitrogen-containing cure site monomer; and a catalyst composition comprising a compound having the general formula: wherein the group HA is an acid, and each R1, R2, and R3 is, independently, the same or a different C1-C20 alkyl group, a C3-C20 cyclic or heterocyclic group, Rf(CH2)x—wherein Rf is a C1-C8 linear or branched and at least partially fluorinated alkylene, cycloalkylene, or oxyalkylene, and x is 1 to 4, or a bond to another R group such that the nitrogen is bonded to or part of an imino or heterocyclic group; wherein two or more R groups may be linked to form a cyclic, bicyclic or aromatic group, optionally comprising a heteroatom. Also provided are a method of making a fluoropolymer composition and articles prepared from the compositions.
摘要翻译：一种组合物，其包含含有源自含氮固化位点单体的共聚单元的含氟聚合物; 和包含具有以下通式的化合物的催化剂组合物：其中基团HA是酸，并且每个R 1，R 2和R 3独立地是相同或不同的C 1 -C 20烷基，C 3 -C 20环状或杂环基团，Rf（CH 2）x - ，其中R f是C 1 -C 8直链或支链和至少部分氟化的亚烷基，亚环烷基或氧化烯，x是1至4，或与另一个R基团的键，使得氮键合至或部分亚氨基或杂环基团; 其中两个或更多个R基团可以连接形成环状，双环或芳族基团，任选地包含杂原子。还提供了制备含氟聚合物组合物和由组合物制备的制品的方法。

10. 发明授权

US09023977B2 Triazine containing fluoropolyether elastomers having very low glass transition temperatures, compositions containing them and methods of making them 有权
标题翻译：含有玻璃化转变温度非常低的含氟聚醚弹性体的三嗪，含有它们的组合物及其制备方法
公开(公告)号：US09023977B2
公开(公告)日：2015-05-05
申请号：US13500526
申请日：2010-10-05
申请人： Steven G. Corveleyn , Rudolf J. Dams , Werner M. A. Grootaert , Gregg D. Dahlke , Miguel A. Guerra
发明人： Steven G. Corveleyn , Rudolf J. Dams , Werner M. A. Grootaert , Gregg D. Dahlke , Miguel A. Guerra
IPC分类号： C08G65/00
CPC分类号： C08G65/007
摘要： A method of making a fluoropolyether elastomer containing triazine groups and having a glass transition temperature of less than −40° C., including providing (i) one or more saturated fluoropolyethers containing repeating moieties selected from (—C4F8O—), (—C3F6O—), (—C2F4O—), (—CF2O—) and combinations thereof and further containing at least one functional group at a terminal carbon atom of the backbone chain, or of a side chain if present, wherein the terminal carbon atom may be a primary or secondary carbon atom and wherein the functional group is capable of reacting with a functional group of the fluorinated compound according to (ii) below to form a triazine ring, (ii) one or more fluorinated compound containing at least one perfluorinated alkyl or perfluorinated alkylene moiety wherein the carbon atoms of the perfluorinated alkyl or alkylene moiety may be interrupted by one or more oxygen atoms and wherein the fluorinated compound further contains at least one functional group capable of reacting with the functional group of the one or more fluoropolyethers to form a triazine; curing the components according to (i) and (ii) to form triazines. Further provided are cured compositions, articles comprising the cured compositions and methods of making articles.
摘要翻译：包括制备含有三嗪基并具有小于-40℃的玻璃化转变温度的氟聚醚弹性体的方法，包括提供（i）一种或多种含有重复部分的饱和含氟聚醚，所述重复部分选自（-C 4 F 8 O - ），（-C 3 F 6 O- ），（-C 2 F 4 O-），（-CF 2 O-）及其组合，并且在主链的末端碳原子或侧链（如果存在）中还含有至少一个官能团，其中末端碳原子可以是伯或仲碳原子，其中所述官能团能够与根据下述（ii）的氟化化合物的官能团反应以形成三嗪环，（ii）一种或多种含有至少一种全氟化烷基或全氟化的含氟化合物亚烷基部分，其中全氟烷基或亚烷基部分的碳原子可被一个或多个氧原子间隔，并且其中所述氟化化合物还含有至少一个f 能够与一种或多种含氟聚醚的官能团反应以形成三嗪的官能团; 根据（i）和（ii）固化组分以形成三嗪。还提供了固化组合物，包含固化组合物的制品和制造制品的方法。

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