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1. 发明申请

US20110275826A1 CHIRAL LIGANDS 审中-公开
公开(公告)号：US20110275826A1
公开(公告)日：2011-11-10
申请号：US13141379
申请日：2009-12-22
申请人： Andreas Pfaltz , Marcus Georg Schrems , Benoît Pugin
发明人： Andreas Pfaltz , Marcus Georg Schrems , Benoît Pugin
IPC分类号： C07F15/00 , C07F7/18 , C07F9/653
CPC分类号： C07F9/653 , C07B53/00 , C07F15/0033
摘要： Chiral compounds of the formula (1), which are optically pure or highly optically enriched in which R0 is C1-C12-alkyl which is unsubstituted or substituted by 1 to 2 C1-C4-alkoxy; cyclo-pentyl or cyclohexyl, which is unsubstituted or substituted by 1 to 3 C1-C4-alkyl or C1-C4-alkoxy; or benzyl, phenyl or naphtyl which is unsubstituted or substituted by 1 to 3 C1-C4-alkyl, C1-C4-alkoxy, C1-C4-fluoroalkyl or C1-C4-fluoroalkoxy, F or Cl, or R0 is —CR5R6OH or —CR5R6OSi(C1-C8-alkyl)3 wherein R5 and R6 are independently selected from the group consisting of H, unsubstituted C1-C12 alkyl, substituted C1-C12 alkyl, unsubstituted C4-C8 cyclo alkyl, substituted C4-C8 cyclo alkyl, unsubstituted aryl, substituted aryl or wherein R5 and R6 can form an unsubstituted 5-6 membered aliphatic carbocycle or a substituted 5-6 membered aliphatic carbocycle, each of R1 and R′1 independently is hydrogen or has the meaning of R0 whereby R1, R′1 and R0 can be same or different, R2 and R3 are independently a C-bonded hydrocarbon radical or a heterohydrocarbon radical, and each of both R4 is C1-C6-alkyl, cyclopentyl, cyclohexyl, phenyl, methylphenyl, methylbenzyl or benzyl, or both R4 together form an aliphatic C4-C6 carbocycle. Metal complexes of these ligands are homogeneous catalysts for asymmetric addition reaction, particularly hydrogenations.
摘要翻译：式（1）的手性化合物，其是光学纯的或高度光学富集的，其中R 0是未被取代或被1至2个C 1 -C 4 - 烷氧基取代的C 1 -C 12 - 烷基; 环戊基或环己基，其是未取代的或被1至3个C 1 -C 4 - 烷基或C 1 -C 4 - 烷氧基取代; 或未被取代或被1至3个C 1 -C 4 - 烷基，C 1 -C 4 - 烷氧基，C 1 -C 4 - 氟代烷基或C 1 -C 4 - 氟烷氧基，F或Cl或R 10表示的苄基，苯基或萘基是-CR 5 R 6 OH或 - CR5R6OSi（C1-C8-烷基）3，其中R5和R6独立地选自H，未取代的C1-C12烷基，取代的C1-C12烷基，未取代的C4-C8环烷基，取代的C4-C8环烷基，未取代的芳基，取代的芳基或其中R5和R6可以形成未取代的5-6元脂族碳环或取代的5-6元脂族碳环，R 1和R'1各自独立地是氢或具有R 0的含义，其中R 1，R' 1和R 0可以相同或不同，R2和R3独立地是C键合的烃基或杂烃基，并且R 2各自为C 1 -C 6 - 烷基，环戊基，环己基，苯基，甲基苯基，甲基苄基或苄基，或 R4一起形成脂族C 4 -C 6碳环。这些配体的金属络合物是用于不对称加成反应，特别是氢化的均相催化剂。

2. 发明申请

US20120101306A1 PROCESS FOR THE PREPARATION OF 1-METHYLCYCLOPENTANE DERIVATIVES 审中-公开
标题翻译：制备1-甲基环戊烷衍生物的方法
公开(公告)号：US20120101306A1
公开(公告)日：2012-04-26
申请号：US13278688
申请日：2011-10-21
申请人： Andreas LANVER , Klaus Ebel , Rainer Klopsch , Werner Bertleff , Richard Dehn , Joaquim Henrique Teles , Helmut Kronemayer , Marcus Georg Schrems
发明人： Andreas LANVER , Klaus Ebel , Rainer Klopsch , Werner Bertleff , Richard Dehn , Joaquim Henrique Teles , Helmut Kronemayer , Marcus Georg Schrems
IPC分类号： C07C41/14 , C07C1/20 , C07C5/29 , C07C29/04
CPC分类号： C07C1/20 , C07C5/29 , C07C29/04 , C07C41/06 , C07C2601/10 , Y02P20/127 , C07C13/12 , C07C35/06 , C07C43/184
摘要： Process for the preparation of 1-methylcyclopentene by thermal reaction of cyclohexanol or cyclohexene or mixtures of both compounds to give 1-methylcyclopentene, wherein the resulting by-products 3-methylcyclopentene and 4-methylcyclopentene (double-bond isomers of 1-methylcyclopentene) are returned to the reaction.
摘要翻译：通过环己醇或环己烯或两种化合物的混合物的热反应制备1-甲基环戊烯得到1-甲基环戊烯的方法，其中得到的副产物3-甲基环戊烯和4-甲基环戊烯（1-甲基环戊烯的双键异构体）是回到了反应。

3. 发明申请

US20130040801A1 PROCESS FOR PREPARING HIGH-PURITY ALUMINUM OXIDE BY PURIFICATION OF ALUMINA 有权
标题翻译：通过氧化铝制备高纯度氧化铝的方法
公开(公告)号：US20130040801A1
公开(公告)日：2013-02-14
申请号：US13413278
申请日：2012-03-06
申请人： Marcus Georg Schrems , Anna Katharina Dürr , Günther Huber , Jesus Enrique Zerpa Unda , Katrin Freitag , Christian Eichholz , Franky Ruslim
发明人： Marcus Georg Schrems , Anna Katharina Dürr , Günther Huber , Jesus Enrique Zerpa Unda , Katrin Freitag , Christian Eichholz , Franky Ruslim
IPC分类号： C04B35/10 , C01F7/46
CPC分类号： C01F7/46 , C01P2006/80 , C04B35/10 , C04B35/62655 , C04B35/632 , C04B35/63444 , C04B2235/3201 , C04B2235/72 , C04B2235/721 , C04B2235/722 , C04B2235/94
摘要： A process for preparing aluminum oxide with a low calcium content, in which(1) crude alpha- and/or gamma-aluminum oxide with a total calcium content in the range from 50 to 2000 ppm, based on the crude alpha- and/or gamma-aluminum oxide, is mixed with an aqueous solution or suspension comprising the compounds selected from the group of inorganic acid, organic acid and complexing agent, (2) the mixture from step (1) is admixed with a flocculating aid, (3) in the mixture of step (2), the solids are separated from the liquid, (4) the solids separated are mixed with water in the presence or in the absence of a flocculating aid, (5) in the mixture of step (4), the solids are separated from the liquid, (6) optionally, steps (4) and (5) are repeated once or more than once, (7) optionally, the solids separated optionally after addition of further compounds, are dried.
摘要翻译：一种制备具有低钙含量的氧化铝的方法，其中（1）基于粗α和/或α的总钙含量在50至2000ppm范围内的粗α和/或γ-氧化铝将γ-氧化铝与包含选自无机酸，有机酸和络合剂的化合物的水溶液或悬浮液混合，（2）将来自步骤（1）的混合物与絮凝助剂混合，（3）在步骤（2）的混合物中，固体与液体分离，（4）在存在或不存在絮凝助剂的情况下将分离的固体与水混合，（5）在步骤（4）的混合物中，，固体与液体分离，（6）任选地，步骤（4）和（5）重复一次或多于一次，（7）任选地，任选地，在加入其它化合物之后分离的固体被干燥。

4. 发明申请

US20120101307A1 PROCESS FOR THE PREPARATION OF 1-METHYL-1-ALKOXYCYCLOPENTANES 审中-公开
标题翻译：制备1-甲基-1-烷氧基环戊二烯的方法
公开(公告)号：US20120101307A1
公开(公告)日：2012-04-26
申请号：US13279915
申请日：2011-10-24
申请人： Andreas LANVER , Klaus Ebel , Rainer Klopsch , Werner Bertleff , Richard Dehn , Joaquim Henrique Teles , Helmut Kronemayer , Marcus Georg Schrems
发明人： Andreas LANVER , Klaus Ebel , Rainer Klopsch , Werner Bertleff , Richard Dehn , Joaquim Henrique Teles , Helmut Kronemayer , Marcus Georg Schrems
IPC分类号： C07C41/01
CPC分类号： C07C41/06 , C07C5/29 , C07C2521/08 , C07C2601/08 , C07C2601/10 , Y02P20/127 , C07C43/184 , C07C13/12
摘要： Process for the preparation of cyclopentane derivatives of the formula I in which R is a C1- to C10-alkyl group, which comprises reacting cyclohexanol or cyclohexene or mixtures of both compounds to give 1-methyl-1-cyclopentene (1st stage) and subsequently adding a C1- to C10-alkanol onto the double bond of the 1-methyl-1-cyclopentene (2nd stage).
摘要翻译：制备式Ⅰ的环戊烷衍生物的方法，其中R为C1-至C10烷基，其包括使环己醇或环己烯或两种化合物的混合物反应得到1-甲基-1-环戊烯（第一阶段），随后在1-甲基-1-环戊烯的双键中加入C 1〜C 10链烷醇（第2阶段）。

5. 发明授权

US08524191B2 Process for preparing high-purity aluminum oxide by purification of alumina 有权
标题翻译：通过纯化氧化铝制备高纯度氧化铝的方法
公开(公告)号：US08524191B2
公开(公告)日：2013-09-03
申请号：US13413278
申请日：2012-03-06
申请人： Marcus Georg Schrems , Anna Katharina Dürr , Günther Huber , Jesus Enrique Zerpa Unda , Katrin Freitag , Christian Eichholz , Franky Ruslim
发明人： Marcus Georg Schrems , Anna Katharina Dürr , Günther Huber , Jesus Enrique Zerpa Unda , Katrin Freitag , Christian Eichholz , Franky Ruslim
IPC分类号： C01F7/00
CPC分类号： C01F7/46 , C01P2006/80 , C04B35/10 , C04B35/62655 , C04B35/632 , C04B35/63444 , C04B2235/3201 , C04B2235/72 , C04B2235/721 , C04B2235/722 , C04B2235/94
摘要： A process for preparing aluminum oxide with a low calcium content, in which (1) crude alpha- and/or gamma-aluminum oxide with a total calcium content in the range from 50 to 2000 ppm, based on the crude alpha- and/or gamma-aluminum oxide, is mixed with an aqueous solution or suspension comprising the compounds selected from the group of inorganic acid, organic acid and complexing agent, (2) the mixture from step (1) is admixed with a flocculating aid, (3) in the mixture of step (2), the solids are separated from the liquid, (4) the solids separated are mixed with water in the presence or in the absence of a flocculating aid, (5) in the mixture of step (4), the solids are separated from the liquid, (6) optionally, steps (4) and (5) are repeated once or more than once, (7) optionally, the solids separated optionally after addition of further compounds, are dried.
摘要翻译：一种制备具有低钙含量的氧化铝的方法，其中（1）基于粗α和/或α的总钙含量在50至2000ppm范围内的粗α和/或γ-氧化铝将γ-氧化铝与包含选自无机酸，有机酸和络合剂的化合物的水溶液或悬浮液混合，（2）将来自步骤（1）的混合物与絮凝助剂混合，（3）在步骤（2）的混合物中，固体与液体分离，（4）在存在或不存在絮凝助剂的情况下将分离的固体与水混合，（5）在步骤（4）的混合物中，，固体与液体分离，（6）任选地，步骤（4）和（5）重复一次或多于一次，（7）任选地，任选地，在加入其它化合物之后分离的固体被干燥。

6. 发明申请

US20130040799A1 PROCESS FOR PREPARING HIGH-PURITY MAGNESIUM HYDROXIDE AND MAGNESIUM OXIDE 审中-公开
标题翻译：制备高纯度氢氧化镁和氧化镁的方法
公开(公告)号：US20130040799A1
公开(公告)日：2013-02-14
申请号：US13413259
申请日：2012-03-06
申请人： Marcus Georg Schrems , Anna Katharina Dürr , Günther Huber , Jesus Enrique Zerpa Unda , Katrin Freitag , Michael Karcher , Axel Salden
发明人： Marcus Georg Schrems , Anna Katharina Dürr , Günther Huber , Jesus Enrique Zerpa Unda , Katrin Freitag , Michael Karcher , Axel Salden
IPC分类号： C01F5/14 , C04B35/04 , C01F5/22
CPC分类号： C01F5/22 , C01F5/20 , C01F5/24 , C04B35/04 , C04B35/62675 , C04B2235/3206 , C04B2235/3217 , C04B2235/725 , C04B2235/94
摘要： A process for preparing magnesium compounds by precipitation, in which an aqueous solution or suspension of a magnesium compound is mixed with a precipitant and the corresponding magnesium compound is precipitated wherein the aqueous solution or suspension of a magnesium compound is obtained by reaction of an organomagnesium compound with an aldehyde or a ketone or another electrophile and subsequent aqueous workup of the reaction mixture at a pH of at most 10 or from a magnesium salt with a maximum calcium content and/or potassium content of 200 ppm, based on the magnesium salt used.
摘要翻译：通过沉淀制备镁化合物的方法，其中将镁化合物的水溶液或悬浮液与沉淀剂混合，并且沉淀出相应的镁化合物，其中镁化合物的水溶液或悬浮液通过有机镁化合物与醛或酮或另外的亲电子试剂反应，随后在pH最高为10的情况下反应混合物的水处理，或以所使用的镁盐为最高钙含量和/或钾含量为200ppm的镁盐。

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