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1. 发明授权

US4642304A Activated carbon and process for its production 失效
标题翻译：活性炭及其生产工艺
公开(公告)号：US4642304A
公开(公告)日：1987-02-10
申请号：US845246
申请日：1986-03-28
申请人： Alfons Karl , Erwin Walter , Peter Kleinschmit , Hermann Gottschlich , Roland Kutz , Detley Koth
发明人： Alfons Karl , Erwin Walter , Peter Kleinschmit , Hermann Gottschlich , Roland Kutz , Detley Koth
IPC分类号： C01B31/08 , C01B31/10 , C01B31/12 , B01J20/20
CPC分类号： C01B31/10
摘要： Activated carbon is produced from lignite coke. It is characterized by the product of the molasses number times the iodine number divided by 1000 being 350 to 1000 and/or the product of the molasses number times the methylene blue number divided by 10 being 500 to 1200. It is produced by adding aqueous alkali or alkaline earth carbonate solution and/or aqueous alkali or alkaline earth hydroxide solution by means of lance during the steam activation of lignite coke in a rotating tube.
摘要翻译：活性炭由褐煤焦炭生产。其特征在于，糖蜜数乘以1000的摩尔数乘以350至1000，和/或糖蜜数乘以10的分数乘以500至1200的产物。它是通过加入碱水溶液或碱土金属碳酸盐溶液和/或碱金属或碱土金属氢氧化物水溶液，在旋转管中的褐煤焦炭的蒸汽活化期间通过喷枪。

2. 发明授权

US4603119A Process for production of activated carbon from lignite coke 失效
标题翻译：从褐煤焦炭生产活性炭的方法
公开(公告)号：US4603119A
公开(公告)日：1986-07-29
申请号：US732407
申请日：1985-05-09
申请人： Alfons Karl , Erwin Walter , Peter Kleinschmit , Hermann Gottschlich , Roland Kutz , Detlev Koth
发明人： Alfons Karl , Erwin Walter , Peter Kleinschmit , Hermann Gottschlich , Roland Kutz , Detlev Koth
IPC分类号： C01B31/08 , C01B31/10 , C01B31/12 , B01J20/20
CPC分类号： C01B31/10
摘要： Activated carbon is produced from lignite coke. It is characterized by the product of the molasses number times the iodine number divided by 1000 being 350 to 1000 and/or the product of the molasses number times the methylene blue number divided by 10 being 500 to 1200. It is produced by adding aqueous alkali or alkaline earth carbonate solution and/or aqueous alkali or alkaline earth hydroxide solution by means of lance during the steam activation of lignite coke in a rotating tube.
摘要翻译：活性炭由褐煤焦炭生产。其特征在于，糖蜜数乘以1000的摩尔数乘以350至1000，和/或糖蜜数乘以10的分数乘以500至1200的产物。它是通过加入碱水溶液或碱土金属碳酸盐溶液和/或碱金属或碱土金属氢氧化物水溶液，在旋转管中的褐煤焦炭的蒸汽活化期间通过喷枪。

3. 发明授权

US4362885A Process for the manufacture of (iodoorganyl)alkoxysilanes 失效
标题翻译：（碘代有机基）烷氧基硅烷的制备方法
公开(公告)号：US4362885A
公开(公告)日：1982-12-07
申请号：US330355
申请日：1981-12-14
申请人： Peter Panster , Alfons Karl , Wolfgang Buder , Peter Kleinschmit
发明人： Peter Panster , Alfons Karl , Wolfgang Buder , Peter Kleinschmit
IPC分类号： C07F7/18 , C07F7/08
CPC分类号： C07F7/1888
摘要： The subject of the invention is a process for the manufacture of (iodoorganyl)alkoxysilanes of the general formula: ##STR1## in which R.sup.1 is an alkylene group, R.sup.2 is an alkoxy group and R.sup.3 and R.sup.4 an alkoxy group and/or an alkyl or aryl group, whereby the chlorine or bromine compound corresponding to that of formula (1) is caused to react with stoichiometric to double molar quantities of an inorganic iodine donor in the presence of 0.01-5 mol % of an organic substituted onium salt of nitrogen, phosphorus, arsenic or antimony or an organic substituted sulfonium salt or a crown ether as catalyst, in certain solubilizing agents.
摘要翻译：本发明的主题是制备通式如下的（碘代有机基）烷氧基硅烷的方法：其中R1是亚烷基，R2是烷氧基，R3和R4是烷氧基和/或烷基或芳基，其中使与对应于式（1）的氯或溴化合物在0.01-5mol％的有机取代鎓盐的存在下与化学计量比与双摩尔量的无机碘供体反应的氮，磷，砷或锑或有机取代的锍盐或冠醚作为催化剂，在某些增溶剂中。

4. 发明授权

US4390712A Aqueous solution of cationic organosilicon compounds and process for the production of the solutions 失效
标题翻译：阳离子有机硅化合物的水溶液及其制备方法
公开(公告)号：US4390712A
公开(公告)日：1983-06-28
申请号：US298251
申请日：1981-08-31
申请人： Alfons Karl , Wolfgang Buder , Peter Kleinschmit
发明人： Alfons Karl , Wolfgang Buder , Peter Kleinschmit
IPC分类号： B03D1/01 , C07F7/18 , C07F7/10
CPC分类号： C07F7/1892 , B03D1/0046 , B03D1/01
摘要： There are prepared aqueous solutions of cationic organosilicon compounds which are produced by reacting an alkoxysilylalkyl halide of the formula (RO).sub.3-n R.sub.n.sup.1 --Si--R.sup.2 --X (I) where R is C.sub.1 to C.sub.5 alkyl, methoxy, ethoxy, phenyl, or C.sub.5 to C.sub.8 cycloalkyl; R.sup.1 is C.sub.1 to C.sub.5 alkyl, phenyl, tolyl, benzyl, or C.sub.5 to C.sub.8 cycloalkyl; R.sup.2 is a divalent ethylenic double bond free hydrocarbon group having 3 to 8 carbon atoms, n is zero, 1 or 2 and X is chlorine, bromine, or iodine with a tertiary amine of the formula R.sup.3 NR.sup.4 R.sup.5 (II) where R.sup.3, R.sup.4, and R.sup.5 are the same or different and each is an alkyl group or benzyl in which the number of carbon atoms of the alkyl group or the alkyl groups together is up to 30 or R.sup.4 and .sup.5 together with the nitrogen atom, as well as in a given case a further hetero atom selected from the group consisting of oxygen, nitrogen, and sulfur is a univalent five to eight membered heterocyclic ring having three to seven --CH.sub.2 -- groups in the heterocyclic ring, or R.sup.5 is a C.sub.3 to C.sub.12 cycloalkyl group in aqueous medium at a temperature from room temperature (e.g. about 20.degree. C.) to 300.degree. C. at a mole ratio of (I) to (II) between 1:0.8 to 1:1,2 and in a given case under pressure.
摘要翻译：制备阳离子有机硅化合物的水溶液，其通过使式（RO）3-nRn1-Si-R2-X（I）的烷氧基甲硅烷基烷基卤化物反应制备，其中R是C1至C5烷基，甲氧基，乙氧基，苯基或 C5至C8环烷基; R 1是C 1至C 5烷基，苯基，甲苯基，苄基或C 5至C 8环烷基; R2是具有3-8个碳原子的二价烯键式双键无键烃基，n为0,1或2，X为氯，溴或碘，与式R3NR4R5（Ⅱ）的叔胺反应，其中R3，R4和 R5相同或不同，并且各自为烷基或苄基，其中烷基或烷基的碳原子数一起为至多30或R4和5以及氮原子以及在给定的在另一个选自氧，氮和硫的杂原子的情况下，杂环中具有三至七个-CH 2 - 基的一价五元至八元杂环，或者R5是水性中的C3至C12环烷基介质在室温（例如约20℃）至300℃的温度下以（I）至（II）的摩尔比为1:0.8至1:1.2，在给定情况下在压力下。

5. 发明授权

US08003069B2 Carbon black, method for the production of carbon black or other flame aerosols, and device for carrying out said method 有权
标题翻译：炭黑，炭黑或其他火焰气溶胶的生产方法，以及用于实施所述方法的装置
公开(公告)号：US08003069B2
公开(公告)日：2011-08-23
申请号：US12813192
申请日：2010-06-10
申请人： Ulrich Riebel , Matthias Katzer , Kai Krauss , Alfons Karl , Juergen Behnisch
发明人： Ulrich Riebel , Matthias Katzer , Kai Krauss , Alfons Karl , Juergen Behnisch
IPC分类号： C01B31/02
CPC分类号： F23D99/00 , C01P2004/04 , C01P2006/19 , C09C1/48 , C09C1/50 , C09C1/52 , F23D2900/21005 , F23D2900/21007
摘要： The invention relates to a method for producing carbon black or other flame aerosols, comprising the following steps: the heat is removed from the flame by dissipation and/or radiation; a thin gas boundary layer is formed; the flow formed by the flame and the gas boundary layer is accelerated or expanded; the obtained aerosol is withdrawn; and the cooling surface is cleaned. The invention further relates to a device for carrying out such a method and a black carbon having a maximum pH value of 6.0, a maximum ignition residue of 0.1 percent, and a maximum 5 μm screening refuse of 200 ppm. The inventive black carbon can be used in rubber, plastic, printing inks, inks, inkjet inks, toners, lacquers, dyes, paper, bitumen, concrete, and other construction materials.
摘要翻译：本发明涉及一种生产炭黑或其他火焰气溶胶的方法，包括以下步骤：通过耗散和/或辐射将热量从火焰中除去; 形成薄的气体边界层; 由火焰和气体边界层形成的流动被加速或扩大; 取出所得气溶胶; 并清洁冷却表面。本发明还涉及一种用于实施这种方法的设备和最大pH值为6.0，最大点火残留量为0.1％，最大5μm筛选垃圾为200ppm的黑碳。本发明的黑碳可用于橡胶，塑料，印刷油墨，油墨，喷墨油墨，调色剂，油漆，染料，纸，沥青，混凝土和其他建筑材料。

6. 发明申请

US20100248120A1 CARBON BLACK, METHOD FOR THE PRODUCTION OF CARBON BLACK OR OTHER FLAME AEROSOLS, AND DEVICE FOR CARRYING OUT SAID METHOD 有权
标题翻译：碳黑，碳黑或其他火焰气溶胶的生产方法，以及实施方法的装置
公开(公告)号：US20100248120A1
公开(公告)日：2010-09-30
申请号：US12813192
申请日：2010-06-10
申请人： Ulrich RIEBEL , Matthias Katzer , Kai Krauss , Alfons Karl , Jürgen Behnisch
发明人： Ulrich RIEBEL , Matthias Katzer , Kai Krauss , Alfons Karl , Jürgen Behnisch
IPC分类号： G03G9/08 , C01B31/02 , C09C1/00 , C09D11/02 , C04B14/00 , C09D1/00
CPC分类号： F23D99/00 , C01P2004/04 , C01P2006/19 , C09C1/48 , C09C1/50 , C09C1/52 , F23D2900/21005 , F23D2900/21007
摘要： The invention relates to a method for producing carbon black or other flame aerosols, comprising the following steps: the heat is removed from the flame by dissipation and/or radiation; a thin gas boundary layer is formed; the flow formed by the flame and the gas boundary layer is accelerated or expanded; the obtained aerosol is withdrawn; and the cooling surface is cleaned. The invention further relates to a device for carrying out such a method and a black carbon having a maximum pH value of 6.0, a maximum ignition residue of 0.1 percent, and a maximum 5 μm screening refuse of 200 ppm. The inventive black carbon can be used in rubber, plastic, printing inks, inks, inkjet inks, toners, lacquers, dyes, paper, bitumen, concrete, and other construction materials.
摘要翻译：本发明涉及一种生产炭黑或其他火焰气溶胶的方法，包括以下步骤：通过耗散和/或辐射将热量从火焰中除去; 形成薄的气体边界层; 由火焰和气体边界层形成的流动被加速或扩大; 取出所得气溶胶; 并清洁冷却表面。本发明还涉及一种用于实施这种方法的设备和最大pH值为6.0，最大点火残留量为0.1％，最大5μm筛选垃圾为200ppm的黑碳。本发明的黑碳可用于橡胶，塑料，印刷油墨，油墨，喷墨油墨，调色剂，油漆，染料，纸，沥青，混凝土和其他建筑材料。

7. 发明授权

US5859120A Carbon black and processes for manufacturing 失效
标题翻译：炭黑和制造工艺
公开(公告)号：US5859120A
公开(公告)日：1999-01-12
申请号：US824246
申请日：1997-03-25
申请人： Alfons Karl , Burkhard Freund , Karl Vogel
发明人： Alfons Karl , Burkhard Freund , Karl Vogel
IPC分类号： B60C1/00 , B60C11/00 , C08K3/04 , C08K9/02 , C08L21/00 , C09C1/50 , C08K9/06 , C09C1/44
CPC分类号： C09C1/50 , C08K3/04 , C08K9/02 , C01P2004/80 , C01P2006/12 , C01P2006/19
摘要： Carbon blacks containing silicon and a process for manufacturing them. The carbon blacks containing silicon are suitable as reinforcing carbon blacks for rubber mixtures and give the latter viscoelastic properties such as reduced rolling resistance in tires. At the same time, the wet traction is even improved in the process.
摘要翻译：含硅的炭黑及其制造方法。含硅的炭黑适合用作橡胶混合物的增强炭黑，并赋予后者粘弹性，如轮胎中的滚动阻力降低。同时，在这个过程中，湿牵引力甚至有所改善。

8. 发明授权

US4401598A Production of organosilicon compounds having azido groups 失效
标题翻译：生产具有叠氮基的有机硅化合物
公开(公告)号：US4401598A
公开(公告)日：1983-08-30
申请号：US312979
申请日：1981-10-20
申请人： Alfons Karl , Wolfgang Buder
发明人： Alfons Karl , Wolfgang Buder
IPC分类号： G01F23/00 , G01F23/24 , C07C117/00
CPC分类号： G01F23/245 , G01F23/0023
摘要： There are prepared azido groups containing organosilicon compounds of the formula ##EQU1## where R is a divalent hydrocarbon group having 1 to 8 carbon atoms which is free from ethylenically unsaturated bonds and whose carbon chain in a given case, is interrupted once by --O--, --S--, or --NR.sup.3 where R.sup.3 is hydrogen, methyl, ethyl, or phenyl,R.sup.1 is a univalent alkyl group having 1 to 3 carbon atoms, phenyl, benzyl, or tolyl,R.sup.2 is an alkyl group having 1 to 4 carbon atoms, phenyl, benzyl, or an alkoxyalkyl group having a total of up to four carbon atoms,m is zero, 1, 2, or 3, andn is zero, 1 or 2 whereby m
摘要翻译：制备含有式（I）的有机硅化合物的叠氮基，其中R是不含烯属不饱和键的碳原子数为1至8的二价烃基，并且在给定情况下碳链被中断一次-O - ， - S-或-NR 3，其中R 3是氢，甲基，乙基或苯基，R 1是具有1至3个碳原子的一价烷基，苯基，苄基或甲苯基，R 2是具有1至4个碳原子，苯基，苄基或总数最多为4个碳原子的烷氧基烷基，m为0,1,2或3，n为0,1或2，由此m <3-n，通过使式XR-SiRn1（OR2）3-n，II的卤代硅烷，其中X是氯或溴，其他符号如上所定义，其中M是锂，钠，钾或铵的式MN3 III的叠氮化物由此，在给出的情况下，使用相转移催化剂，由此进行水解或部分水解。或者，可以首先进行水解或部分水解，其中首先进行一个或多个烷氧基甲硅烷基-OR 2的水解，随后进行与叠氮化物的反应。有机硅化合物是有价值的中间体，也可用作制备二氧化硅增强橡胶的偶联剂。

9. 发明申请

US20130015175A1 METHOD FOR PRODUCING SILICON 审中-公开
标题翻译：生产硅的方法
公开(公告)号：US20130015175A1
公开(公告)日：2013-01-17
申请号：US13509838
申请日：2010-11-04
申请人： Alfons Karl , Jürgen Erwin Lang , Hartwig Rauleder , Bodo Frings
发明人： Alfons Karl , Jürgen Erwin Lang , Hartwig Rauleder , Bodo Frings
IPC分类号： H01B1/04 , F27D11/00
CPC分类号： C01B33/025 , C01B32/05
摘要： The present invention relates to an improved process for producing silicon, preferably solar silicon, using novel high-purity graphite mouldings, especially graphite electrodes, and to an industrial process for production of the novel graphite mouldings.
摘要翻译：本发明涉及使用新型高纯度石墨模制品，特别是石墨电极，以及用于生产新型石墨模制品的工业方法来生产硅，优选太阳能硅的改进方法。

10. 发明申请

US20110262336A1 PRODUCTION OF SOLAR-GRADE SILICON FROM SILICON DIOXIDE 审中-公开
标题翻译：从二氧化硅生产太阳能级硅
公开(公告)号：US20110262336A1
公开(公告)日：2011-10-27
申请号：US13121761
申请日：2009-09-28
申请人： Hartwig Rauleder , Ekkehard Mueh , Mustafa Siray , Peter Nagler , Bodo Frings , Ingrid Lunt-Rieg , Alfons Karl , Christian Panz , Thomas Groth , Guido Stochniol , Matthias Rochnia , Juergen Erwin Lang , Oliver Wolf , Rudolf Schmitz , Bernd Nowitzki , Dietmar Wewers
发明人： Hartwig Rauleder , Ekkehard Mueh , Mustafa Siray , Peter Nagler , Bodo Frings , Ingrid Lunt-Rieg , Alfons Karl , Christian Panz , Thomas Groth , Guido Stochniol , Matthias Rochnia , Juergen Erwin Lang , Oliver Wolf , Rudolf Schmitz , Bernd Nowitzki , Dietmar Wewers
IPC分类号： C01B31/36 , B01J19/32 , B01J19/00 , C01B33/025 , C01B33/02
CPC分类号： C01B33/025 , C01B32/05 , C01B32/956
摘要： The invention relates to a complete method for producing pure silicon that is suitable for use as solar-grade silicon, comprising the reduction of a silicon oxide, purified by acidic precipitation from an aqueous solution of a silicon oxide dissolved in an aqueous phase, using one or more pure carbon sources, the purified silicon oxide being obtained, in particular, by the precipitation of a silicon oxide dissolved in an aqueous phase in an acidifier. The invention also relates to a formulation containing an activator and to a device for producing silicon, a reactor and electrodes.
摘要翻译：本发明涉及一种适用于太阳能级硅的纯硅生产的完整方法，其中包括通过酸性沉淀从溶解在水相中的氧化硅水溶液中纯化的氧化硅，使用一种或更多的纯碳源，纯化的氧化硅，特别是通过在酸化器中沉淀溶解在水相中的氧化硅。本发明还涉及含有活化剂和用于生产硅，反应器和电极的装置的制剂。

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