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1. 发明授权

US4713469A Fluorine-containing multifunctional ester compound 失效
标题翻译：含氟多官能酯化合物
公开(公告)号：US4713469A
公开(公告)日：1987-12-15
申请号：US845106
申请日：1986-03-27
申请人： Yoshio Takeuchi , Toru Koizumi , Kozo Hori
发明人： Yoshio Takeuchi , Toru Koizumi , Kozo Hori
IPC分类号： C07C69/14 , C07C117/00
CPC分类号： C07C247/00 , C07C321/00 , C07C323/00
摘要： A fluorine-containing multifunctional ester compound represented by the formula ##STR1## wherein A is halogen atom, NO.sub.2 or N.sub.3, B is halogen atom or SR.sup.2, R.sup.1 is lower aliphatic group, aromatic group or aralkyl, R.sup.2 is lower aliphatic group or aromatic group.
摘要翻译：由下式表示的含氟多官能酯化合物，其中A为卤原子，NO 2或N 3，B为卤素原子或SR 2，R 1为低级脂族基，芳基或芳烷基，R 2为低级脂族基或芳基。

2. 发明授权

US4474700A .beta.-Substituted polyfluoropropionate salts and derivatives 失效
标题翻译： β-取代的多氟丙酸盐和衍生物
公开(公告)号：US4474700A
公开(公告)日：1984-10-02
申请号：US380016
申请日：1982-05-20
申请人： Carl G. Krespan
发明人： Carl G. Krespan
IPC分类号： C07C69/40 , C07C247/04 , C07C247/12 , C07C305/00 , C07C309/80 , C07C315/04 , C07C317/00 , C07C317/18 , C07C317/44 , C07C319/20 , C07C323/12 , C07C323/52 , C07F9/40 , C07F9/42 , C08F14/18 , C08F16/14 , C08F16/24 , C08F214/18 , C08F216/14 , C08J5/22 , C25B13/08 , C07C117/00 , C07C121/00 , C07C121/38 , C07C121/413
CPC分类号： C07C247/00 , C07C255/00 , C07C317/44 , C07C323/52 , C07F9/4006 , C07F9/42 , C08F216/1416
摘要： .beta.-substituted polyfluoropropionate salts, derivatives and copolymers and processes for the preparation thereof.
摘要翻译： β-取代的聚氟丙酸盐，衍生物和共聚物及其制备方法。

3. 发明授权

US4410519A Tetraline derivatives, their production and pharmaceutical compositions containing them 失效
标题翻译：四氮烯衍生物，它们的生产和包含它们的药物组合物
公开(公告)号：US4410519A
公开(公告)日：1983-10-18
申请号：US243267
申请日：1981-03-12
申请人： Max P. Seiler , Andre Stoll
发明人： Max P. Seiler , Andre Stoll
IPC分类号： C07C255/24 , A61K31/655 , A61K31/275 , C07C117/00 , C07C121/60
CPC分类号： C07C255/24
摘要： An optically active or racemic 2-amino-5-hydroxy-1,2,3,4-tetrahydronaphthalene wherein the nitrogen atom of the amino group carrier two alkyl groups, one of which is unsubstituted and the other is substituted by at least one functional group, or a physiologically hydrolysable ester thereof in free base form or in the form of an acid addition salt thereof is provided which is active against heart circulatory disorders and Morbus Parkinson and inhibits prolactin secretion inhibition.
摘要翻译：光学活性或外消旋的2-氨基-5-羟基-1,2,3,4-四氢化萘，其中氨基的氮原子携带两个烷基，其中一个是未取代的，另一个被至少一个官能提供其对游离碱形式或其酸加成盐形式的生理上可水解的酯，其对心脏循环障碍和莫斯帕金森病具有活性并且抑制催乳素分泌抑制。

4. 发明授权

US4354976A Process for the preparation of azidobenzal compounds 失效
标题翻译：制备叠氮基亚苄基化合物的方法
公开(公告)号：US4354976A
公开(公告)日：1982-10-19
申请号：US218250
申请日：1980-12-19
申请人： Michael Romer
发明人： Michael Romer
IPC分类号： C07C247/16 , C07C67/00 , C07C241/00 , C08K5/22 , C09D115/00 , C07C117/00
CPC分类号： C09D115/00 , C07C247/00 , C08K5/22 , C08C19/10 , Y02P20/55
摘要： A process for preparing a 2,6-bis-[(4-azidophenyl)methylene]-cyclohexanone of the formula ##STR1## wherein R is hydrogen or alkyl of 1-6 C atoms, comprises condensing a cyclohexanone of the formula ##STR2## wherein R is as defined above, with 4-aminobenzaldehyde, the 4-amino group optionally being protected, in the presence of an alkaline condensing agent; removing the protective group when the 4-amino group is protected; diazotizing the resultant 2,6-bis-[(4-aminophenyl)methylene]-cyclohexanone of the formula ##STR3## wherein R is as defined above, and reacting the diazotization product with an alkali metal azide.
摘要翻译：制备式“IMAGE”的2,6-二 - [（4-叠氮基苯基）亚甲基] - 环己酮的方法，其中R是氢或1-6C原子的烷基，包括将下式的环己酮：其中R如上定义，与4-氨基苯甲醛，4-氨基任选被保护，在碱性缩合剂的存在下; 当4-氨基被保护时，去除保护基; 将得到的式（IMAGE）的2,6-二 - [（4-氨基苯基）亚甲基] - 环己酮重氮化，其中R如上定义，并使重氮化产物与碱金属叠氮化物反应。

5. 发明授权

US3939184A Production of carbonyl compounds substituted in .alpha.-position 失效
标题翻译：生成在{60-位取代的羰基化合物
公开(公告)号：US3939184A
公开(公告)日：1976-02-17
申请号：US344632
申请日：1973-03-26
申请人： Horst Koenig , Horst Metzger , Werner Reif
发明人： Horst Koenig , Horst Metzger , Werner Reif
IPC分类号： C07C323/22 , C07C69/66 , C07C117/00 , C07C121/76 , C07C122/00
CPC分类号： C07C45/518 , C07C201/08 , C07C231/10 , C07C231/12 , C07C247/12 , C07C253/04 , C07C253/30 , C07C255/00 , C07C315/00 , C07C319/14 , C07C323/22
摘要： Production of carbonyl compounds substituted in the .alpha.-position and having the formula: ##EQU1## wherein R.sup.1 is alkyl, aralkyl, phenyl, toluyl, naphthyl, alkoxy or amino; R.sup.2 is hydrogen ##EQU2## A is hydrogen, alkyl, halo or ##EQU3## R.sup.6 is hydrogen or methyl, and R.sup.11 is alkyl; wherein said compounds are formed by reacting a sulfur ylide having the formula: ##EQU4## wherein Y is the radical ##EQU5## and R.sup.9 and R.sup.10 are alkyl or phenyl, with a solution containing both an electrophilic agent A' that is converted into the radical A and a nucleophilic agent B' that is converted into the radical B. The resulting carbonyl compounds are useful as starting materials for the production of paper, textile, and leather auxiliaries, plant protection agents, alkyd resins, polyesters and polyamides.
摘要翻译：制备在α-位取代的具有下式的羰基化合物：其中R1是烷基，芳烷基，苯基，甲苯基，萘基，烷氧基或氨基; R2是氢R6R6O R6R6O || PARALLEL || PARALLEL -CH-CH-CN，-C-R1或-CH-CH-C-OR11; A是氢，烷基，卤素或R6R6 | -CH-CH-CN R6是氢或甲基，R11是烷基; 其中所述化合物通过使具有下列结构式的硫叶立德反应形成：其中Y是基团CH 3 R 9 = S ANGLE或= S ANGLE PARALLEL OCH 3 R 10，R 9和R 10是烷基或苯基，与含有转化为自由基A的亲电子试剂A'和转化为自由基B的亲核试剂B'的溶液。得到的羰基化合物可用作生产纸，纺织品和皮革助剂的原料植物保护剂，醇酸树脂，聚酯和聚酰胺。

6. 发明授权

US3770779A Substituted dinitroanilines 失效
标题翻译：取代的DINITROANILINES
公开(公告)号：US3770779A
公开(公告)日：1973-11-06
申请号：US3770779D
申请日：1971-08-09
申请人： BASF AG
发明人： KIEHS K , KOENIG K , FISCHER A
IPC分类号： A01N33/18 , A01P13/02 , C07C271/06 , C07C323/25 , C07C117/00
CPC分类号： C07C323/25 , C07C247/00 , C07C255/00 , C07C271/06
摘要： NEW AND VALUABLE SUBSTITUTED DINITROANILINES HAVING A GOOD HERBICIDAL ACTION AND A PROCESS FOR CONTROLLING THE GROWTH OF UNWANTED PLANTS WITH THESE COMPOUNDS.

7. 发明授权

US3705911A Silyl-azidoformates 失效
标题翻译： SILYL-AZIDOFORMATES
公开(公告)号：US3705911A
公开(公告)日：1972-12-12
申请号：US3705911D
申请日：1971-11-16
申请人： HERCULES INC
发明人： THOMSON J BRENT
IPC分类号： C07F7/10 , C07F7/18 , C08J5/06 , C08J5/08 , C08K9/06 , C09D4/00 , C07C117/00 , C07D109/00
CPC分类号： C08J5/06 , C07F7/10 , C07F7/1836 , C08J5/08 , C08J2383/04 , C08K9/06 , C09D4/00 , C08G77/22
摘要： DISCLOSED ARE NITROGEN CONTAINING SILANE COMPOUNDS OF THE FORMULA

(X)A-SI(-(T)B)-(R-(O-C(=O)-N3)C)D

WHERE R IS AN ORGANIC RADICAL, X IS SELECTED FROM HALO, HYDROXY, ALKOXY, ARYLOXY, ORGANO OXYCARBONYL, AZIDO, AMINE, AND AMIDE RADICALS; T IS SELECTED FROM ALKYL, CYCLOALKYL, ARYL, ALKARYL, AND ARALKYL RADICALS; A IS AN INTEGER FROM 1 TO 3; B IS AN INTEGER FROM 0 TO 2; C IS AN INTEGER FROM 1 TO 10; D IS AN INTEGER FROM 1 TO 3; AND A+B+D EQUALS 4;

-OOC-C(-R'')-N2, -OOC-N3, AND -SO2-N3

WHERE R'' IS SELECTED FROM HYDROGEN, ALKYL, CYCLOALKYL, ARYL AND -COOR" RADICALS; WHERE R" IS SELECTED FROM ALKYL, CYCLOALKYL, AND ARYL RADICALS.

8. 发明授权

US3562298A Dimeric azidophospha (iii)-carboranes 失效
标题翻译：二甲基氨基甲酸（III）-CARBORANES
公开(公告)号：US3562298A
公开(公告)日：1971-02-09
申请号：US3562298D
申请日：1967-10-09
申请人： OLIN CORP
发明人： ALEXANDER ROY P , SCHROEDER HANSJUERGEN A
IPC分类号： C07F5/02 , C07F9/6596 , C08G79/14 , C07C117/00 , C07D107/02
CPC分类号： C07F9/6596 , C07F5/027 , C08G79/14 , Y10S149/121
摘要： DIMERIC AZIDOPHOSPHA (III)-CARBORANES ARE PREPARED BY REACTING A DIMERIC HALOPHOSPHA (III)-CARBORANE, SUCH AS:

CL-P
WITH AN ALKALI METAL AZIDE SUCH AS SODIUM AZIDE IN THE PRESENCE OF AN INORGANIC LIQUID AND A TEMPERATURE RANGING FROM ABOUT -20*C. TO ABOUT +80*C. THE DIMERIC AZIDOPHOSPHA (III)-CARBORANES CAN BE CONDENSED WITH A DIPHOSPHINE TO YIELD VALUABLE POLYMERIC MATERIALS WHICH, WHEN COMPOUNDED WITH INERT MINERAL FILLERS AND PRESSURE MOLDED, ARE SUITABLE FOR USE IN HIGH PRESSURE AND HIGH TEMPERATURE APPLICATIONS.

9. 发明授权

US3527775A Tricyclohexyltin nitrate and azide 失效
标题翻译：硝酸苄酯和亚胺酸三丁酯
公开(公告)号：US3527775A
公开(公告)日：1970-09-08
申请号：US3527775D
申请日：1968-09-20
申请人： DOW CHEMICAL CO
发明人： BUBLITZ DONALD E
IPC分类号： C07F7/22 , C07C117/00
CPC分类号： C07F7/2204 , C07F7/2248

10. 发明授权

US4795593A 4-azido-4,4-dinitro-1-butanol and derivatives thereof 失效
标题翻译： 4-叠氮基-4,4-二硝基-1-丁醇及其衍生物
公开(公告)号：US4795593A
公开(公告)日：1989-01-03
申请号：US82775
申请日：1987-08-05
申请人： Milton B. Frankel , James F. Weber
发明人： Milton B. Frankel , James F. Weber
IPC分类号： C06B25/00 , C07C205/15 , C07C117/00
CPC分类号： C07C205/15 , C06B25/00 , C07C205/44 , C07C247/00
摘要： There is provided the compound 4-azido-4,4-dinitro-1-butanol (ADNBOH) and a method for making same which comprises reacting trinitromethane and acrolein at a reduced temperature to provide 4,4,4-trinitro-butyraldehyde (TNBAl), reducing the TNBSl to provide 4,4-trinitro-1-butanol (TNBOH) which is further reduced to provide 4,4-dinitro-1-butanol (DNBOH), reacting the DNBOH with acetyl chloride to provide 4,4-dinitro-1-butyl acetate (DNBAc), reacting the DNBAc with an alkali metal azide in an electrolysis cell to provide 4-azido-4,4-dinitro-1-butyl acetate (ADNBAc) and reacting the ADNBAc with a lower alcohol and recovering the 4-azido-4,4-dinitro-1-butanol (ADNBOH).Also provided are several azidodinitro derivatives of 4-azido-4,4-dinitro-1-butanol and methods for making same.
摘要翻译：提供化合物4-叠氮基-4,4-二硝基-1-丁醇（ADNBOH）及其制备方法，其包括在降低的温度下使三硝基甲烷和丙烯醛反应，得到4,4,4-三硝基丁醛（TNBAl ），还原TNBS1以提供4 - 三硝基-1-丁醇（TNBOH），进一步还原以提供4,4-二硝基-1-丁醇（DNBOH），使DNBOH与乙酰氯反应，得到4,4-二硝基-1-丁醇二丁基-1-丁基乙酸酯（DNBAc），使DNBAc与电解槽中的碱金属叠氮化物反应，得到4-叠氮基-4,4-二硝基-1-丁酸乙酯（ADNBAc），并使ADNBAc与低级醇和回收4-叠氮基-4,4-二硝基-1-丁醇（ADNBOH）。还提供了4-叠氮基-4,4-二硝基-1-丁醇的几种叠氮基硝基衍生物及其制备方法。

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