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1. 发明授权

US07199270B2 Method for the separation of methyl mercaptan from reaction gas mixtures 有权
标题翻译：从反应气体混合物中分离甲硫醇的方法
公开(公告)号：US07199270B2
公开(公告)日：2007-04-03
申请号：US11016130
申请日：2004-12-17
申请人： Alexander Möller , Wolfgang Böck , Stephan Rautenberg , Hans-Joachim Hasselbach , Wolfgang Taugner , Harald Heinzel , Theo Zarfl
发明人： Alexander Möller , Wolfgang Böck , Stephan Rautenberg , Hans-Joachim Hasselbach , Wolfgang Taugner , Harald Heinzel , Theo Zarfl
IPC分类号： C07C319/00
CPC分类号： C07C319/08 , C07C319/18 , C07C319/28 , C07C321/04 , C07C323/22
摘要： The invention relates to a method for the separation of methyl mercaptan from reaction gas mixtures obtained by means of the catalytic conversion of H2S with methanol, by means of converting the methyl mercaptan into MMP in the presence of the byproducts with acrolein, and separating the same.
摘要翻译：本发明涉及通过在丙烯醛的副产物存在下将甲硫醇转化为MMP，将甲硫醇与通过H 2 S与甲醇的催化转化得到的反应气体混合物分离的方法，。

2. 发明申请

US20050137426A1 Method for the separation of methyl mercaptan from reaction gas mixtures 有权
标题翻译：从反应气体混合物中分离甲硫醇的方法
公开(公告)号：US20050137426A1
公开(公告)日：2005-06-23
申请号：US11016130
申请日：2004-12-17
申请人： Alexander Moller , Wolfgang Bock , Stephan Rautenberg , Hans-Joachim Hasselbach , Wolfgang Taugner , Harald Heinzel , Theo Zarfl
发明人： Alexander Moller , Wolfgang Bock , Stephan Rautenberg , Hans-Joachim Hasselbach , Wolfgang Taugner , Harald Heinzel , Theo Zarfl
IPC分类号： C07C319/18 , C07C319/28 , C07C321/04 , C07C323/22 , C07C319/08
CPC分类号： C07C319/08 , C07C319/18 , C07C319/28 , C07C321/04 , C07C323/22
摘要： The invention relates to a method for the separation of methyl mercaptan from reaction gas mixtures obtained by means of the catalytic conversion of H2S with methanol, by means of converting the methyl mercaptan into MMP in the presence of the byproducts with acrolein, and separating the same.
摘要翻译：本发明涉及通过在丙烯醛的副产物存在下将甲硫醇转化为MMP，将甲硫醇与通过H 2 S与甲醇的催化转化得到的反应气体混合物分离的方法，。

3. 发明授权

US06008409A Method for obtaining 2-hydroxy-4-methylthiobutyric acid (MHA) which is stable in storage 失效
标题翻译：获得储存稳定的2-羟基-4-甲硫基丁酸（MHA）的方法
公开(公告)号：US06008409A
公开(公告)日：1999-12-28
申请号：US999000
申请日：1997-12-29
申请人： Hans-Albrechl Hasseberg , Hans-Joachim Hasselbach , Klaus Huthmacher , Volker Hafner , Harald Heinzel , Axel Ronneburg
发明人： Hans-Albrechl Hasseberg , Hans-Joachim Hasselbach , Klaus Huthmacher , Volker Hafner , Harald Heinzel , Axel Ronneburg
IPC分类号： C07C319/20 , A23K20/105 , C07C319/26 , C07C319/28 , C07C323/52 , C07C315/00
CPC分类号： C07C319/28 , A23K20/105 , C07C319/26
摘要： A method for obtaining 2-hydroxy-4-methylthiobutyric acid (methionine-hydroxy analog, MHA) in primarily free form which is stable in storage by distilling a product solution containing MHA and by producing MHA product mixtures with improved storage stability from such a distillate. The distillate can be produced directly starting from MHA raw products from any MHA production process, which can optionally also contain solvent or water. The starting material may also be a commercial MHA product.
摘要翻译：获得主要游离形式的2-羟基-4-甲硫基丁酸（甲硫氨酸 - 羟基类似物，MHA）的方法，其通过蒸馏含有MHA的产物溶液并通过生产具有改善的储存稳定性的这种馏出物的MHA产物混合物而在储存中稳定。馏出物可以从任何MHA生产过程的MHA原始产品直接生产，其可任选地还含有溶剂或水。起始材料也可以是商业MHA产品。

4. 发明申请

US20050267314A1 Process for producing methionine 有权
标题翻译：生产甲硫氨酸的方法
公开(公告)号：US20050267314A1
公开(公告)日：2005-12-01
申请号：US11054424
申请日：2005-02-10
申请人： Dieter Buss , Ron Stockfleth , Martin Korfer , Jurgen Stock , Ralf Goedecke , Hans-Joachim Hasselbach , Gundolf Hornung
发明人： Dieter Buss , Ron Stockfleth , Martin Korfer , Jurgen Stock , Ralf Goedecke , Hans-Joachim Hasselbach , Gundolf Hornung
IPC分类号： C07C319/20 , C07C319/28 , C07C323/58 , C07C323/25
CPC分类号： C07C319/28 , C07C319/20 , C07C323/58
摘要： The present invention is directed to an improved process for producing methionine in which the by-product methionyl-methionine is quickly converted to the product methionine by a hydrolysis reaction. The process is performed at high temperatures (200° C. to 280° C.) and short residence times (20 s to 200 s) and results in an improved yield of end product methionine.
摘要翻译：本发明涉及一种生产甲硫氨酸的改进方法，其中副产物甲硫氨酰 - 甲硫氨酸通过水解反应快速转化为产物甲硫氨酸。该过程在高温（200℃至280℃）和短停留时间（20秒至200秒）下进行，并导致最终产物甲硫氨酸的产率提高。

5. 发明授权

US07655072B2 Process for purifying CO2 gas streams 有权
标题翻译：二氧化碳气流净化方法
公开(公告)号：US07655072B2
公开(公告)日：2010-02-02
申请号：US11185367
申请日：2005-07-20
申请人： Hans-Joachim Hasselbach , Jose Vanrobaeys , Martin Körfer
发明人： Hans-Joachim Hasselbach , Jose Vanrobaeys , Martin Körfer
IPC分类号： B01D53/14
CPC分类号： B01D53/62 , C07C319/20 , Y02C10/04 , C07C323/58
摘要： A process for purifying CO2 offgas streams to free them of chemical compounds, and to the recycling of the purified gas streams into the production process.
摘要翻译：一种净化二氧化碳废气流以释放其化学化合物的方法，以及将净化气流再循环到生产过程中。

6. 发明申请

US20060016334A1 Process for purifying CO2 gas streams 有权
标题翻译：二氧化碳气流净化方法
公开(公告)号：US20060016334A1
公开(公告)日：2006-01-26
申请号：US11185367
申请日：2005-07-20
申请人： Hans-Joachim Hasselbach , Jose Vanrobaeys , Martin Korfer
发明人： Hans-Joachim Hasselbach , Jose Vanrobaeys , Martin Korfer
IPC分类号： B01D53/14
CPC分类号： B01D53/62 , C07C319/20 , Y02C10/04 , C07C323/58
摘要： A process for purifying CO2 offgas streams to free them of chemical compounds, and to the recycling of the purified gas streams into the production process.
摘要翻译：一种纯化CO 2废气流以释放其化学化合物的方法，以及将纯化气流再循环到生产过程中。

7. 发明授权

US5049283A Method for the recovery of aqueous solutions of free, neutral .alpha.-amino acids from aqueous solutions of their alkali-metal salts 失效
标题翻译：从其碱金属盐的水溶液中回收游离的中性α-氨基酸的水溶液的方法
公开(公告)号：US5049283A
公开(公告)日：1991-09-17
申请号：US483048
申请日：1990-02-21
申请人： Hans-Joachim Hasselbach , Axel Kleeman , Herbert Klenk , Horst Weigel
发明人： Hans-Joachim Hasselbach , Axel Kleeman , Herbert Klenk , Horst Weigel
IPC分类号： C07C227/18 , B01D15/04 , C07C227/16 , C07C227/40 , C07C229/08
CPC分类号： C07C227/16
摘要： Aqueous solutions of free, neutral .alpha.-amino acids are recovered from aqueous solutions of their alkali-metal salts. Two equally large rectifying columns filled with a strongly acidic cation exchanger in the H.sup.+ form are used, the discharge of the first column being connected to the head of the second column. The solution of the alkali-metal salt is at first delivered to the head of the first column, then the residual solution, reduced by the alkali-metal cations adsorbed in the exchanger, is displaced to the second column by means of the addition of water. A product-free forerun is first separated at the discharge of the second column and, when free .alpha.-amino acid begins to exit in the flow-off from the second column, the receiver is changed and the delivery of water to the head of the first column continues further until a mixed pH between 5 and 7 has been achieved in the receiver. Then, the previously first column is decoupled and regenerated, the previously second column, which is now the first column, is coupled to a freshly regenerated column as second column and the entire process is repeated as often as desired.
摘要翻译：游离的中性α-氨基酸的水溶液从其碱金属盐的水溶液中回收。使用填充有H +形式的强酸性阳离子交换器的两个同等大的精馏塔，第一塔的排放物连接到第二塔的头部。首先将碱金属盐的溶液输送到第一塔的头部，然后通过吸附在交换器中的碱金属阳离子还原的残留溶液通过加入水而置换到第二塔。首先在第二柱的排出口处分离出无产物的前驱体，当游离的α-氨基酸在从第二塔的流出物中开始离开时，接收器被改变并且将水输送到第一列继续进行，直到在接收器中达到5和7之间的混合pH。然后，先前的第一列被解耦和再生，先前的第二列（现在是第一列）被耦合到作为第二列的新鲜再生的列，并且整个过程根据需要经常重复。

8. 发明授权

US07119228B2 Process for producing methionine 有权
标题翻译：生产甲硫氨酸的方法
公开(公告)号：US07119228B2
公开(公告)日：2006-10-10
申请号：US11054424
申请日：2005-02-10
申请人： Dieter Buss , Ron Stockfleth , Martin Körfer , Jürgen Stock , Ralf Goedecke , Hans-Joachim Hasselbach , Gundolf Hornung
发明人： Dieter Buss , Ron Stockfleth , Martin Körfer , Jürgen Stock , Ralf Goedecke , Hans-Joachim Hasselbach , Gundolf Hornung
IPC分类号： C07C51/00
CPC分类号： C07C319/28 , C07C319/20 , C07C323/58
摘要： The present invention is directed to an improved process for producing methionine in which the by-product methionyl-methionine is quickly converted to the product methionine by a hydrolysis reaction. The process is performed at high temperatures (200° C. to 280° C.) and short residence times (20 s to 200 s) and results in an improved yield of end product methionine.
摘要翻译：本发明涉及一种生产甲硫氨酸的改进方法，其中副产物甲硫氨酰 - 甲硫氨酸通过水解反应快速转化为产物甲硫氨酸。该过程在高温（200℃至280℃）和短停留时间（20秒至200秒）下进行，并导致最终产物甲硫氨酸的产率提高。

9. 发明授权

US06265617B1 Process for the preparation of 3,5,5-trimethylcyclohexa-3-en-1-one (&bgr;-isophorone) by isomerization of 3,5,5- trimethylcyclohexa-2-en-1-one (&agr;-isophorone) 失效
标题翻译：通过3,5,5-三甲基环己-2-烯-1-酮（α-异佛尔酮）的异构化制备3,5,5-三甲基环己-3-烯-1-酮（β-异佛尔酮）的方法
公开(公告)号：US06265617B1
公开(公告)日：2001-07-24
申请号：US09310971
申请日：1999-05-13
申请人： Steffen Krill , Stephan Kretz , Hans-Joachim Hasselbach , Klaus Huthmacher , Rainer Hahn , Hermann Schmitt
发明人： Steffen Krill , Stephan Kretz , Hans-Joachim Hasselbach , Klaus Huthmacher , Rainer Hahn , Hermann Schmitt
IPC分类号： C07C4500
CPC分类号： C07C45/67 , C07C45/82 , C07C49/603
摘要： A process for the preparation of 3,5,5-trimethylcyclohexa-3-en-1-one (&bgr;-isophorone) by isomerization of 3,5,5-trimethylcyclohexa-2-en-1-one (&agr;-isophorone) in the liquid phase in the presence of a salt-like or organometallic catalyst. By using catalytic quantities of alkali-metal salts or alkaline-earth salts and/or their organometallic compounds, and without addition of a further auxiliary substance, the space-time yield in the preparation of &bgr;-isophorone is high. &bgr;-Isophorone is particularly suitable as an intermediate product for the preparation of ketoisophorone.
摘要翻译：通过3,5,5-三甲基环己-2-烯-1-酮（α-异佛尔酮）异构化制备3,5,5-三甲基环己-3-烯-1-酮（β-异佛尔酮）的方法在盐状或有机金属催化剂存在下的液相。通过使用催化量的碱金属盐或碱土金属盐和/或其有机金属化合物，并且不加入另外的辅助物质，β-异佛尔酮的制备中的时空产率高。 β-异佛尔酮特别适合用作制备酮异二酮的中间产物。

10. 发明授权

US5990349A Process for the preparation of D,L-methionine or the salt thereof 失效
标题翻译：制备D，L-甲硫氨酸或其盐的方法
公开(公告)号：US5990349A
公开(公告)日：1999-11-23
申请号：US37020
申请日：1998-03-09
申请人： Friedhelm Geiger , Baudouin Halsberghe , Hans-Joachim Hasselbach , Klaus Hentschel , Klaus Huthmacher , Martin Korfer , Sven-Peter Mannsfeld , Herbert Tanner , Ferdinand Theissen , Jose Vanrobaeys , Klaus Willigerodt
发明人： Friedhelm Geiger , Baudouin Halsberghe , Hans-Joachim Hasselbach , Klaus Hentschel , Klaus Huthmacher , Martin Korfer , Sven-Peter Mannsfeld , Herbert Tanner , Ferdinand Theissen , Jose Vanrobaeys , Klaus Willigerodt
IPC分类号： C07C319/20 , C07C319/28 , C07C323/58 , C07D233/76 , C07C321/00 , C07C315/00
CPC分类号： C07C319/20 , C07C319/28 , C07D233/76
摘要： A process for the preparation of methionine or a salt of methionine by reaction of the components 3-methylmercaptopropionaldhyde, hydrogen cyanide, ammonia and carbon dioxide or components from which the above-mentioned components can be prepared, optionally in the presence of water, to 5-(2-methylmercaptoethyl)-hydantoin and further reaction thereof to methionine or the salt thereof, characterised in that the reaction of the components is initiated by means of at least one premixture in such a way that a first mixture is formed containing at least the predominant proportion (at least 5/10) of the 3-methylmercaptopropionaldeyde and at least 1/10 of the hydrogen cyanide component or corresponding quantities of components from which these components can be prepared, and less than 5/10 of one of the components ammonia, carbon dioxide or of the components from which ammonia or carbon dioxide can be prepared, and in that this first mixture is combined with the other component(s) for the reactive conversion to 5-(2-methylmercaptoethyl)-hydantoin, wherein this (these) latter component(s) may be premixed in one or more other mixtures.
摘要翻译：通过将3-甲基巯基丙酸，氰化氢，氨和二氧化碳或可由其制备上述组分的组分，任选地在水存在下，将组分3-甲基巯基丙酸，氰化氢，氨和二氧化碳或组分反应制备甲硫氨酸或甲硫氨酸的方法， - （2-甲基巯基乙基） - 乙内酰脲及其与甲硫氨酸或其盐的反应，其特征在于，组分的反应通过至少一种预混物引发，使得形成第一混合物至少含有 3-甲基巯基丙酸的主要比例（至少+ E，fra 5/10 + EE）和氰化氢组分的至少+ E，fra 1/10 + EE或可以制备这些组分的相应量的组分，并且可以制备氨，二氧化碳或其中可以制备氨或二氧化碳的组分之一的小于+ E，fra 5/10 + EE，并且因为该第一混合物与反应转化成5-（2-甲基巯基乙基） - 乙内酰脲的其它组分，其中这些（这些）后一种组分可以在一种或多种其它混合物中预混合。

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