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1. 发明授权

US06344348B1 Process for the production of aspartic acid condensate 失效
标题翻译：生产天冬氨酸缩合物的方法
公开(公告)号：US06344348B1
公开(公告)日：2002-02-05
申请号：US09284234
申请日：1999-11-22
申请人： Aharon Eyal , Robert J. Jansen , Asher Vitner , Pierre Cami , Emmanuel Mailly , Thomas Chattaway , Bruno Jarry , Joelle More
发明人： Aharon Eyal , Robert J. Jansen , Asher Vitner , Pierre Cami , Emmanuel Mailly , Thomas Chattaway , Bruno Jarry , Joelle More
IPC分类号： C12P1320
CPC分类号： C12P13/20 , C08G73/1092
摘要： The invention provides a process for the production of aspartic acid poly-condensate from a carbohydrate comprising the steps of: fermenting a carbohydrate-containing medium by means of a fumaric acid-producing microorganism, whereby a fumarate-containing fermentation liquor is formed; forming a purified ammonium fumarate solution from the fumarate-containing fermentation liquor; enzymatically converting the purified ammonium fumarate into purified ammonium aspartate; heating an aqueous solution of an aspartate salt derived from the purified ammonium aspartate whereby water is removed, an aspartic acid condensate is formed and a second product is formed, which second product is basic and contains the cation of the aspartate salt; and removing and using the basic second product as a reagent in another step of the process.
摘要翻译：本发明提供了一种从碳水化合物制备天冬氨酸聚缩合物的方法，包括以下步骤：通过产生富马酸的微生物发酵含碳水化合物的培养基，从而形成含富马酸的发酵液; 从含富马酸的发酵液中形成纯化的富马酸铵溶液; 将纯化的富马酸铵酶促转化成纯天然天冬氨酸铵; 加热源自纯化天冬氨酸铵的天冬氨酸盐的水溶液，由此除去水，形成天冬氨酸缩合物并形成第二产物，该第二产物是碱性的，并含有天冬氨酸盐的阳离子; 以及在该方法的另一步骤中除去和使用碱性第二产物作为试剂。

2. 发明授权

US07763232B2 Methods for production of titanium oxide particles, and particles and preparations produced thereby 有权
标题翻译：生产氧化钛颗粒的方法，以及由此制备的颗粒和制剂
公开(公告)号：US07763232B2
公开(公告)日：2010-07-27
申请号：US12096143
申请日：2006-12-21
申请人： Asher Vitner , Aharon Eyal
发明人： Asher Vitner , Aharon Eyal
IPC分类号： C01G23/047 , C01G23/053 , C01G23/04
CPC分类号： C01G23/053 , B82Y30/00 , C01G23/0532 , C01G23/0536 , C01G23/08 , C01P2004/62 , C01P2004/64 , C01P2006/12
摘要： The invention provides a method for the formation of small-size titanium oxide particles, comprising the steps of a) preparing a starting aqueous solution comprising at least one of titanic ions and complexes thereof, at a concentration of at least 0.1% w/w titanium; b) maintaining the solution at a temperature lower than 70° C. for a retention time in which hydrolysis takes place, the extent of the hydrolysis being sufficient to produce O.i mmol protons per mmol of titanium present in solution, wherein the time does not exceed 14 days, to form a system containing a retained solution; and c) adjusting the conditions in the system by at least one of the steps of: i) heating the retained solution to elevate the temperature thereof by at least 1° C.; ii) changing the pH of the retained solution by at least 0.1 units; and iii) diluting the retained solution by at least 20% whereby there are formed particles, wherein the majority of the particles formed are between about 2 nm and about 500 nm in size.
摘要翻译：本发明提供一种形成小尺寸氧化钛颗粒的方法，包括以下步骤：a）制备含有至少0.1％w / w钛的钛离子及其配合物中的至少一种的起始水溶液 ; b）将溶液保持在低于70℃的温度下进行水解的停留时间，水解程度足以产生溶解在溶液中的每毫摩尔钛的O 1 mmol质子，其中时间不超过 14天，形成含有保留溶液的体系; 以及c）通过以下步骤中的至少一个步骤来调节所述系统中的条件：i）加热所述保留的溶液以将其温度升高至少1℃; ii）将保留溶液的pH值改变至少0.1单位; 和iii）将保留的溶液稀释至少20％，由此形成颗粒，其中形成的大部分颗粒的尺寸在约2nm和约500nm之间。

3. 发明申请

US20080311031A1 Methods For Production of Metal Oxide Nano Particles With Controlled Properties, and Nano Particles and Preparations Produced Thereby 审中-公开
标题翻译：具有控制性能的金属氧化物纳米颗粒的制备方法，以及由此产生的纳米颗粒和制备物
公开(公告)号：US20080311031A1
公开(公告)日：2008-12-18
申请号：US12096157
申请日：2006-12-21
申请人： Asher Vitner , Aharon Eyal
发明人： Asher Vitner , Aharon Eyal
IPC分类号： C01B13/14 , C01F7/02 , C01G9/02 , C01G19/02 , C01G45/02 , C01G3/02
CPC分类号： C09C3/00 , B82Y30/00 , C01G1/02 , C01P2002/04 , C01P2004/10 , C01P2004/32 , C01P2004/51 , C01P2004/54 , C01P2004/61 , C01P2004/62 , C01P2004/64 , C01P2006/12
摘要： The invention provides a method for the formation of small-size metal oxide particles, comprising the steps of a) preparing a starting aqueous solution comprising at least one of metallic ions and complexes thereof, at a concentration of at least 0.1 % w/w of the metal component; b) maintaining the solution at a temperature lower than 50° C. for a retention time in which hydrolysis takes place, the extent of the hydrolysis being sufficient to produce O.1 mmol protons per mmol of metal present in solution, wherein the time does not exceed 14 days, to form a system containing a retained solution; and c) adjusting the conditions in the system by at least one of the steps of: i) heating the retained solution to elevate the temperature thereof by at least 1° C.; ii) changing the pH of the retained solution by at least 0.1 units; and iii) diluting the retained solution by at least 20% whereby there are formed particles, wherein the majority of the particles formed are between about 2 nm and about 500 nm in size.
摘要翻译：本发明提供了一种形成小尺寸金属氧化物颗粒的方法，包括以下步骤：a）制备以至少0.1％w / w的浓度制备包含至少一种金属离子及其配合物的起始水溶液，金属部件; b）将溶液保持在低于50℃的温度下进行水解的保留时间，水解程度足以产生每毫摩尔存在于溶液中的金属O.1mmol质子，其中时间不超过14天，形成含有保留溶液的体系; 以及c）通过以下步骤中的至少一个步骤来调节所述系统中的条件：i）加热所述保留的溶液以将其温度升高至少1℃; ii）将保留溶液的pH值改变至少0.1单位; 和iii）将保留的溶液稀释至少20％，由此形成颗粒，其中形成的大部分颗粒的尺寸在约2nm和约500nm之间。

4. 发明申请

US20140190470A1 METHODS AND SYSTEMS FOR PROCESSING A SUCROSE CROP AND SUGAR MIXTURES 有权
标题翻译：用于加工蔗糖和糖混合物的方法和系统
公开(公告)号：US20140190470A1
公开(公告)日：2014-07-10
申请号：US13807479
申请日：2011-06-28
申请人： Aharon Eyal , Robert Jansen , Asher Vitner , Revital Mali
发明人： Aharon Eyal , Robert Jansen , Asher Vitner , Revital Mali
IPC分类号： C13K11/00 , C13K1/02
CPC分类号： C13K11/00 , C13B5/04 , C13B10/02 , C13K1/02 , C13K13/00 , C13K13/002
摘要： A method comprising: (a) providing a partially processed sucrose crop product containing at least 2% optionally at least 5% of the sucrose content of said crop at harvest on a dry solids basis, cellulose and lignin; (b) hydrolyzing said partially processed crop product with HCl to produce an acid hydrolyzate stream and a lignin stream; and (c) de-acidifying said hydrolyzate stream to produce a de-acidified sugar solution and an HCl recovery stream. Additional, methods, systems and sugar mixtures are also disclosed.
摘要翻译：一种方法，包括：（a）提供部分加工的蔗糖作物产品，其在干固体收获时提供含有至少2％任选至少5％的所述作物蔗糖含量的纤维素和木质素; （b）用HCl水解所述部分加工的作物产物以产生酸水解产物流和木质素流; 和（c）使所述水解产物流脱酸以产生脱酸糖溶液和HCl回收流。还公开了方法，系统和糖混合物。

5. 发明申请

US20130028832A1 METHODS FOR THE SEPARATION OF HCL FROM A CARBOHYDRATE AND COMPOSITIONS PRODUCED THEREBY 审中-公开
标题翻译：从碳酸氢盐分离HCL的方法及其制备的组合物
公开(公告)号：US20130028832A1
公开(公告)日：2013-01-31
申请号：US13577213
申请日：2011-02-06
申请人： Aharon Eyal , Asher Vitner , Revital Mali
发明人： Aharon Eyal , Asher Vitner , Revital Mali
IPC分类号： C01B7/01 , C09K3/00
CPC分类号： C01B7/0731 , C01B7/0737 , C13K1/02 , Y02E50/16
摘要： The present invention provides an organic phase composition comprising: (a) a first solvent (S1) characterized by a water solubility of less than 10% and by at least one of (a1) having a polarity related component of Hoy's cohesion parameter (delta-P) between 5 and 10 MPa1/2 and (b1) having a Hydrogen bonding related component of Hoy's cohesion parameter (delta-H) between 5 and 20 MPa1/2; (b) a second solvent (S2) characterized by a water solubility of at least 30% and by at least one of (a2) having a delta-P greater than 8 MPa1/2 and (b2) having a delta-H greater than 12 MPa1/2; (c) water; (d) HCl; and (e) a carbohydrate.
摘要翻译：本发明提供一种有机相组合物，其包含：（a）第一溶剂（S1），其特征在于水溶解度小于10％，和至少一种（a1）具有Hoy的内聚参数（δ- P）为5〜10MPa1 / 2，（b1）具有5〜20MPa1 / 2的Hoy粘附参数（δ-H）的氢键相关成分; （b）第二溶剂（S2），其特征在于水溶解度为至少30％，并且至少一种（a2）具有大于8MPa1 / 2的δ-P和（b2），其中δ-H大于 12 MPa1 / 2; （c）水; （d）HCl; 和（e）碳水化合物。

6. 发明申请

US20090158895A1 Process for the Production of Titanium Products 有权
标题翻译：钛产品生产工艺
公开(公告)号：US20090158895A1
公开(公告)日：2009-06-25
申请号：US12083362
申请日：2006-10-15
申请人： Asher Vitner , Aharon Eyal , Revital Mali
发明人： Asher Vitner , Aharon Eyal , Revital Mali
IPC分类号： C01B17/96 , C01G23/04 , C01G25/06 , C22B34/12
CPC分类号： C01G23/002 , B82Y30/00 , C01G23/008 , C01G23/04 , C01G23/0532 , C01G49/009 , C01G49/14 , C01P2004/62 , C01P2004/64 , C01P2006/80
摘要： The invention provides a method for the Industrial purification of a titanium feed stream of purity P1, by the formation of a titanium-double-salt precipitate of purity P2 and a titanium solution with purity P3, wherein P2>P1>P3, the method comprising the steps of: i. forming, from the feed, a medium comprising water, titanium ion, a cation selected from the group consisting of ammonium, cations of alkali metals, protons and a combination thereof, and an anion selected from the group consisting of OH, SO4, HSO4, halides and a combination thereof, which formed medium is further characterized by the presence of (a) a double-salt precipitate comprising titanium ion, at least one of the cations and at least one of the anions; and (b) a titanium solution; and wherein the concentration of the anion in the titanium solution is higher than 15% and the ratio between the concentrations of the cation and the anion in the titanium solution is higher than 0.2 and lower than 1.6; and ii. separating at least a portion of the precipitate from the solution.
摘要翻译：本发明提供了通过形成纯度为P2的钛 - 双盐沉淀物和纯度为P3的钛溶液（其中P2> P1> P3），纯化P1纯钛进料流的工业纯化方法，该方法包括步骤：i。从进料形成包含水，钛离子，选自铵，碱金属阳离子，质子及其组合的阳离子和选自OH，SO 4，HSO 4，形成介质的卤化物及其组合的特征还在于存在（a）包含钛离子，至少一种阳离子和至少一种阴离子的双盐沉淀物; 和（b）钛溶液; 并且其中钛溶液中阴离子的浓度高于15％，并且钛溶液中阳离子和阴离子的浓度之比高于0.2且低于1.6; 和ii。从溶液中分离出至少一部分沉淀物。

7. 发明申请

US20080305025A1 Methods for Production of Metal Oxide Nano Particles, and Nano Particles and Preparations Produced Thereby 审中-公开
标题翻译：金属氧化物纳米颗粒的制造方法以及由此制备的纳米颗粒和制剂
公开(公告)号：US20080305025A1
公开(公告)日：2008-12-11
申请号：US12096154
申请日：2006-12-21
申请人： Asher Vitner , Aharon Eyal
发明人： Asher Vitner , Aharon Eyal
IPC分类号： C01F17/00 , C01B13/18 , C01G3/02 , C01G45/02 , C01G37/02 , C01G39/02 , C01G25/02 , C01G19/02 , C01G9/02 , C01F7/02 , C01F5/00 , C01G31/02 , C01G11/00 , C01G53/04 , C01B33/113 , B01J19/10 , B01J19/12 , C01G51/04
CPC分类号： C01B13/36 , B01J23/16 , B01J35/0013 , B01J37/03 , B82Y30/00 , C01G1/02 , C01G3/02 , C01G9/02 , C01G11/02 , C01G19/02 , C01G25/02 , C01G31/00 , C01G37/02 , C01G37/033 , C01G39/02 , C01G45/02 , C01G51/04 , C01G53/04 , C01G55/004 , C01P2002/04 , C01P2004/10 , C01P2004/20 , C01P2004/32 , C01P2004/51 , C01P2004/62 , C01P2004/64 , C01P2006/12 , C01P2006/40 , C01P2006/42 , C01P2006/80
摘要： The invention provides a method for the formation of small-size metal oxide particles, comprising the steps of: a) preparing a starting aqueous solution comprising at least one of metallic ion and complexes thereof, at a concentration of at least 0.1% w/w of the metal component; b) preparing a modifying aqueous solution having a temperature greater than 50° C.; c) contacting the modifying aqueous solution with the starting aqueous solution in a continuous mode in a mixing chamber to form a-modified system; d) removing the modified system from the mixing chamber in a plug-flow mode; wherein the method is characterized in that: i) the residence time in the mixing chamber is less than about 5 minutes; and iii) there are formed particles or aggregates thereof, wherein the majority of the particles formed are between about 2 nm and about 500 nm in size.
摘要翻译：本发明提供一种形成小尺寸金属氧化物颗粒的方法，包括以下步骤：a）以至少0.1％w / w的浓度制备包含至少一种金属离子及其配合物的起始水溶液的金属组分; b）制备温度大于50℃的改性水溶液; c）在混合室中以连续模式将改性水溶液与起始水溶液接触以形成改性体系; d）以插塞模式从混合室中取出改性体系; 其特征在于：i）在混合室中的停留时间小于约5分钟; 和iii）形成其颗粒或聚集体，其中形成的大部分颗粒的尺寸为约2nm至约500nm。

8. 发明授权

US09476106B2 Methods and systems for processing a sucrose crop and sugar mixtures 有权
标题翻译：用于加工蔗糖作物和糖混合物的方法和系统
公开(公告)号：US09476106B2
公开(公告)日：2016-10-25
申请号：US13807479
申请日：2011-06-28
申请人： Aharon Eyal , Robert Jansen , Asher Vitner , Revital Mali
发明人： Aharon Eyal , Robert Jansen , Asher Vitner , Revital Mali
IPC分类号： C13K11/00 , C13K1/02 , C13K13/00 , C13B10/02 , C13B5/04
CPC分类号： C13K11/00 , C13B5/04 , C13B10/02 , C13K1/02 , C13K13/00 , C13K13/002
摘要： A method comprising: (a) providing a partially processed sucrose crop product containing at least 2% optionally at least 5% of the sucrose content of said crop at harvest on a dry solids basis, cellulose and lignin; (b) hydrolyzing said partially processed crop product with HCl to produce an acid hydrolyzate stream and a lignin stream; and (c) de-acidifying said hydrolyzate stream to produce a de-acidified sugar solution and an HCl recovery stream. Additional, methods, systems and sugar mixtures are also disclosed.
摘要翻译：一种方法，包括：（a）提供部分加工的蔗糖作物产品，其在干固体收获时提供含有至少2％任选至少5％的所述作物蔗糖含量的纤维素和木质素; （b）用HCl水解所述部分加工的作物产物以产生酸水解产物流和木质素流; 和（c）使所述水解产物流脱酸以产生脱酸糖溶液和HCl回收流。还公开了方法，系统和糖混合物。

9. 发明申请

US20130028833A1 METHOD FOR PREPARING A HYDROLYZATE 审中-公开
标题翻译：制备水解产物的方法
公开(公告)号：US20130028833A1
公开(公告)日：2013-01-31
申请号：US13577215
申请日：2011-02-06
申请人： Aharon Eyal , Asher Vitner , Revital Mali
发明人： Aharon Eyal , Asher Vitner , Revital Mali
IPC分类号： C01B7/01 , C09K3/00
CPC分类号： C01B7/0737
摘要： The present invention provides an organic phase composition comprising (f) a first solvent (S1) characterized by water solubility of less than 10% and by at least one of (a1) having a polarity related component of Hoy's cohesion parameter (delta-P) between 5 and 10 mPa1/2 and (b1) having a Hydrogen bonding related component of Hoy's cohesion parameter (delta-H) between 5 and 20 MPa1/2; (g) a second solvent (S2) characterized by water solubility of at least 30% and by at least one of (a2) having a delta-P greater than 8 MPa1/2 and (b2) having a delta-H greater than 12 MPa1/2; (h) water (i) HCl, and (j) a chloride salt.
摘要翻译：本发明提供一种有机相组合物，其包含（f）第一溶剂（S1），其特征在于水溶解度小于10％，和至少一种（a1）具有Hoy的内聚参数（Δ-P）的极性相关成分， 5和10mPa1 / 2之间，（b1）具有5至20MPa1 / 2的Hoy粘附参数（δ-H）的氢键相关组分; （g）第二溶剂（S2），其特征在于水溶解度为至少30％，并且至少一种具有δ-P大于8MPa1 / 2的（a2）和（b2）具有大于12的Δ-H MPa1 / 2; （h）水（i）HCl，和（j）氯化物盐。

10. 发明申请

US20120301389A1 METHOD FOR THE SEPARATION OF A NON-VOLATILE STRONG ACID FROM A SALT THEREOF AND COMPOSITIONS PRODUCED THEREBY 审中-公开
标题翻译：从其盐分离非挥发性强酸的方法及其制备的组合物
公开(公告)号：US20120301389A1
公开(公告)日：2012-11-29
申请号：US13574641
申请日：2011-02-06
申请人： Aharon Eyal , Asher Vitner , Revital Mali , Carmi Raz
发明人： Aharon Eyal , Asher Vitner , Revital Mali , Carmi Raz
IPC分类号： C01B17/90 , C09K3/00
CPC分类号： C01B25/234 , C01B17/903 , C01B21/46
摘要： The present invention provides an organic phase composition comprising (a) a first solvent (S1) characterized by water solubility of less than 10% and by at least one of (a1) having a polarity related component of Hoy's cohesion parameter (delta-P) between 5 and 10 MPa1/2 and (b1) having a Hydrogen bonding related component of Hoy's cohesion parameter (delta-H) between 5 and 20 MPa1/2; (b) a second solvent (S2) characterized by a water solubility of at least 30% and by at least one of (a2) having delta-P greater than 8 MPa1/2 and (b2) having delta-H greater than 12 MPa1/2; (c) water; (d) a non-volatile strong acid; and (e) a salt thereof.
摘要翻译：本发明提供一种有机相组合物，其包含（a）第一溶剂（S1），其特征在于水溶性小于10％，和至少一种具有Hoy的内聚参数（Δ-P）的极性相关成分的（a1） 5〜10MPa1 / 2，（b1）具有5〜20MPa·1/2的Hoy粘结参数（δ-H）的氢键相关成分; （b）第二溶剂（S2），其特征在于水溶解度为至少30％，并且至少一种具有δ-P大于8MPa1 / 2的（a2）和（b2）具有大于12MPa1的Δ-H / 2; （c）水; （d）不挥发性强酸; 和（e）其盐。

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